The In Situ Ion Irradiation Toolbox: Time-Resolved Structure and Property Measurements

Lang, E.; Dennett, C. A.; Madden, N.; Hattar, K.

doi:10.1007/s11837-021-04993-4

Title: The In Situ Ion Irradiation Toolbox: Time-Resolved Structure and Property Measurements

Journal Article · 23 November 2021 · JOM. Journal of the Minerals, Metals & Materials Society

DOI: https://doi.org/10.1007/s11837-021-04993-4 · OSTI ID:1832495

;

; Madden, N.; Hattar, K.

Abstract The dynamic interactions of ions with matter drive a host of complex evolution mechanisms, requiring monitoring on short spatial and temporal scales to gain a full picture of a material response. Understanding the evolution of materials under ion irradiation and displacement damage is vital for many fields, including semiconductor processing, nuclear reactors, and space systems. Despite materials in service having a dynamic response to radiation damage, typical characterization is performed post-irradiation, washing out all information from transient processes. Characterizing active processes in situ during irradiation allows the mechanisms at play during the dynamic ion-material interaction process to be deciphered. In this review, we examine the in situ characterization techniques utilized for examining material structure, composition, and property evolution under ion irradiation. Covering analyses of microstructure, surface composition, and material properties, this work offers a perspective on the recent advances in methods for in situ monitoring of materials under ion irradiation, including a future outlook examining the role of complementary and combined characterization techniques in understanding dynamic materials evolution.

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Research Organization:: Sandia National Laboratories (SNL-NM), Albuquerque, NM (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA), Office of Defense Nuclear Nonproliferation

Grant/Contract Number:: AC07-05ID14517; NA0003525

OSTI ID:: 1832495

Report Number(s):: SAND--2021-14441J; PII: 4993

Journal Information:: JOM. Journal of the Minerals, Metals & Materials Society, Journal Name: JOM. Journal of the Minerals, Metals & Materials Society Journal Issue: 1 Vol. 74; ISSN 1047-4838

