ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa

Wang, Z.; McPherson, C.; Kadado, R.; Brandt, N.; Edwards, S.; Casey, W. H.; Curro, N. J.

doi:10.1103/physrevapplied.16.054014

Title: ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa

Abstract

Nitrogen-vacancy color centers in diamond have attracted broad attention as quantum sensors for both static and dynamic magnetic, electrical, strain, and thermal fields and are particularly attractive for quantum sensing under pressure in diamond anvil cells. Optically based nuclear magnetic resonance may be possible at pressures greater than a few gigapascals and offers an attractive alternative to conventional Faraday-induction-based detection. In this work, we present ac sensing results and demonstrate synchronized readout up to 6 GPa but find that the sensitivity is reduced due to inhomogeneities of the microwave field and pressure within the sample space. These experiments enable the possibility of all-optical high resolution magnetic resonance of nanoliter sample volumes at high pressures.

Authors:

Wang, Z. ^[1]; McPherson, C. ^[1]; Kadado, R. ^[1]; Brandt, N. ^[1];

^[1];

^[1]

Univ. of California, Davis, CA (United States)

Publication Date:: 2021-11-05

Research Org.:: Univ. of California, Davis, CA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division

OSTI Identifier:: 1830753

Grant/Contract Number:: FG02-05ER15693

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review Applied

Additional Journal Information:: Journal Volume: 16; Journal Issue: 5; Journal ID: ISSN 2331-7019

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 58 GEOSCIENCES; geochemistry; NMR spectroscopy; diamonds; high pressure

Citation Formats


                    Wang, Z., McPherson, C., Kadado, R., Brandt, N., Edwards, S., Casey, W. H., and Curro, N. J. ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa.  United States: N. p., 2021. 
Web.  doi:10.1103/physrevapplied.16.054014.

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                    Wang, Z., McPherson, C., Kadado, R., Brandt, N., Edwards, S., Casey, W. H., & Curro, N. J. ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa.  United States.  https://doi.org/10.1103/physrevapplied.16.054014

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                    Wang, Z., McPherson, C., Kadado, R., Brandt, N., Edwards, S., Casey, W. H., and Curro, N. J. Fri .  
"ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa".  United States.  https://doi.org/10.1103/physrevapplied.16.054014.  https://www.osti.gov/servlets/purl/1830753.

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@article{osti_1830753,

  title        = {ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa},

  author       = {Wang, Z. and McPherson, C. and Kadado, R. and Brandt, N. and Edwards, S. and Casey, W. H. and Curro, N. J.},

  abstractNote = {Nitrogen-vacancy color centers in diamond have attracted broad attention as quantum sensors for both static and dynamic magnetic, electrical, strain, and thermal fields and are particularly attractive for quantum sensing under pressure in diamond anvil cells. Optically based nuclear magnetic resonance may be possible at pressures greater than a few gigapascals and offers an attractive alternative to conventional Faraday-induction-based detection. In this work, we present ac sensing results and demonstrate synchronized readout up to 6 GPa but find that the sensitivity is reduced due to inhomogeneities of the microwave field and pressure within the sample space. These experiments enable the possibility of all-optical high resolution magnetic resonance of nanoliter sample volumes at high pressures.},

  doi          = {10.1103/physrevapplied.16.054014},

  journal      = {Physical Review Applied},

  number       = 5,

  volume       = 16,

  place        = {United States},

  year         = {2021},

  month        = {11}

}

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Similar Records

Title: ac Sensing Using Nitrogen-Vacancy Centers in a Diamond Anvil Cell up to 6 GPa

Abstract

Citation Formats

Electronic Properties and Metrology Applications of the Diamond NV − Center under Pressure journal, January 2014

Novel color center platforms enabling fundamental scientific discovery journal, June 2020

Diamond formation due to a pH drop during fluid–rock interactions journal, November 2015

NMR signal averaging in 62T pulsed fields journal, May 2011

Measuring magnetic field texture in correlated electron systems under extreme conditions journal, December 2019

Quantum diamond spectrometer for nanoscale NMR and ESR spectroscopy journal, August 2019

Imaging stress and magnetism at high pressures using a nanoscale quantum sensor journal, December 2019

Water in the deep Earth: The dielectric constant and the solubilities of quartz and corundum to 60kb and 1200°C journal, March 2014

