Overview of HPCAT and capabilities for studying minerals and various other materials at high-pressure conditions

Bommannavar, Arunkumar; Chow, Paul; Ferry, Rich; Hrubiak, Rostislav; Humble, Freda; Kenney-Benson, Curtis; Lv, Mingda; Meng, Yue; Park, Changyong; Popov, Dmitry; Rod, Eric; Somayazulu, Maddury; Shen, Guoyin; Smith, Dean; Smith, Jesse; Xiao, Yuming; Velisavljevic, Nenad

doi:10.1007/s00269-022-01209-2

Title: Overview of HPCAT and capabilities for studying minerals and various other materials at high-pressure conditions

Journal Article · 14 August 2022 · Physics and Chemistry of Minerals

DOI: https://doi.org/10.1007/s00269-022-01209-2 · OSTI ID:1881554

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Abstract High-Pressure Collaborative Access Team (HPCAT) is a synchrotron-based facility located at the Advanced Photon Source (APS). With four online experimental stations and various offline capabilities, HPCAT is focused on providing synchrotron x-ray capabilities for high pressure and temperature research and supporting a broad user community. Overall, the array of online/offline capabilities is described, including some of the recent developments for remote user support and the concomitant impact of the current pandemic. General overview of work done at HPCAT and with a focus on some of the minerals relevant work and supporting capabilities is also discussed. With the impending APS-Upgrade (APS-U), there is a considerable effort within HPCAT to improve and add capabilities. These are summarized briefly for each of the end-stations.

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Research Organization:: Argonne National Laboratory (ANL), Lemont, IL (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-06CH11357; AC52-07NA27344

OSTI ID:: 1881554

Report Number(s):: LLNL-JRNL-842503; 36; PII: 1209

Journal Information:: Physics and Chemistry of Minerals, Journal Name: Physics and Chemistry of Minerals Journal Issue: 9 Vol. 49; ISSN 0342-1791

Publisher:: Springer Science + Business MediaCopyright Statement

Country of Publication:: Germany

Language:: English

References (57)

