On the thermal coarsening and transformation of nanoscale oxide inclusions in 316L stainless steel manufactured by laser powder bed fusion and its influence on impact toughness

Deng, Pu; Song, Miao; Yang, Jingfan; Pan, Qingyu; McAllister, Sarah; Li, Lin; Prorok, Barton C.; Lou, Xiaoyuan

doi:10.1016/j.msea.2022.142690

Title: On the thermal coarsening and transformation of nanoscale oxide inclusions in 316L stainless steel manufactured by laser powder bed fusion and its influence on impact toughness

Journal Article · 18 January 2022 · Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing

DOI: https://doi.org/10.1016/j.msea.2022.142690 · OSTI ID:1977464

^[1]; Song, Miao ^[2];

^[3];

^[4]; Li, Lin ^[4];

^[3];

^[3]

Auburn Univ., AL (United States); OSTI
Univ. of Michigan, Ann Arbor, MI (United States)
Auburn Univ., AL (United States)
Univ. of Alabama, Tuscaloosa, AL (United States)

The thermal evolution of nanoscale oxide inclusions in 316L stainless steel (SS) manufactured by laser powder bed fusion additive manufacturing (AM) was explored. The size, chemical composition, morphology, and distribution of the oxides were characterized as the function of heat treatment conditions. The study revealed the mechanistic driving force of the rapid oxide coarsening during recrystallization. Ostwald ripening governs oxide coarsening. The active grain boundary-oxide interaction at the early stage of recrystallization accelerated oxide coarsening via enhanced solute diffusion along grain boundaries. Pipe diffusion along dislocation cellular boundaries has a negligible contribution to oxide coarsening. At high temperatures (T> 1065 °C), although lattice diffusion primarily controlled the oxide growth, the contribution from the grain-boundary diffusion was necessary. The transformation from MnSiO₃ to CrMn₂O₄ took place in the un-recrystallized grains but was not observed when recrystallization started. The interaction of grain boundary and oxides during recrystallization resulted in a high fraction of oxides accumulated at grain boundaries. While oxide coarsening does not significantly alter the toughness value, grain-boundary oxides promote microvoid formation and intergranular fracture under Charpy impact in the recrystallized AM 316L SS.

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Research Organization:: General Electric Co., Boston, MA (United States)

Sponsoring Organization:: National Inst. of Standards and Technology (NIST); USDOE; USDOE Office of Nuclear Energy (NE)

Grant/Contract Number:: NE0008428

OSTI ID:: 1977464

Journal Information:: Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing, Journal Name: Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing Journal Issue: C Vol. 835; ISSN 0921-5093

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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36 MATERIALS SCIENCE
Austenitic stainless steel
Coarsening
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Heat treatment
Impact toughness
Laser-powder bed fusion additive manufacturing
Materials Science
Metallurgy & Metallurgical Engineering
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Title: On the thermal coarsening and transformation of nanoscale oxide inclusions in 316L stainless steel manufactured by laser powder bed fusion and its influence on impact toughness

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