Wide frequency dielectric properties of CVD diamond journal, April 1997

Optically detected magnetic resonance of high-density ensemble of NV − centers in diamond journal, May 2016

Submillihertz magnetic spectroscopy performed with a nanoscale quantum sensor journal, May 2017

Activation and Reaction Volumes in Solution. 3 journal, September 1998

Magnetic measurements on micrometer-sized samples under high pressure using designed NV centers journal, December 2019

Pressure calibration of diamond anvil Raman gauge to 310GPa journal, August 2006

Coherence levels and coherence pathways in NMR. A simple way to design phase cycling procedures journal, February 1984

Pressure and temperature dependence of the longitudinal proton relaxation times in supercooled water to −87 °C and 2500 bar journal, July 1977

Activation and reaction volumes in solution journal, August 1978

NMR at pressures up to 90 GPa journal, July 2018

Hyperfine interaction in the ground state of the negatively charged nitrogen vacancy center in diamond journal, February 2009

Magnetic flux tailoring through Lenz lenses for ultrasmall samples: A new pathway to high-pressure nuclear magnetic resonance journal, December 2017

NMR probe for high pressure and high temperature journal, November 1995

Epitaxial diamond encapsulation of metal microprobes for high pressure experiments journal, November 2000

Design and Analysis of Microcoils for NMR Microscopy journal, August 1995

The nitrogen-vacancy colour centre in diamond journal, July 2013

Improving resolution of solid state NMR in dense molecular hydrogen journal, September 2019

Hyperpolarization-Enhanced NMR Spectroscopy with Femtomole Sensitivity Using Quantum Defects in Diamond journal, June 2020

Perspectives of shaped pulses for EPR spectroscopy journal, July 2017

Activation and reaction volumes in solution. 2 journal, May 1989

Simple clamp pressure cell up to 30 kbar journal, October 1980

Magnetic Sensing inside a Diamond Anvil Cell via Nitrogen-Vacancy Center Spins * journal, August 2019

Diamond NV centers for quantum computing and quantum networks journal, February 2013

2 H and 139 La NMR Spectroscopy in Aqueous Solutions at Geochemical Pressures journal, September 2015

Ruby under pressure journal, June 2008

Carbon speciation in saline solutions in equilibrium with aragonite at high pressure journal, August 2016

Dielectric properties of water under extreme conditions and transport of carbonates in the deep Earth journal, March 2013

In situ Raman study and thermodynamic model of aqueous carbonate speciation in equilibrium with aragonite under subduction zone conditions journal, May 2014

High-resolution magnetic resonance spectroscopy using a solid-state spin sensor journal, March 2018

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Superconductivity at 250 K in lanthanum hydride under high pressures journal, May 2019

Quantum sensing journal, July 2017

New, compensated Carr-Purcell sequences journal, October 1990

Anvil cell gasket design for high pressure nuclear magnetic resonance experiments beyond 30 GPa journal, December 2015

Conventional superconductivity at 203 kelvin at high pressures in the sulfur hydride system journal, August 2015

Optically detected magnetic resonance of nitrogen vacancies in a diamond anvil cell using designer diamond anvils journal, November 2017

The signal-to-noise ratio of the nuclear magnetic resonance experiment journal, October 1976

A High-Pressure, High-Resolution NMR Probe for Experiments at 500 MHz journal, July 1998

Evidence for Superconductivity above 260 K in Lanthanum Superhydride at Megabar Pressures journal, January 2019

Evolution of hyperfine parameters across a quantum critical point in CeRhIn 5 journal, October 2015

Nonmagnetic indenter-type high-pressure cell for magnetic measurements journal, February 2007

Multipulse Double-Quantum Magnetometry with Near-Surface Nitrogen-Vacancy Centers journal, July 2014

High-sensitivity NMR beyond 200,000 atmospheres of pressure journal, August 2015

Electronic Properties and Metrology Applications of the Diamond ${NV}^{-}$ Center under Pressure
journal, January 2014

Novel color center platforms enabling fundamental scientific discovery
journal, June 2020

Diamond formation due to a pH drop during fluid–rock interactions
journal, November 2015

NMR signal averaging in 62T pulsed fields
journal, May 2011

Measuring magnetic field texture in correlated electron systems under extreme conditions
journal, December 2019

Quantum diamond spectrometer for nanoscale NMR and ESR spectroscopy
journal, August 2019

