Piezoelectric property of PZT nanofibers characterized by resonant piezo-force microscopy
Abstract
Nano-piezoelectric materials have drawn tremendous research interest. However, characterization of their piezoelectric properties, especially measuring the piezoelectric strain coefficients, remains a challenge. Normally, researchers use an AFM-based method to directly measure nano-materials’ piezoelectric strain coefficients. But, the extremely small piezoelectric deformation, the influence from the parasitic electrostatic force, and the environmental noise make the measurement results questionable. In this paper, a resonant piezo-force microscopy method was used to accurately measure the piezoelectric deformation from 1D piezoelectric nanofibers. During the experiment, the AFM tip was brought into contact with the piezoelectric sample and set to work at close to its first resonant frequency. A lock-in amplifier was used to pick up the sample’s deformation signal at the testing frequency. By using this technique, the piezoelectric strain constant d 33 of the Lead Zirconate Titanate (PZT) nanofiber with a diameter of 76 nm was measured. The result showed that d 33 of this PZT nanofiber was around 387 pm/V. Meanwhile, by tracking the piezoelectric deformation phase image, domain structures inside PZT nanofibers were identified.
- Authors:
-
[3];
[1]
- Stevens Institute of Technology, Hoboken, NJ (United States)
- City Univ. of New York (CUNY), NY (United States)
- Brookhaven National Lab. (BNL), Upton, NY (United States). National Synchrotron Light Source II (NSLS-II)
- State Univ. of New York (SUNY), Syracuse, NY (United States). Upstate Medical University
- Publication Date:
- Research Org.:
- Brookhaven National Laboratory (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1973504
- Alternate Identifier(s):
- OSTI ID: 1846856
- Report Number(s):
- BNL-224378-2023-JAAM
Journal ID: ISSN 2158-3226; TRN: US2314095
- Grant/Contract Number:
- SC0012704; AC02-98CH10886
- Resource Type:
- Accepted Manuscript
- Journal Name:
- AIP Advances
- Additional Journal Information:
- Journal Volume: 12; Journal Issue: 3; Journal ID: ISSN 2158-3226
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; electrical properties and parameters; amplifiers; electrostatics; electric power; PZT; microscopy; piezoelectric materials; nanofiber; nanowires
Citation Formats
Zhang, Guitao, Chen, Xi, Xu, Weihe, Yao, Wei-Dong, and Shi, Yong. Piezoelectric property of PZT nanofibers characterized by resonant piezo-force microscopy. United States: N. p., 2022.
Web. doi:10.1063/5.0081109.
Zhang, Guitao, Chen, Xi, Xu, Weihe, Yao, Wei-Dong, & Shi, Yong. Piezoelectric property of PZT nanofibers characterized by resonant piezo-force microscopy. United States. https://doi.org/10.1063/5.0081109
Zhang, Guitao, Chen, Xi, Xu, Weihe, Yao, Wei-Dong, and Shi, Yong. Tue .
"Piezoelectric property of PZT nanofibers characterized by resonant piezo-force microscopy". United States. https://doi.org/10.1063/5.0081109. https://www.osti.gov/servlets/purl/1973504.
@article{osti_1973504,
title = {Piezoelectric property of PZT nanofibers characterized by resonant piezo-force microscopy},
author = {Zhang, Guitao and Chen, Xi and Xu, Weihe and Yao, Wei-Dong and Shi, Yong},
abstractNote = {Nano-piezoelectric materials have drawn tremendous research interest. However, characterization of their piezoelectric properties, especially measuring the piezoelectric strain coefficients, remains a challenge. Normally, researchers use an AFM-based method to directly measure nano-materials’ piezoelectric strain coefficients. But, the extremely small piezoelectric deformation, the influence from the parasitic electrostatic force, and the environmental noise make the measurement results questionable. In this paper, a resonant piezo-force microscopy method was used to accurately measure the piezoelectric deformation from 1D piezoelectric nanofibers. During the experiment, the AFM tip was brought into contact with the piezoelectric sample and set to work at close to its first resonant frequency. A lock-in amplifier was used to pick up the sample’s deformation signal at the testing frequency. By using this technique, the piezoelectric strain constant d 33 of the Lead Zirconate Titanate (PZT) nanofiber with a diameter of 76 nm was measured. The result showed that d 33 of this PZT nanofiber was around 387 pm/V. Meanwhile, by tracking the piezoelectric deformation phase image, domain structures inside PZT nanofibers were identified.},
doi = {10.1063/5.0081109},
journal = {AIP Advances},
number = 3,
volume = 12,
place = {United States},
year = {Tue Mar 01 00:00:00 EST 2022},
month = {Tue Mar 01 00:00:00 EST 2022}
}
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