Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy

Li, Xinfeng; Li, Qizhen; Wang, Tan; Zhang, Jin

doi:10.1016/j.corsci.2019.108171

Title: Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy

Abstract

A nickel-based superalloy IN718 was fabricated by laser melting additive manufacturing process and hydrogen embrittlement (HE) behavior of this alloy was assessed via slow strain rate tensile tests. The results reveal that hydrogen-charged as-deposited samples along vertical plane exhibit the lowest susceptibility to HE, followed by as-deposited samples along horizontal plane and then heat-treated samples. Additionally, hydrogen-assisted cracking of as-deposited samples initiates from γ-matrix/Laves phase interfaces, whereas γ-matrix/δ phase interfaces along grain boundaries act as preferable damage sites for hydrogen charged heat-treated samples. These hydrogen-assisted cracking can be explained by synergistic effect of HELP mechanism and HEDE mechanism.

Authors:

Li, Xinfeng ^[1]; Li, Qizhen ^[2]; Wang, Tan ^[3]; Zhang, Jin ^[2]

Sun Yat-sen Univ., Zhuhai (China); Washington State Univ., Pullman, WA (United States)
Washington State Univ., Pullman, WA (United States)
Xi’an Jiaotong Univ. (China)

Publication Date:: Fri Aug 16 00:00:00 EDT 2019

Research Org.:: Washington State Univ., Pullman, WA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1802932

Alternate Identifier(s):: OSTI ID: 1775694

Grant/Contract Number:: SC0016333

Resource Type:: Accepted Manuscript

Journal Name:: Corrosion Science

Additional Journal Information:: Journal Volume: 160; Journal ID: ISSN 0010-938X

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; superalloy; tensile testing; hydrogen embrittlement; laser additive manufacturing

Citation Formats


                    Li, Xinfeng, Li, Qizhen, Wang, Tan, and Zhang, Jin. Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy.  United States: N. p., 2019. 
Web.  doi:10.1016/j.corsci.2019.108171.

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                    Li, Xinfeng, Li, Qizhen, Wang, Tan, & Zhang, Jin. Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy.  United States.  https://doi.org/10.1016/j.corsci.2019.108171

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                    Li, Xinfeng, Li, Qizhen, Wang, Tan, and Zhang, Jin. Fri .  
"Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy".  United States.  https://doi.org/10.1016/j.corsci.2019.108171.  https://www.osti.gov/servlets/purl/1802932.

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@article{osti_1802932,

  title        = {Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy},

  author       = {Li, Xinfeng and Li, Qizhen and Wang, Tan and Zhang, Jin},

  abstractNote = {A nickel-based superalloy IN718 was fabricated by laser melting additive manufacturing process and hydrogen embrittlement (HE) behavior of this alloy was assessed via slow strain rate tensile tests. The results reveal that hydrogen-charged as-deposited samples along vertical plane exhibit the lowest susceptibility to HE, followed by as-deposited samples along horizontal plane and then heat-treated samples. Additionally, hydrogen-assisted cracking of as-deposited samples initiates from γ-matrix/Laves phase interfaces, whereas γ-matrix/δ phase interfaces along grain boundaries act as preferable damage sites for hydrogen charged heat-treated samples. These hydrogen-assisted cracking can be explained by synergistic effect of HELP mechanism and HEDE mechanism.},

  doi          = {10.1016/j.corsci.2019.108171},

  journal      = {Corrosion Science},

  number       = ,

  volume       = 160,

  place        = {United States},

  year         = {Fri Aug 16 00:00:00 EDT 2019},

  month        = {Fri Aug 16 00:00:00 EDT 2019}

}

Copy to clipboard

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Title: Hydrogen-assisted failure of laser melting additive manufactured IN718 superalloy

Abstract

Citation Formats

The Role of Hydrogen and Other Interstitials in the Mechanical Behavior of Metals: (1959 Edward De Mille Campbell Memorial Lecture) journal, November 2016

Effect of hydrogen on the mechanical properties of alloy 945X (UNS N09945) and influence of microstructural features journal, January 2017

Microstructure and mechanical properties of Inconel 718 produced by selective laser melting: Sample orientation dependence and effects of post heat treatments journal, January 2018

The effect of nanosized (Ti,Mo)C precipitates on hydrogen embrittlement of tempered lath martensitic steel journal, August 2014

The advantage of grain refinement in the hydrogen embrittlement of Fe–18Mn–0.6C twinning-induced plasticity steel journal, April 2015

High temperature oxidation of IN 718 manufactured by laser beam melting and electron beam melting: Effect of surface topography journal, August 2018

Hydrogen compatibility of austenitic stainless steel tubing and orbital tube welds journal, December 2014

Effect of Strain Rate on the Hydrogen Embrittlement Property of Ultra High-strength Low Alloy TRIP-aided Steel journal, January 2018

Alloy 718 for Oilfield Applications journal, February 2012

Effect of heat treatment on hydrogen-assisted fracture behavior of PH13-8Mo steel journal, November 2017

Suppression of hydrogen embrittlement by formation of a stable austenite layer in metastable austenitic stainless steel journal, November 2014

Effects of ferrite/pearlite alignment on the hydrogen permeation in a AISI 4130 steel journal, November 1996