Imaging stress and magnetism at high pressures using a nanoscale quantum sensor
journal, December 2019

Water in the deep Earth: The dielectric constant and the solubilities of quartz and corundum to 60kb and 1200°C
journal, March 2014

Wide frequency dielectric properties of CVD diamond
journal, April 1997

Optically detected magnetic resonance of high-density ensemble of NV ⁻ centers in diamond
journal, May 2016

Submillihertz magnetic spectroscopy performed with a nanoscale quantum sensor
journal, May 2017

Activation and Reaction Volumes in Solution. 3
journal, September 1998

Magnetic measurements on micrometer-sized samples under high pressure using designed NV centers
journal, December 2019

Pressure calibration of diamond anvil Raman gauge to 310GPa
journal, August 2006

Coherence levels and coherence pathways in NMR. A simple way to design phase cycling procedures
journal, February 1984

Pressure and temperature dependence of the longitudinal proton relaxation times in supercooled water to −87 °C and 2500 bar
journal, July 1977

Activation and reaction volumes in solution
journal, August 1978

NMR at pressures up to 90 GPa
journal, July 2018

Hyperfine interaction in the ground state of the negatively charged nitrogen vacancy center in diamond
journal, February 2009

Magnetic flux tailoring through Lenz lenses for ultrasmall samples: A new pathway to high-pressure nuclear magnetic resonance
journal, December 2017

NMR probe for high pressure and high temperature
journal, November 1995

Epitaxial diamond encapsulation of metal microprobes for high pressure experiments
journal, November 2000

Design and Analysis of Microcoils for NMR Microscopy
journal, August 1995

The nitrogen-vacancy colour centre in diamond
journal, July 2013

Improving resolution of solid state NMR in dense molecular hydrogen
journal, September 2019

Hyperpolarization-Enhanced NMR Spectroscopy with Femtomole Sensitivity Using Quantum Defects in Diamond
journal, June 2020

Perspectives of shaped pulses for EPR spectroscopy
journal, July 2017

Activation and reaction volumes in solution. 2
journal, May 1989

Simple clamp pressure cell up to 30 kbar
journal, October 1980

Magnetic Sensing inside a Diamond Anvil Cell via Nitrogen-Vacancy Center Spins ^*
journal, August 2019

Diamond NV centers for quantum computing and quantum networks
journal, February 2013

² H and ¹³⁹ La NMR Spectroscopy in Aqueous Solutions at Geochemical Pressures
journal, September 2015

Ruby under pressure
journal, June 2008

Carbon speciation in saline solutions in equilibrium with aragonite at high pressure
journal, August 2016

Dielectric properties of water under extreme conditions and transport of carbonates in the deep Earth
journal, March 2013

In situ Raman study and thermodynamic model of aqueous carbonate speciation in equilibrium with aragonite under subduction zone conditions
journal, May 2014

High-resolution magnetic resonance spectroscopy using a solid-state spin sensor
journal, March 2018

Long-time electron spin storage via dynamical suppression of hyperfine-induced decoherence in a quantum dot
journal, March 2008

Superconductivity at 250 K in lanthanum hydride under high pressures
journal, May 2019

Quantum sensing
journal, July 2017

New, compensated Carr-Purcell sequences
journal, October 1990

Anvil cell gasket design for high pressure nuclear magnetic resonance experiments beyond 30 GPa
journal, December 2015

Conventional superconductivity at 203 kelvin at high pressures in the sulfur hydride system
journal, August 2015

Optically detected magnetic resonance of nitrogen vacancies in a diamond anvil cell using designer diamond anvils
journal, November 2017

The signal-to-noise ratio of the nuclear magnetic resonance experiment
journal, October 1976

A High-Pressure, High-Resolution NMR Probe for Experiments at 500 MHz
journal, July 1998

Evidence for Superconductivity above 260 K in Lanthanum Superhydride at Megabar Pressures
journal, January 2019

Evolution of hyperfine parameters across a quantum critical point in ${CeRhIn}_{5}$
journal, October 2015

Nonmagnetic indenter-type high-pressure cell for magnetic measurements
journal, February 2007

Multipulse Double-Quantum Magnetometry with Near-Surface Nitrogen-Vacancy Centers
journal, July 2014

High-sensitivity NMR beyond 200,000 atmospheres of pressure
journal, August 2015