Orientation-selected micro-pillar compression of additively manufactured 316L stainless steels: Comparison of as-manufactured, annealed, and proton-irradiated variants
Abstract
In this work, irradiation response and deformation mechanisms of additively manufactured (AM) 316L stainless steel were studied by atomic scale characterization and micro-pillar compression. The AM 316L stainless steels were fabricated by direct energy deposition, a laser-based additive manufacturing process. Irradiation with 2 MeV protons at 360°C was performed to create ~1.8 displacements-per-atom (dpa) damage in AM 316L. Deformation behaviors of the as-manufactured, annealed, and proton-irradiated variants were studied, focusing on the effects of manufacturing-induced pores, residual stress, and irradiation-introduced defects (dislocation loops and voids). Micro-pillars were prepared from grains of pre-selected orientation, avoiding contributions of grain boundaries and allowing determination of resolved shear stress on {111} glide planes. Transmission electron microscopy was used to characterize the pre- and post-deformation microstructure. It was found that in the as-manufactured alloy variant, moving dislocations were the major deformation carrier, with noticeable blocking by fabrication-induced pores, In the annealed variant, hardness was reduced, and deformation was also accomplished by dislocation gliding. In the proton-irradiated variant, significant twinning was observed. Comparing measured resolved shear stress and predicted critical stress for dislocation dissociation, we conclude that irradiation hardening became high enough to activate twinning. Therefore, the deformation mechanism changes from dislocation gliding to twinning. Themore »
- Authors:
-
- Texas A & M Univ., College Station, TX (United States); Boise State Univ., ID (United States); Center for Advanced Energy Studies, Idaho Falls, ID (United States)
- Idaho National Lab. (INL), Idaho Falls, ID (United States)
- Texas A & M Univ., College Station, TX (United States)
- Publication Date:
- Research Org.:
- Georgia Institute of Technology, Atlanta, GA (United States); Idaho National Laboratory (INL), Idaho Falls, ID (United States)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA); USDOE Laboratory Directed Research and Development (LDRD) Program; USDOE Office of Nuclear Energy (NE)
- OSTI Identifier:
- 1878579
- Alternate Identifier(s):
- OSTI ID: 1865626; OSTI ID: 1895151
- Grant/Contract Number:
- NA0003921; AC07-05ID14517
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Nuclear Materials
- Additional Journal Information:
- Journal Volume: 566; Journal ID: ISSN 0022-3115
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Irradiated metals; Irradiation effect; Deformation; Deformation twinning; Compression test
Citation Formats
Shiau, Ching-Heng, Sun, Cheng, McMurtrey, Michael, O'Brien, Robert, Garner, Frank A., and Shao, Lin. Orientation-selected micro-pillar compression of additively manufactured 316L stainless steels: Comparison of as-manufactured, annealed, and proton-irradiated variants. United States: N. p., 2022.
Web. doi:10.1016/j.jnucmat.2022.153739.
Shiau, Ching-Heng, Sun, Cheng, McMurtrey, Michael, O'Brien, Robert, Garner, Frank A., & Shao, Lin. Orientation-selected micro-pillar compression of additively manufactured 316L stainless steels: Comparison of as-manufactured, annealed, and proton-irradiated variants. United States. https://doi.org/10.1016/j.jnucmat.2022.153739
Shiau, Ching-Heng, Sun, Cheng, McMurtrey, Michael, O'Brien, Robert, Garner, Frank A., and Shao, Lin. Wed .
"Orientation-selected micro-pillar compression of additively manufactured 316L stainless steels: Comparison of as-manufactured, annealed, and proton-irradiated variants". United States. https://doi.org/10.1016/j.jnucmat.2022.153739. https://www.osti.gov/servlets/purl/1878579.
