Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms
Abstract
Bragg coherent diffraction imaging has the potential to provide significant insight into the structure-properties relationship for crystalline materials by imaging, with nanoscale resolution, three-dimensional strain fields within individual grains and nanoparticles. The capability of present-day synchrotrons to locate and measure a multiplicity of Bragg reflections from a single grain makes it possible to recover the full strain tensor with nanometer resolution. Recent methods for coupling reconstructions from several peaks to determine the strain tensor have been developed and applied to synthetic data, but have not been applied to experimental data. Here, using a coupled genetic reconstruction algorithm, we reconstruct an experimental data set and demonstrate improvements in the ability to resolve vector-valued displacement fields internal to the particle as compared to what is achieved with a noncoupled approach. The coupled approach developed in this work was also validated on simulated data sets. In both simulated and experimental data, reconstructions from our coupled Bragg peak algorithm show improvements over the noncoupled independent reconstruction method of 5% in terms of accuracy and 53% in terms of consistency.
- Authors:
-
[1];
[2];
[2];
[1];
[3];
[2];
[2];
[1];
[1]
- Carnegie Mellon Univ., Pittsburgh, PA (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Brigham Young Univ., Provo, UT (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division
- OSTI Identifier:
- 1807904
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Physical Review B
- Additional Journal Information:
- Journal Volume: 103; Journal Issue: 21; Journal ID: ISSN 2469-9950
- Publisher:
- American Physical Society (APS)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; Strain; Coherent X-ray scattering; Genetic algorithm; X-ray diffraction; X-ray imaging
Citation Formats
Wilkin, Matthew J., Maddali, Siddharth, Hruszkewycz, Stephan O., Pateras, Anastasios, Sandberg, Richard L., Harder, Ross, Cha, Wonsuk, Suter, Robert M., and Rollett, Anthony D. Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms. United States: N. p., 2021.
Web. doi:10.1103/physrevb.103.214103.
Wilkin, Matthew J., Maddali, Siddharth, Hruszkewycz, Stephan O., Pateras, Anastasios, Sandberg, Richard L., Harder, Ross, Cha, Wonsuk, Suter, Robert M., & Rollett, Anthony D. Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms. United States. https://doi.org/10.1103/physrevb.103.214103
Wilkin, Matthew J., Maddali, Siddharth, Hruszkewycz, Stephan O., Pateras, Anastasios, Sandberg, Richard L., Harder, Ross, Cha, Wonsuk, Suter, Robert M., and Rollett, Anthony D. Tue .
"Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms". United States. https://doi.org/10.1103/physrevb.103.214103. https://www.osti.gov/servlets/purl/1807904.
@article{osti_1807904,
title = {Experimental demonstration of coupled multi-peak Bragg coherent diffraction imaging with genetic algorithms},
author = {Wilkin, Matthew J. and Maddali, Siddharth and Hruszkewycz, Stephan O. and Pateras, Anastasios and Sandberg, Richard L. and Harder, Ross and Cha, Wonsuk and Suter, Robert M. and Rollett, Anthony D.},
abstractNote = {Bragg coherent diffraction imaging has the potential to provide significant insight into the structure-properties relationship for crystalline materials by imaging, with nanoscale resolution, three-dimensional strain fields within individual grains and nanoparticles. The capability of present-day synchrotrons to locate and measure a multiplicity of Bragg reflections from a single grain makes it possible to recover the full strain tensor with nanometer resolution. Recent methods for coupling reconstructions from several peaks to determine the strain tensor have been developed and applied to synthetic data, but have not been applied to experimental data. Here, using a coupled genetic reconstruction algorithm, we reconstruct an experimental data set and demonstrate improvements in the ability to resolve vector-valued displacement fields internal to the particle as compared to what is achieved with a noncoupled approach. The coupled approach developed in this work was also validated on simulated data sets. In both simulated and experimental data, reconstructions from our coupled Bragg peak algorithm show improvements over the noncoupled independent reconstruction method of 5% in terms of accuracy and 53% in terms of consistency.},
doi = {10.1103/physrevb.103.214103},
journal = {Physical Review B},
number = 21,
volume = 103,
place = {United States},
year = {Tue Jun 01 00:00:00 EDT 2021},
month = {Tue Jun 01 00:00:00 EDT 2021}
}
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