Powder Metallurgy HIP Process Study and Mechanical Property Evaluations for IN740H

Journal Article · 28 June 2022 · JOM. Journal of the Minerals, Metals & Materials Society

DOI: https://doi.org/10.1007/s11837-022-05385-y · OSTI ID:1915241

Huang, Shenyan  ^[1]; Hanlon, Timothy ^[2]; Shingledecker, John  ^[3]; Spinelli, Ian ^[2]; Drobnjak, Marija ^[2]; Shoemaker, Kevin ^[2]; Crawford, Cole ^[2]

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1. GE Research, Niskayuna, NY (United States); GE Research
2. GE Research, Niskayuna, NY (United States)
3. Electric Power Research Inst., Charlotte, NC (United States)

The effects of hot isostatic pressing (HIP) parameters and powder size distribution (PSD) on the resulting microstructure and properties of powder metallurgy (P/M) IN740H have been investigated. Properties can be substantially tailored through the appropriate management of these parameters. Applying a thermal presoak to the input powder prior to the sintering stage of HIP can significantly increase average grain size and coarse grain fraction, enabling a trade for improved creep resistance at the expense of tensile strength. Here, powder thermal presoak was found to have a larger impact on microstructure and properties than the use of a coarser PSD alone. Additionally, substantial grain growth and grain boundary migration is observed in P/M IN740H at HIP temperatures above 1260°C. Given its inherently finer grain size, P/M HIP IN740H typically outperforms its cast and wrought counterparts in tensile response. Creep life at 700–800°C was inferior to wrought due to PPBs coincident with grain boundaries which served as cavity nucleation sites, leading to lower creep ductility. The ability to adjust the microstructure toward a more balanced creep and tensile behavior allows P/M HIP IN740H to be considered for high-temperature applications in advanced ultra-supercritical steam and supercritical carbon dioxide power cycles.

• Research Organization: GE Research, Niskayuna, NY (United States)
• Sponsoring Organization: USDOE Office of Fossil Energy (FE)
• Grant/Contract Number: FE0031818
• OSTI ID: 1915241
• Journal Information: JOM. Journal of the Minerals, Metals & Materials Society, Journal Name: JOM. Journal of the Minerals, Metals & Materials Society Journal Issue: 9 Vol. 74; ISSN 1047-4838
• Publisher: SpringerCopyright Statement
• Country of Publication: United States
• Language: English