@article{osti_1878579,
title = {Orientation-selected micro-pillar compression of additively manufactured 316L stainless steels: Comparison of as-manufactured, annealed, and proton-irradiated variants},
author = {Shiau, Ching-Heng and Sun, Cheng and McMurtrey, Michael and O'Brien, Robert and Garner, Frank A. and Shao, Lin},
abstractNote = {In this work, irradiation response and deformation mechanisms of additively manufactured (AM) 316L stainless steel were studied by atomic scale characterization and micro-pillar compression. The AM 316L stainless steels were fabricated by direct energy deposition, a laser-based additive manufacturing process. Irradiation with 2 MeV protons at 360°C was performed to create ~1.8 displacements-per-atom (dpa) damage in AM 316L. Deformation behaviors of the as-manufactured, annealed, and proton-irradiated variants were studied, focusing on the effects of manufacturing-induced pores, residual stress, and irradiation-introduced defects (dislocation loops and voids). Micro-pillars were prepared from grains of pre-selected orientation, avoiding contributions of grain boundaries and allowing determination of resolved shear stress on {111} glide planes. Transmission electron microscopy was used to characterize the pre- and post-deformation microstructure. It was found that in the as-manufactured alloy variant, moving dislocations were the major deformation carrier, with noticeable blocking by fabrication-induced pores, In the annealed variant, hardness was reduced, and deformation was also accomplished by dislocation gliding. In the proton-irradiated variant, significant twinning was observed. Comparing measured resolved shear stress and predicted critical stress for dislocation dissociation, we conclude that irradiation hardening became high enough to activate twinning. Therefore, the deformation mechanism changes from dislocation gliding to twinning. The study is important for both processing optimization and performance evaluation of AM alloys for reactor applications.},
doi = {10.1016/j.jnucmat.2022.153739},
journal = {Journal of Nuclear Materials},
number = ,
volume = 566,
place = {United States},
year = {Wed Apr 20 00:00:00 EDT 2022},
month = {Wed Apr 20 00:00:00 EDT 2022}
}
Works referenced in this record:
Morphologies, microstructures, and mechanical properties of samples produced using laser metal deposition with 316 L stainless steel wire
journal, July 2017
- Xu, Xiang; Mi, Gaoyang; Luo, Yuanqing
- Optics and Lasers in Engineering, Vol. 94
Deformation behavior and irradiation tolerance of 316 L stainless steel fabricated by direct energy deposition
journal, June 2021
- Shiau, Ching-Heng; McMurtrey, Michael D.; O'Brien, Robert C.
- Materials & Design, Vol. 204
The microstructure, mechanical properties and corrosion resistance of 316L stainless steel fabricated using laser engineered net shaping
journal, November 2016
- Ziętala, Michał; Durejko, Tomasz; Polański, Marek
- Materials Science and Engineering: A, Vol. 677
Quantitative characterization of porosity in stainless steel LENS powders and deposits
journal, July 2006
- Susan, D. F.; Puskar, J. D.; Brooks, J. A.
- Materials Characterization, Vol. 57, Issue 1
Microstructure and mechanical properties of 316L austenitic stainless steel processed by different SLM devices
journal, May 2020
- Röttger, A.; Boes, J.; Theisen, W.
- The International Journal of Advanced Manufacturing Technology, Vol. 108, Issue 3
Investigation of the irradiation effects in additively manufactured 316L steel resulting in decreased irradiation assisted stress corrosion cracking susceptibility
journal, March 2021
- McMurtrey, M.; Sun, C.; Rupp, R. E.
- Journal of Nuclear Materials, Vol. 545
On the stress dependence of partial dislocation separation and deformation microstructure in austenitic stainless steels
journal, June 2003
- Byun, T. S.
- Acta Materialia, Vol. 51, Issue 11
Composition-dependence of stacking fault energy in austenitic stainless steels through linear regression with random intercepts
journal, August 2017
- Meric de Bellefon, G.; van Duysen, J. C.; Sridharan, K.
- Journal of Nuclear Materials, Vol. 492
The contribution of various defects to irradiation-induced hardening in an austenitic model alloy
journal, December 2000
- Ando, M.; Katoh, Y.; Tanigawa, H.
- Journal of Nuclear Materials, Vol. 283-287
Relationship between hardening and damage structure in austenitic stainless steel 316LN irradiated at low temperature in the HFIR
journal, June 1999
- Hashimoto, N.; Wakai, E.; Robertson, J. P.
- Journal of Nuclear Materials, Vol. 273, Issue 1
Competing mechanisms and modeling of deformation in austenitic stainless steel single crystals with and without nitrogen
journal, November 2001
- Karaman, I.; Sehitoglu, H.; Maier, H. J.
- Acta Materialia, Vol. 49, Issue 19
Post-irradiation deformation characteristics of heavy-ion irradiated 304L SS
journal, August 1995
- Cole, James I.; Bruemmer, Stephen M.
