A method to predict texture effect on ion beam channeling analysis of polycrystals and the application to study the mosaic spreading effect in highly oriented pyrolytic graphite
Abstract
We propose a method to convert the channeling Rutherford backscattering spectrum yield map of a single crystal to a polycrystal through a matrix rotation technique. The rotation matrix is determined by the deviation of the crystal axial direction from the original z axis. The final yield map is created after averaging the rotated yields using the texture function as the weight factor. For highly oriented pyrolytic graphite (HOPG) exhibiting mosaic spread, the method leads to a Gaussian kernel averaging of the map obtained from a single crystal. The yield map of a single crystal is obtained by a simulation of ion trajectories in a potential field described by Moliere screened Coulomb potentials. Yield maps are calculated under various σ values (standard deviations of mosaic spread). The simulated results are compared with experimental results obtained using 1.2 MeV alpha particle. σ is extracted through the best fitting, demonstrating that the method can be used to obtain texture details. The effects of mosaic spread on minimum yield χmin and the half-width at half maximum of angular scans ψ½ are systematically modeled and compared with previous theoretical equations. The study also shows that previous theoretical equations are valid only at small σ values.more »
- Authors:
-
- Texas A & M Univ., College Station, TX (United States)
- Univ. of Houston, TX (United States)
- Publication Date:
- Research Org.:
- Texas A & M Univ., College Station, TX (United States). Texas A & M Engineering Experiment Station
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1979070
- Alternate Identifier(s):
- OSTI ID: 1872148
- Grant/Contract Number:
- SC0006725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Applied Physics
- Additional Journal Information:
- Journal Volume: 131; Journal Issue: 22; Journal ID: ISSN 0021-8979
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 73 NUCLEAR PHYSICS AND RADIATION PHYSICS; Physics
Citation Formats
Li, Yongchang, Chauhan, Rijul, Chen, Di, Hu, Zhihan, Wang, X. M., and Shao, Lin. A method to predict texture effect on ion beam channeling analysis of polycrystals and the application to study the mosaic spreading effect in highly oriented pyrolytic graphite. United States: N. p., 2022.
Web. doi:10.1063/5.0088622.
Li, Yongchang, Chauhan, Rijul, Chen, Di, Hu, Zhihan, Wang, X. M., & Shao, Lin. A method to predict texture effect on ion beam channeling analysis of polycrystals and the application to study the mosaic spreading effect in highly oriented pyrolytic graphite. United States. https://doi.org/10.1063/5.0088622
Li, Yongchang, Chauhan, Rijul, Chen, Di, Hu, Zhihan, Wang, X. M., and Shao, Lin. Tue .
"A method to predict texture effect on ion beam channeling analysis of polycrystals and the application to study the mosaic spreading effect in highly oriented pyrolytic graphite". United States. https://doi.org/10.1063/5.0088622. https://www.osti.gov/servlets/purl/1979070.
@article{osti_1979070,
title = {A method to predict texture effect on ion beam channeling analysis of polycrystals and the application to study the mosaic spreading effect in highly oriented pyrolytic graphite},
author = {Li, Yongchang and Chauhan, Rijul and Chen, Di and Hu, Zhihan and Wang, X. M. and Shao, Lin},
abstractNote = {We propose a method to convert the channeling Rutherford backscattering spectrum yield map of a single crystal to a polycrystal through a matrix rotation technique. The rotation matrix is determined by the deviation of the crystal axial direction from the original z axis. The final yield map is created after averaging the rotated yields using the texture function as the weight factor. For highly oriented pyrolytic graphite (HOPG) exhibiting mosaic spread, the method leads to a Gaussian kernel averaging of the map obtained from a single crystal. The yield map of a single crystal is obtained by a simulation of ion trajectories in a potential field described by Moliere screened Coulomb potentials. Yield maps are calculated under various σ values (standard deviations of mosaic spread). The simulated results are compared with experimental results obtained using 1.2 MeV alpha particle. σ is extracted through the best fitting, demonstrating that the method can be used to obtain texture details. The effects of mosaic spread on minimum yield χmin and the half-width at half maximum of angular scans ψ½ are systematically modeled and compared with previous theoretical equations. The study also shows that previous theoretical equations are valid only at small σ values. The proposed method can be applied to any type of polycrystal and is not limited to HOPG. It provides near-surface mosaic spread and crystallography information with a longitudinal depth resolution of tens of nanometers and is not influenced by grain shapes.},
doi = {10.1063/5.0088622},
journal = {Journal of Applied Physics},
number = 22,
volume = 131,
place = {United States},
year = {Tue Jun 14 00:00:00 EDT 2022},
month = {Tue Jun 14 00:00:00 EDT 2022}
}
Works referenced in this record:
Irradiation effects in carbon nanostructures
journal, July 1999
- Banhart, Florian
- Reports on Progress in Physics, Vol. 62, Issue 8
Channeling studies in graphite
journal, October 1984
- Elman, B. S.; Braunstein, G.; Dresselhaus, M. S.
- Journal of Applied Physics, Vol. 56, Issue 7
Separate estimate of crystalline orientations and scattering centers in polycrystals by backscattering technique
journal, April 1976
- Ishiwara, Hiroshi; Furukawa, Seijiro
- Journal of Applied Physics, Vol. 47, Issue 4
Observation and analysis of epitaxial growth of CoSi 2 on (100) Si
journal, March 1992
- Bulle‐Lieuwma, C. W. T.; van Ommen, A. H.; Hornstra, J.
- Journal of Applied Physics, Vol. 71, Issue 5
The role of flux-focusing in the origin of shoulders in ion channeling angular scans
journal, April 2012
- Wijesundera, Dharshana N.; Ma, Ki B.; Wang, Xuemei
- Physics Letters A, Vol. 376, Issue 22
Defect production in ceramics
journal, November 1997
- Zinkle, S. J.; Kinoshita, C.
- Journal of Nuclear Materials, Vol. 251
Experimental and modeling study on increasing accuracy of strain measurement by ion beam analysis in SiGe strained layer thin films
journal, August 2014
- Martin, Michael S.; Wijesundera, Dharshana; Thompson, Phillip E.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 332
SRIM – The stopping and range of ions in matter (2010)
journal, June 2010
- Ziegler, James F.; Ziegler, M. D.; Biersack, J. P.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 268, Issue 11-12
Effect of damage cascades on the irradiation-induced amorphization in graphite
journal, May 1997
- Abe, Hiroaki; Naramoto, Hiroshi; Iwase, Akihiro
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 127-128
Planar channeling in wurtzite structured ZnO (0001): Anisotropic effects due to the non-centrosymmetric structure
journal, June 2012
- Wijesundera, Dharshana N.; Chen, Quark; Ma, Ki Bui
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 281