Publisher:: Springer Science + Business MediaCopyright Statement

Country of Publication:: United States

Language:: English

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An experiment on the dynamics of ion implantation and sputtering of surfaces Wright, G. M.; Barnard, H. A.; Kesler, L. A. Review of Scientific Instruments, Vol. 85, Issue 2 https://doi.org/10.1063/1.4861917	journal	February 2014
Open volume defects and magnetic phase transition in Fe ₆₀ Al ₄₀ transition metal aluminide Liedke, M. O.; Anwand, W.; Bali, R. Journal of Applied Physics, Vol. 117, Issue 16 https://doi.org/10.1063/1.4919014	journal	April 2015
In-situ evolution of helium bubbles in SiC under irradiation Beaufort, M. -F.; Vallet, M.; Nicolaï, J. Journal of Applied Physics, Vol. 118, Issue 20 https://doi.org/10.1063/1.4936562	journal	November 2015
Unraveling wall conditioning effects on plasma facing components in NSTX-U with the Materials Analysis Particle Probe (MAPP) Bedoya, F.; Allain, J. P.; Kaita, R. Review of Scientific Instruments, Vol. 87, Issue 11 https://doi.org/10.1063/1.4955276	journal	July 2016
Positron annihilation lifetime and Doppler broadening spectroscopy at the ELBE facility Wagner, Andreas; Butterling, Maik; Liedke, Maciej O. INTERNATIONAL WORKSHOP ON PHYSICS WITH POSITRONS AT JEFFERSON LAB, AIP Conference Proceedings https://doi.org/10.1063/1.5040215	conference	January 2018
Ionoluminescence to study irradiation stability of zirconia Srivastava, S. K.; Magudapathy, P.; Chinnathambi, S. DAE SOLID STATE PHYSICS SYMPOSIUM 2019, AIP Conference Proceedings https://doi.org/10.1063/5.0017650	conference	January 2020
Development of the materials analysis and particle probe for Proto-MPEX Beers, C. J.; Jaramillo, C.; Reid, N. C. Review of Scientific Instruments, Vol. 92, Issue 4 https://doi.org/10.1063/5.0043111	journal	April 2021
In situ investigation of 75 MeV boron and 100 MeV oxygen ion irradiation effects on 50 GHz silicon–germanium heterojunction bipolar transistors Praveen, K. C.; Pushpa, N.; Naik, P. S. Radiation Effects and Defects in Solids, Vol. 168, Issue 7-8 https://doi.org/10.1080/10420150.2013.787073	journal	August 2013
Study of defect evolution by TEM with in situ ion irradiation and coordinated modeling Li, Meimei; Kirk, M. A.; Baldo, P. M. Philosophical Magazine, Vol. 92, Issue 16 https://doi.org/10.1080/14786435.2012.662601	journal	June 2012
Superior tolerance of Ag/Ni multilayers against Kr ion irradiation: an in situ study Yu, K. Y.; Sun, C.; Chen, Y. Philosophical Magazine, Vol. 93, Issue 26 https://doi.org/10.1080/14786435.2013.815378	journal	July 2013
Field ion microscope examination of heavy ion radiation damage in iridium: I. experimental technique Hudson, J. A.; Nelson, R. S.; Ralph, B. Philosophical Magazine, Vol. 18, Issue 154 https://doi.org/10.1080/14786436808227504	journal	October 1968
Cavity Formation in Molybdenum Studied In Situ in TEM Bufford, D. C.; Snow, C. S.; Hattar, K. Fusion Science and Technology, Vol. 71, Issue 3 https://doi.org/10.1080/15361055.2016.1273700	journal	February 2017
Cavity Evolution at Grain Boundaries as a Function of Radiation Damage and Thermal Conditions in Nanocrystalline Nickel Muntifering, Brittany; Blair, Sarah Jane; Gong, Cajer Materials Research Letters, Vol. 4, Issue 2 https://doi.org/10.1080/21663831.2015.1121165	journal	December 2015
In situ spectroscopic ellipsometry as a versatile tool for studying atomic layer deposition Langereis, E.; Heil, S. B. S.; Knoops, H. C. M. Journal of Physics D: Applied Physics, Vol. 42, Issue 7 https://doi.org/10.1088/0022-3727/42/7/073001	journal	March 2009
In situ x-ray reflectivity study of swift heavy ion induced interface modification in a W/Si multilayer x-ray mirror Potdar, Satish; Gupta, Ranjeeta; Gupta, Ajay Journal of Physics D: Applied Physics, Vol. 48, Issue 1 https://doi.org/10.1088/0022-3727/48/1/015305	journal	December 2014
Helium induced nanoscopic morphology on tungsten under fusion relevant plasma conditions Baldwin, M. J.; Doerner, R. P. Nuclear Fusion, Vol. 48, Issue 3 https://doi.org/10.1088/0029-5515/48/3/035001	journal	January 2008
Effects of helium irradiation on degradation of optical properties of single and polycrystalline Mo mirrors for plasma diagnostics Ono, K.; Miyamoto, M.; Nakano, T. Physica Scripta, Vol. T138 https://doi.org/10.1088/0031-8949/2009/T138/014065	journal	December 2009
Unraveling atomic-level self-organization at the plasma-material interface Allain, J. P.; Shetty, A. Journal of Physics D: Applied Physics, Vol. 50, Issue 28 https://doi.org/10.1088/1361-6463/aa7506	journal	June 2017
Low energy Ar ⁺ ion irradiation induced surface modification in cadmium zinc telluride (CdZnTe) Tripathi, J. K.; Harilal, S. S.; Hassanein, A. Materials Research Express, Vol. 1, Issue 3 https://doi.org/10.1088/2053-1591/1/3/035904	journal	September 2014
Resistivity changes and defect mobility in ion-irradiated YBa 2 Cu 3 O 7 − x Marwick, A. D.; Clark, G. J.; Yee, D. S. Physical Review B, Vol. 39, Issue 13 https://doi.org/10.1103/PhysRevB.39.9061	journal	May 1989
In situ electrical resistivity of thin-film β-NiAl under Ar irradiation at 77 K Borges da Costa, J. A. T.; Vasconcellos, M. A. Z.; Teixeira, S. R. Physical Review B, Vol. 45, Issue 17 https://doi.org/10.1103/PhysRevB.45.9626	journal	May 1992
Phonon scattering effects from point and extended defects on thermal conductivity studied via ion irradiation of crystals with self-impurities Scott, Ethan A.; Hattar, Khalid; Rost, Christina M. Physical Review Materials, Vol. 2, Issue 9 https://doi.org/10.1103/PhysRevMaterials.2.095001	journal	September 2018
Formation of Ordered Nanoscale Semiconductor Dots by Ion Sputtering Facsko, S. Science, Vol. 285, Issue 5433 https://doi.org/10.1126/science.285.5433.1551	journal	September 1999
Studying Radiation Damage in Structural Materials by Using Ion Accelerators Hosemann, Peter Reviews of Accelerator Science and Technology, Vol. 04, Issue 01 https://doi.org/10.1142/S1793626811000513	journal	January 2011
Phase Transitions in Ge-Sb-Te Alloys Induced by Ion Irradiations Privitera, Stefania; Mio, Antonio M.; Benke, Julia MRS Advances, Vol. 1, Issue 39 https://doi.org/10.1557/adv.2016.280	journal	April 2016
Transmission electron microscopy with in situ ion irradiation Hinks, Jonathan Andrew Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2014.384	journal	February 2015
Oxidation of Zircaloy-4 during in situ proton irradiation and corrosion in PWR primary water Wang, Peng; Was, Gary S. Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2014.408	journal	March 2015
Ion irradiation and radiation effect characterization at the JANNUS-Saclay triple beam facility Beck, Lucile; Serruys, Yves; Miro, Sandrine Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2014.414	journal	February 2015
Transient grating spectroscopy: An ultrarapid, nondestructive materials evaluation technique Hofmann, Felix; Short, Michael P.; Dennett, Cody A. MRS Bulletin, Vol. 44, Issue 5 https://doi.org/10.1557/mrs.2019.104	journal	May 2019
In Situ and Operando Spectroscopy: A Powerful Approach Towards Understanding Catalysts Lukashuk, Liliana; Foettinger, Karin Johnson Matthey Technology Review, Vol. 62, Issue 3 https://doi.org/10.1595/205651318X15234323420569	journal	July 2018
Erosion of Carbon-Based Materials Under High-Fluence Heavy-Ion Irradiation Andrianova, N. N.; Borisov, A. M.; Mashkova, E. S. Journal of Spacecraft and Rockets, Vol. 48, Issue 1 https://doi.org/10.2514/1.49462	journal	January 2011
In Situ TEM Multi-Beam Ion Irradiation as a Technique for Elucidating Synergistic Radiation Effects Taylor, Caitlin; Bufford, Daniel; Muntifering, Brittany Materials, Vol. 10, Issue 10 https://doi.org/10.3390/ma10101148	journal	September 2017
Irradiation Induced Microstructure Evolution in Nanostructured Materials: A Review Liu, Wenbo; Ji, Yanzhou; Tan, Pengkang Materials, Vol. 9, Issue 2 https://doi.org/10.3390/ma9020105	journal	February 2016

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