Synthesis and Stability of Lanthanum Superhydrides Geballe, Zachary M.; Liu, Hanyu; Mishra, Ajay K. Angewandte Chemie International Edition, Vol. 57, Issue 3 https://doi.org/10.1002/anie.201709970	journal	December 2017
New Laue Micro-diffraction Setup for Real-Time In Situ Microstructural Characterization of Materials Under External Stress Popov, D.; Sinogeikin, S.; Park, C. The Minerals, Metals & Materials Series https://doi.org/10.1007/978-3-030-06143-2_5	book	January 2019
Heat-treated glassy carbon under pressure exhibiting superior hardness, strength and elasticity Hu, Meng; Zhang, Shuangshuang; Liu, Bing Journal of Materiomics, Vol. 7, Issue 1 https://doi.org/10.1016/j.jmat.2020.06.007	journal	January 2021
Toward comprehensive studies of liquids at high pressures and high temperatures: Combined structure, elastic wave velocity, and viscosity measurements in the Paris–Edinburgh cell Kono, Yoshio; Park, Changyong; Kenney-Benson, Curtis Physics of the Earth and Planetary Interiors, Vol. 228 https://doi.org/10.1016/j.pepi.2013.09.006	journal	March 2014
Progress of in situ synchrotron X-ray diffraction studies on the mechanical behavior of materials at small scales Cornelius, Thomas W.; Thomas, Olivier Progress in Materials Science, Vol. 94 https://doi.org/10.1016/j.pmatsci.2018.01.004	journal	May 2018
Elastic properties of polyethylene from high pressure sound speed measurements Jordan, Jennifer L.; Rowland, Rick L.; Greenhall, John Polymer, Vol. 212 https://doi.org/10.1016/j.polymer.2020.123164	journal	January 2021
Structural Changes in Liquid Lithium under High Pressure Shu, Yu; Kono, Yoshio; Ohira, Itaru The Journal of Physical Chemistry B, Vol. 124, Issue 33 https://doi.org/10.1021/acs.jpcb.0c05324	journal	July 2020
Pressure-Induced Enhancement of Thermoelectric Figure of Merit and Structural Phase Transition in TiNiSn Baker, Jason L.; Park, Changyong; Kenney-Benson, Curtis The Journal of Physical Chemistry Letters, Vol. 12, Issue 3 https://doi.org/10.1021/acs.jpclett.0c03609	journal	January 2021
Observation of 9-Fold Coordinated Amorphous TiO ₂ at High Pressure Shu, Yu; Kono, Yoshio; Ohira, Itaru The Journal of Physical Chemistry Letters, Vol. 11, Issue 2 https://doi.org/10.1021/acs.jpclett.9b03378	journal	December 2019
Probing High-Pressure Structural Evolution in Polyurea with In Situ Energy-Dispersive X-ray Diffraction and Molecular Dynamics Simulations Eastmond, Tyler; Hu, Jing; Alizadeh, Vahidreza Macromolecules, Vol. 54, Issue 2 https://doi.org/10.1021/acs.macromol.0c02266	journal	January 2021
Pressure Induced Assembly and Coalescence of Lead Chalcogenide Nanocrystals Meng, Lingyao; Duwal, Sakun; Lane, J. Matthew D. Journal of the American Chemical Society, Vol. 143, Issue 7 https://doi.org/10.1021/jacs.0c13350	journal	February 2021
Experimental Investigation of Mercury's Magma Ocean Viscosity: Implications for the Formation of Mercury's Cumulate Mantle, Its Subsequent Dynamic Evolution, and Crustal Petrogenesis Mouser, Megan D.; Dygert, Nicholas; Anzures, Brendan A. Journal of Geophysical Research: Planets, Vol. 126, Issue 11 https://doi.org/10.1029/2021JE006946	journal	November 2021
Microstructures define melting of molybdenum at high pressures Hrubiak, Rostislav; Meng, Yue; Shen, Guoyin Nature Communications, Vol. 8, Issue 1 https://doi.org/10.1038/ncomms14562	journal	March 2017
Pressing on: The legacy of Percy W. Bridgman McMillan, Paul F. Nature Materials, Vol. 4, Issue 10 https://doi.org/10.1038/nmat1488	journal	October 2005
Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar Jenei, Zs.; O’Bannon, E. F.; Weir, S. T. Nature Communications, Vol. 9, Issue 1 https://doi.org/10.1038/s41467-018-06071-x	journal	September 2018
Ultrahigh-pressure isostructural electronic transitions in hydrogen Ji, Cheng; Li, Bing; Liu, Wenjun Nature, Vol. 573, Issue 7775 https://doi.org/10.1038/s41586-019-1565-9	journal	September 2019
Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions Moore, Samuel L.; Samudrala, Gopi K.; Catledge, Shane A. Scientific Reports, Vol. 8, Issue 1 https://doi.org/10.1038/s41598-018-19915-9	journal	January 2018
Diamond and methane formation from the chemical decomposition of polyethylene at high pressures and temperatures Watkins, E. B.; Huber, R. C.; Childs, C. M. Scientific Reports, Vol. 12, Issue 1 https://doi.org/10.1038/s41598-021-04206-7	journal	January 2022
Dynamic diamond anvil cell (dDAC): A novel device for studying the dynamic-pressure properties of materials Evans, William J.; Yoo, Choong-Shik; Lee, Geun Woo Review of Scientific Instruments, Vol. 78, Issue 7 https://doi.org/10.1063/1.2751409	journal	July 2007