- Journal of Nuclear Materials, Vol. 225
Role of cavities on deformation-induced martensitic transformation pathways in a laser-welded, neutron irradiated austenitic stainless steel
journal, March 2020
- Mao, Keyou S.; Sun, Cheng; Shiau, Ching-Heng
- Scripta Materialia, Vol. 178
A comprehensive study on microstructure and tensile behaviour of a selectively laser melted stainless steel
journal, May 2018
- Qiu, Chunlei; Kindi, Mohammed Al; Aladawi, Aiman Salim
- Scientific Reports, Vol. 8, Issue 1
Evolution of Microstructure, Residual Stress, and Tensile Properties of Additively Manufactured Stainless Steel Under Heat Treatments
journal, November 2020
- Zhang, Xinchang; McMurtrey, Michael D.; Wang, Liang
- JOM, Vol. 72, Issue 12
Neutron irradiation effects in Fe and Fe-Cr at 300 °C
journal, June 2016
- Chen, Wei-Ying; Miao, Yinbin; Gan, Jian
- Acta Materialia, Vol. 111
Grain boundary engineering of new additive manufactured polycrystalline alloys
journal, October 2021
- Abdi, Frank; Eftekharian, Amirhossein; Huang, Dade
- Forces in Mechanics, Vol. 4
On the origin of deformation microstructures in austenitic stainless steel: Part II—Mechanisms
journal, September 2001
- Lee, E. H.; Yoo, M. H.; Byun, T. S.
- Acta Materialia, Vol. 49, Issue 16
Twinning induced plasticity in austenitic stainless steel 316L made by additive manufacturing
journal, September 2017
- Pham, M. S.; Dovgyy, B.; Hooper, P. A.
- Materials Science and Engineering: A, Vol. 704
Microstructure and Mechanical Properties of AISI 316L Produced by Directed Energy Deposition-Based Additive Manufacturing: A Review
journal, May 2020
- Saboori, Abdollah; Aversa, Alberta; Marchese, Giulio
- Applied Sciences, Vol. 10, Issue 9
Ion-irradiation-induced damage in Fe–Cr alloys characterized by nanoindentation
journal, October 2011
- Heintze, C.; Bergner, F.; Hernández-Mayoral, M.
- Journal of Nuclear Materials, Vol. 417, Issue 1-3
Hardened austenite steel with columnar sub-grain structure formed by laser melting
journal, February 2015
- Saeidi, K.; Gao, X.; Zhong, Y.
- Materials Science and Engineering: A, Vol. 625
On the use of SRIM for computing radiation damage exposure
journal, September 2013
- Stoller, R. E.; Toloczko, M. B.; Was, G. S.
- Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 310
Quantifying the resistance to dislocation glide in single phase FeCrAl alloy
journal, September 2020
- Xu, Shun; Xie, Dongyue; Liu, Guisen
- International Journal of Plasticity, Vol. 132
Application of a three-feature dispersed-barrier hardening model to neutron-irradiated Fe–Cr model alloys
journal, May 2014
- Bergner, F.; Pareige, C.; Hernández-Mayoral, M.
- Journal of Nuclear Materials, Vol. 448, Issue 1-3
Crystallographic Orientation Dependence of Mechanical Responses of FeCrAl Micropillars
journal, October 2020
- Xie, Dongyue; Wei, Binqiang; Wu, Wenqian
- Crystals, Vol. 10, Issue 10
In situ SEM-EBSD analysis of plastic deformation mechanisms in neutron-irradiated austenitic steel
journal, April 2019
- Gussev, M. N.; Leonard, K. J.
- Journal of Nuclear Materials, Vol. 517
Additive manufacturing of 316L stainless steel by electron beam melting for nuclear fusion applications
journal, April 2017
- Zhong, Yuan; Rännar, Lars-Erik; Liu, Leifeng
- Journal of Nuclear Materials, Vol. 486
Twinning and martensite in a 304 austenitic stainless steel
journal, August 2012
- Shen, Y. F.; Li, X. X.; Sun, X.
- Materials Science and Engineering: A, Vol. 552
Anisotropy and heterogeneity of microstructure and mechanical properties in metal additive manufacturing: A critical review
journal, February 2018
- Kok, Y.; Tan, X. P.; Wang, P.
- Materials & Design, Vol. 139
Strain hardening and plastic instability properties of austenitic stainless steels after proton and neutron irradiation
journal, October 2001
- Byun, T. S.; Farrell, K.; Lee, E. H.
- Journal of Nuclear Materials, Vol. 298, Issue 3
On the origin of deformation microstructures in austenitic stainless steel: part I—microstructures
journal, September 2001
- Lee, E. H.; Byun, T. S.; Hunn, J. D.
- Acta Materialia, Vol. 49, Issue 16