DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Characterization of the Formability of High-Purity Polycrystalline Niobium Sheets for Superconducting Radiofrequency Applications

Journal Article · · Journal of Engineering Materials and Technology
DOI: https://doi.org/10.1115/1.4052557 · OSTI ID:1893870
 [1];  [2];  [3];  [4];  [5];  [3];  [2]
  1. I-Cube Research/Bmax (France); ENSTA Bretagne (France); Centre National de la Recherche Scientifique-Mixed Organizations (CNRS-UMR), Paris (France); Research Institute Dupuy De Lôme (IRDL) (France)
  2. Universite de Lorraine, Champenoux (France); Centre National de la Recherche Scientifique-Mixed Organizations (CNRS-UMR), Paris (France); Arts et Métiers ParisTech (France)
  3. I-Cube Research/Bmax (France)
  4. European Organization for Nuclear Research (CERN), Geneva (Switzerland)
  5. ENSTA Bretagne (France); Centre National de la Recherche Scientifique-Mixed Organizations (CNRS-UMR), Paris (France); Research Institute Dupuy De Lôme (IRDL) (France)

The forming limit diagram (FLD) of high-purity niobium sheets used for the manufacturing of superconducting radiofrequency (SRF) cavities is presented. The Marciniak (in-plane) test was used with niobium blanks with a thickness of 1 mm and blank carriers of annealed oxygen-free electronic (OFE) copper. A high formability was measured, with an approximate true major strain at necking for plane strain of 0.44. The high formability of high-purity niobium is likely caused by its high strain rate sensitivity of 0.112. Plastic strain anisotropies (r-values) of 1.66, 1.00, and 2.30 were measured in the 0 deg, 45 deg, and 90 deg directions. However, stress–strain curves at a nominal strain rate of ~10–3 s–1 showed similar mechanical properties in the three directions. Theoretical calculations of the forming limit curves (FLCs) were conducted using an analytical two-zone model. The obtained results indicate that the anisotropy and strain rate sensitivity of niobium affect its formability. The model was used to investigate the influence of strain rate on strains at necking. The obtained results suggest that the use of high-speed sheet forming should further increase the formability of niobium.

Research Organization:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE Office of Science (SC); European Union (EU)
Grant/Contract Number:
AC02-05CH11231
OSTI ID:
1893870
Journal Information:
Journal of Engineering Materials and Technology, Journal Name: Journal of Engineering Materials and Technology Journal Issue: 2 Vol. 144; ISSN 0094-4289
Publisher:
ASMECopyright Statement
Country of Publication:
United States
Language:
English

References (20)

Effect of changing strain paths on journal November 1993
Increased ductility in high velocity electromagnetic ring expansion journal July 1996
A simple technique to generate in-plane forming limit curves and selected applications journal August 1995
High-velocity metal forming—An old technology addresses new problems journal July 1995
Effect of Strain Rate on the Tensile Mechanical Properties of Electron Beam Welded OFE Copper and High-Purity Niobium for SRF Applications journal February 2021
Limit strains in the processes of stretch-forming sheet metal journal September 1967
Influence of the plastic properties of a material on the forming limit diagram for sheet metal in tension journal October 1973
Prediction of the forming limit diagrams of anisotropic sheets in linear and non-linear loading journal January 1985
Enhanced formability of interstitial free iron at high strain rates journal December 1992
Flow stress of commercially pure niobium over a broad range of temperatures and strain rates journal May 2000
Direct measurement of isothermal flow stress of metals at elevated temperatures and high strain rates with application to Ta and TaW alloys journal March 1997
An analytical model for necking strains in stretched plates under dynamic biaxial loading journal September 2020
Material aspects of dynamic neck retardation journal January 2008
Experimental analysis and modelling of the strain-rate sensitivity of sheet niobium journal January 2018
Dislocation‐mechanics‐based constitutive relations for material dynamics calculations journal March 1987
The Influence of Strain Hardening and Strain-Rate Sensitivity on Sheet Metal Forming journal July 1977
FCC-ee: The Lepton Collider: Future Circular Collider Conceptual Design Report Volume 2 journal June 2019
FCC-hh: The Hadron Collider: Future Circular Collider Conceptual Design Report Volume 3 journal July 2019
Theoretical analysis of strain- and stress-based forming limit diagrams journal March 2013
Uniaxial near plane strain tensile tests applied to the determination of the FLC0 formabillity parameter journal June 2014