Real-time, high-resolution x-ray diffraction measurements on shocked crystals at a synchrotron facility Gupta, Y. M.; Turneaure, Stefan J.; Perkins, K. Review of Scientific Instruments, Vol. 83, Issue 12 https://doi.org/10.1063/1.4772577	journal	December 2012
Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression Smith, Jesse S.; Sinogeikin, Stanislav V.; Lin, Chuanlong Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926887	journal	July 2015
The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team Hrubiak, Rostislav; Sinogeikin, Stanislav; Rod, Eric Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926889	journal	July 2015
Focusing polycapillary to reduce parasitic scattering for inelastic x-ray measurements at high pressure Chow, P.; Xiao, Y. M.; Rod, E. Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926890	journal	July 2015
Online remote control systems for static and dynamic compression and decompression using diamond anvil cells Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926892	journal	July 2015
New developments in micro-X-ray diffraction and X-ray absorption spectroscopy for high-pressure research at 16-BM-D at the Advanced Photon Source Park, Changyong; Popov, Dmitry; Ikuta, Daijo Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926893	journal	July 2015
High pressure Laue diffraction and its application to study microstructural changes during the α → β phase transition in Si Popov, D.; Park, C.; Kenney-Benson, C. Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926894	journal	July 2015
New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team Meng, Yue; Hrubiak, Rostislav; Rod, Eric Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926895	journal	July 2015
X-ray imaging for studying behavior of liquids at high pressures and high temperatures using Paris-Edinburgh press Kono, Yoshio; Kenney-Benson, Curtis; Shibazaki, Yuki Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4927227	journal	July 2015
Containment system for experiments on radioactive and other hazardous materials in a Paris-Edinburgh press Jacobsen, M. K.; Velisavljevic, N. Review of Scientific Instruments, Vol. 86, Issue 11 https://doi.org/10.1063/1.4935830	journal	November 2015
A CO ₂ laser heating system for in situ high pressure-temperature experiments at HPCAT Smith, Dean; Smith, Jesse S.; Childs, Christian Review of Scientific Instruments, Vol. 89, Issue 8 https://doi.org/10.1063/1.5040508	journal	August 2018
A broadband wavelet implementation for rapid ultrasound pulse-echo time-of-flight measurements Sturtevant, Blake T.; Velisavljevic, Nenad; Sinha, Dipen N. Review of Scientific Instruments, Vol. 91, Issue 7 https://doi.org/10.1063/5.0010475	journal	July 2020
High-pressure high-temperature synthesis and thermal equation of state of high-entropy transition metal boride Iwan, Seth; Burrage, Kaleb C.; Storr, Bria C. AIP Advances, Vol. 11, Issue 3 https://doi.org/10.1063/5.0045592	journal	March 2021
Shear strength measurements and hydrostatic compression of rhenium diboride under high pressures Burrage, Kaleb C.; Park, Changyong; Vohra, Yogesh K. Journal of Applied Physics, Vol. 129, Issue 20 https://doi.org/10.1063/5.0050057	journal	May 2021
Ultrahigh-pressure polyamorphism in GeO ₂ glass with coordination number >6 Kono, Yoshio; Kenney-Benson, Curtis; Ikuta, Daijo Proceedings of the National Academy of Sciences, Vol. 113, Issue 13 https://doi.org/10.1073/pnas.1524304113	journal	March 2016
A new type of compact large-capacity press for neutron and x-ray scattering Klotz, S.; Hamel, G.; Frelat, J. High Pressure Research, Vol. 24, Issue 1 https://doi.org/10.1080/08957950410001661963	journal	January 2004
Diamond anvil cell, 50th birthday Bassett, William A. High Pressure Research, Vol. 29, Issue 2 https://doi.org/10.1080/08957950802597239	journal	May 2009
High pressure X-ray emission spectroscopy at the advanced photon source Xiao, Yuming; Chow, Paul; Shen, Guoyin High Pressure Research, Vol. 36, Issue 3 https://doi.org/10.1080/08957959.2016.1209498	journal	July 2016
Opposed type double stage cell for Mbar pressure experiment with large sample volume Kono, Yoshio; Kenney-Benson, Curtis; Shen, Guoyin High Pressure Research, Vol. 40, Issue 1 https://doi.org/10.1080/08957959.2019.1710744	journal	January 2020
