When x-rays alter the course of your experiments

Bras, Wim; Myles, Dean A. A.; Felici, Roberto

doi:10.1088/1361-648x/ac1767

Title: When x-rays alter the course of your experiments

Journal Article · 08 August 2021 · Journal of Physics. Condensed Matter

DOI: https://doi.org/10.1088/1361-648x/ac1767 · OSTI ID:1813182

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Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
National Research Council (CNR), Rome (Italy)

The continuing increase in the brilliance of synchrotron radiation beamlines allows for many new and exciting experiments that were impossible before the present generation of synchrotron radiation sources came on line. However, the exposure to such intense beams also tests the limits of what samples can endure. Whilst the effects of radiation induced damage in a static experiment often can easily be recognized by changes in the diffraction or spectroscopy curves, the influence of radiation on chemical or physical processes, where one expects curves to change, is less often recognized and can be misinterpreted as a 'real' result instead of as a 'radiation influenced result'. This is especially a concern in time-resolved materials science experiments using techniques as powder diffraction, small angle scattering and x-ray absorption spectroscopy. In this work, the effects of radiation (5–50 keV) on some time-resolved processes in different types of materials and in different physical states are discussed. We show that such effects are not limited to soft matter and biology but rather can be found across the whole spectrum of materials research, over a large range of radiation doses and is not limited to very high brilliance beamlines.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1813182

Journal Information:: Journal of Physics. Condensed Matter, Journal Name: Journal of Physics. Condensed Matter Journal Issue: 42 Vol. 33; ISSN 0953-8984

Publisher:: IOP PublishingCopyright Statement

Country of Publication:: United States

Language:: English

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In situ small-angle X-ray scattering characterization of X-ray-induced local heating Witala, Monika; Han, Jun; Menzel, Andreas Journal of Applied Crystallography, Vol. 47, Issue 6 https://doi.org/10.1107/s1600576714020159	journal	October 2014
High-resolution thermal imaging with a combination of nano-focus X-ray diffraction and ultra-fast chip calorimetry Rosenthal, Martin; Doblas, David; Hernandez, Jaime J. Journal of Synchrotron Radiation, Vol. 21, Issue 1 https://doi.org/10.1107/s1600577513024892	journal	November 2013
X-ray irradiation induces local rearrangement of silica particles in swollen rubber Shinohara, Yuya; Yamamoto, Naoko; Kishimoto, Hiroyuki Journal of Synchrotron Radiation, Vol. 22, Issue 1 https://doi.org/10.1107/s1600577514022954	journal	January 2015
X-ray-induced Cu deposition and patterning on insulators at room temperature Hsu, Pei-Cheng; Chen, Yu-Sheng; Hwu, Yeukuang Journal of Synchrotron Radiation, Vol. 22, Issue 6 https://doi.org/10.1107/s1600577515015234	journal	September 2015
Simulated sample heating from a nanofocused X-ray beam Wallander, Harald; Wallentin, Jesper Journal of Synchrotron Radiation, Vol. 24, Issue 5 https://doi.org/10.1107/s1600577517008712	journal	August 2017
Nanoscale mapping of carrier collection in single nanowire solar cells using X-ray beam induced current Chayanun, Lert; Otnes, Gaute; Troian, Andrea Journal of Synchrotron Radiation, Vol. 26, Issue 1 https://doi.org/10.1107/s1600577518015229	journal	January 2019
Direct measurement of X-ray-induced heating of microcrystals Warren, Anna J.; Axford, Danny; Owen, Robin L. Journal of Synchrotron Radiation, Vol. 26, Issue 4 https://doi.org/10.1107/s1600577519003849	journal	May 2019
Water-mediated photo-induced reduction of platinum films Fraxedas, Jordi; Zhang, Kuan; Sepúlveda, Borja Journal of Synchrotron Radiation, Vol. 26, Issue 4 https://doi.org/10.1107/s1600577519004685	journal	June 2019
Solid/liquid-interface-dependent synthesis and immobilization of copper-based particles nucleated by X-ray-radiolysis-induced photochemical reaction Yamaguchi, Akinobu; Sakurai, Ikuya; Okada, Ikuo Journal of Synchrotron Radiation, Vol. 27, Issue 4 https://doi.org/10.1107/s1600577520005184	journal	May 2020
Deciphering the intrinsic dynamics from the beam-induced atomic motions in oxide glasses Chushkin, Yuriy Journal of Synchrotron Radiation, Vol. 27, Issue 5 https://doi.org/10.1107/s1600577520009753	journal	August 2020
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Estimation of Life Times and Diffusion Distances of Radicals Involved in X-Ray-Induced DNA Strand Breaks or Killing of Mammalian Cells Roots, Ruth; Okada, Shigefumi Radiation Research, Vol. 64, Issue 2 https://doi.org/10.2307/3574267	journal	November 1975
EPR studies on the interaction between additives and polyethylene matrix initiated by gamma radiation Przybytniak, G.; Sadlo, J.; Walo, M. Express Polymer Letters, Vol. 14, Issue 6 https://doi.org/10.3144/expresspolymlett.2020.45	journal	January 2020
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Data Mining of Polymer Phase Transitions upon Temperature Changes by Small and Wide-Angle X-ray Scattering Combined with Raman Spectroscopy Saidi, Sarah; Portale, Giuseppe; Bras, Wim Polymers, Vol. 13, Issue 23 https://doi.org/10.3390/polym13234203	journal	November 2021

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