Evidence for superionic H₂O and diffusive He–H₂O at high temperature and high pressure Kim, Minseob; Oka, Kenta; Ahmed, Sohan Journal of Physics: Condensed Matter, Vol. 34, Issue 39 https://doi.org/10.1088/1361-648X/ac8134	journal	July 2022
High-pressure studies with x-rays using diamond anvil cells Shen, Guoyin; Mao, Ho Kwang Reports on Progress in Physics, Vol. 80, Issue 1 https://doi.org/10.1088/1361-6633/80/1/016101	journal	November 2016
High Pressure Melting of Lithium Schaeffer, Anne Marie J.; Talmadge, William B.; Temple, Scott R. Physical Review Letters, Vol. 109, Issue 18 https://doi.org/10.1103/PhysRevLett.109.185702	journal	November 2012
Venture into Water’s No Man’s Land: Structural Transformations of Solid H 2 O under Rapid Compression and Decompression Lin, Chuanlong; Smith, Jesse S.; Liu, Xuqiang Physical Review Letters, Vol. 121, Issue 22 https://doi.org/10.1103/PhysRevLett.121.225703	journal	November 2018
Evidence for Superconductivity above 260 K in Lanthanum Superhydride at Megabar Pressures Somayazulu, Maddury; Ahart, Muhtar; Mishra, Ajay K. Physical Review Letters, Vol. 122, Issue 2 https://doi.org/10.1103/PhysRevLett.122.027001	journal	January 2019
High-Pressure Melt Curve and Phase Diagram of Lithium Frost, Mungo; Kim, Jongjin B.; McBride, Emma E. Physical Review Letters, Vol. 123, Issue 6 https://doi.org/10.1103/PhysRevLett.123.065701	journal	August 2019
Oxygen Quadclusters in SiO 2 Glass above Megabar Pressures up to 160 GPa Revealed by X-Ray Raman Scattering Lee, Sung Keun; Kim, Yong-Hyun; Yi, Yoo Soo Physical Review Letters, Vol. 123, Issue 23 https://doi.org/10.1103/PhysRevLett.123.235701	journal	December 2019
Pressure-Induced Collapse of Magnetic Order in Jarosite Klein, Ryan A.; Walsh, James P. S.; Clarke, Samantha M. Physical Review Letters, Vol. 125, Issue 7 https://doi.org/10.1103/PhysRevLett.125.077202	journal	August 2020
Structural Evolution of SiO 2 Glass with Si Coordination Number Greater than 6 Kono, Yoshio; Shu, Yu; Kenney-Benson, Curtis Physical Review Letters, Vol. 125, Issue 20 https://doi.org/10.1103/PhysRevLett.125.205701	journal	November 2020
Nature of polyamorphic transformations in H 2 O under isothermal compression and decompression Shen, Guoyin; Smith, Jesse S.; Kenney-Benson, Curtis Physical Review Materials, Vol. 3, Issue 7 https://doi.org/10.1103/PhysRevMaterials.3.073404	journal	July 2019
Design and performance of an ultra-high-vacuum-compatible artificial channel-cut monochromator Narayanan, Suresh; Sandy, Alec; Shu, Deming Journal of Synchrotron Radiation, Vol. 15, Issue 1 https://doi.org/10.1107/S090904950705340X	journal	December 2007
APS deposition facility upgrades and future plans Conley, Ray; Shi, Bing; Erdmann, Mark SPIE Proceedings https://doi.org/10.1117/12.2062427	conference	September 2014
Carbon-boron clathrates as a new class of sp ³ -bonded framework materials Zhu, Li; Borstad, Gustav M.; Liu, Hanyu Science Advances, Vol. 6, Issue 2 https://doi.org/10.1126/sciadv.aay8361	journal	January 2020
Sound wave velocities of Fe5Si at high-pressure and high-temperature conditions: Implications to lunar and planetary cores Deng, Liwei; Kono, Yoshio; Shen, Guoyin American Mineralogist, Vol. 104, Issue 2 https://doi.org/10.2138/am-2019-6564	journal	February 2019
Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction Popov, Dmitry; Velisavljevic, Nenad; Somayazulu, Maddury Crystals, Vol. 9, Issue 12 https://doi.org/10.3390/cryst9120672	journal	December 2019
The Viscosity and Atomic Structure of Volatile-Bearing Melilititic Melts at High Pressure and Temperature and the Transport of Deep Carbon Stagno, Vincenzo; Stopponi, Veronica; Kono, Yoshio Minerals, Vol. 10, Issue 3 https://doi.org/10.3390/min10030267	journal	March 2020
X-Ray Diffraction under Extreme Conditions at the Advanced Light Source Stan, Camelia; Beavers, Christine; Kunz, Martin Quantum Beam Science, Vol. 2, Issue 1 https://doi.org/10.3390/qubs2010004	journal	January 2018
Viscosity Measurement of Liquids at High Pressures Using Ultrafast X-Ray Imaging Kono, Yoshio The Review of High Pressure Science and Technology, Vol. 29, Issue 2 https://doi.org/10.4131/jshpreview.29.86	journal	January 2019
Ultrahigh pressure structural changes in a 60 mol. % Al2O3–40 mol. % SiO2 glass Ohira, I.; Kono, Y.; Shibazaki, Y. Geochemical Perspectives Letters https://doi.org/10.7185/geochemlet.1913	journal	May 2019

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Title: Overview of HPCAT and capabilities for studying minerals and various other materials at high-pressure conditions

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