Dendritic microstructure and hot cracking of laser additive manufactured Inconel 718 under improved base cooling journal, June 2016

Correlation of mechanical properties to microstructure in Inconel 718 fabricated by Direct Metal Laser Sintering journal, January 2018

Mechanical properties and fracture behavior of hydrogen charged AHSS/UHSS grades at high- and low strain rate tests journal, January 2014

Additive manufacturing of metals journal, September 2016

Hydrogen-assisted failure in Ni-based superalloy 718 studied under in situ hydrogen charging: The role of localized deformation in crack propagation journal, April 2017

Study of the effect of δ phase on hydrogen embrittlement of Inconel 718 by notch tensile tests journal, February 2005

The role of localized deformation in hydrogen-assisted crack propagation in 21Cr–6Ni–9Mn stainless steel journal, August 2009

Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting journal, March 2012

Decrease in hydrogen embrittlement sensitivity of INCONEL 718 by laser surface softening journal, November 1996

Hydrogen-induced intergranular failure in nickel revisited journal, April 2012

Hydrogen-assisted decohesion and localized plasticity in dual-phase steel journal, May 2014

Effects of microstructure banding on hydrogen assisted fatigue crack growth in X65 pipeline steels journal, January 2016

Additive layer manufacturing of titanium matrix composites using the direct metal deposition laser process journal, November 2016

Rationalization of Microstructure Heterogeneity in INCONEL 718 Builds Made by the Direct Laser Additive Manufacturing Process journal, June 2014

Variation of hardness, microstructure, and Laves phase distribution in direct laser deposited alloy 718 cuboids journal, April 2017

Microstructure and directional fatigue behavior of Inconel 718 produced by selective laser melting journal, January 2016

The behavior of sensitized 309S stainless steel in hydrogen journal, June 1974

Hydrogen embrittlement behavior of Inconel 718 alloy at room temperature journal, April 2019

Hydrogen diffusion coefficients through Inconel 718 in different metallurgical conditions journal, March 2014

The microstructure and mechanical properties of deposited-IN718 by selective laser melting journal, February 2012

Effect of temperature on hydrogen embrittlement susceptibility of alloy 718 in Light Water Reactor environment journal, August 2017

Effects of precipitation phases on the hydrogen embrittlement sensitivity of Inconel 718 journal, January 2002

Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment journal, March 2017

Hydrogen embrittlement of AISI 4130 steel with an alternate ferrite/pearlite banded structure journal, August 1991

Corrosion in the Oil and Gas Industry: An Increasing Challenge for Materials journal, July 2013

Bending fatigue life characterisation of direct metal laser sintering nickel alloy 718: BENDING FATIGUE LIFE OF DIRECT METAL LASER SINTERING journal, February 2015

Effect of heat treatment on the microstructure and mechanical properties of Inconel 718 processed by selective laser melting journal, July 2015

An investigation of micro-mechanisms in hydrogen induced cracking in nickel-based superalloy 718 journal, April 2016

Effect of Microstructure and Alloy Chemistry on Hydrogen Embrittlement of Precipitation-Hardened Ni-Based Alloys journal, February 2018

Selective laser melting additive manufactured Inconel 718 superalloy parts: High-temperature oxidation property and its mechanisms journal, October 2014

Effect of microstructure on hydrogen diffusion and notch tensile strength of large steel forging journal, March 2015

Effect of standard heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 superalloy journal, September 2015

Suppression of hydrogen-assisted fatigue crack growth in austenitic stainless steel by cavitation peening journal, March 2012

Slow Strain Rate Testing for Hydrogen Embrittlement Susceptibility of Alloy 718 in Substitute Ocean Water journal, April 2017

Multi-scale and spatially resolved hydrogen mapping in a Ni–Nb model alloy reveals the role of the δ phase in hydrogen embrittlement of alloy 718 journal, May 2016

Tensile mechanical properties and fracture behaviors of nickel-based superalloy 718 in the presence of hydrogen journal, October 2018

Micro-and meso-structures and their influence on mechanical properties of selectively laser melted Ti-6Al-4V journal, August 2018

Microstructure and Mechanical Properties of Inconel 718 Produced by SLM and Subsequent Heat Treatment journal, July 2015

Anisotropy and heterogeneity of microstructure and mechanical properties in metal additive manufacturing: A critical review journal, February 2018

Laves phase control of Inconel 718 alloy using quasi-continuous-wave laser additive manufacturing journal, May 2017

The role of hydrogen in hydrogen embrittlement fracture of lath martensitic steel journal, August 2012

On the microstructural and mechanical properties of post-treated additively manufactured Inconel 718 superalloy under quasi-static and cyclic loading journal, July 2016

Study of the effect of hydrogen charging on the tensile properties and microstructure of four variant heat treatments of nickel alloy 718 journal, September 2017

Hydrogen-induced intergranular failure of iron journal, May 2014

The dual role of shot peening in hydrogen-assisted cracking of PSB1080 high strength steel journal, November 2016

Hydrogen assisted crack initiation and propagation in a nickel-based superalloy journal, July 2016

The Role of Hydrogen and Other Interstitials in the Mechanical Behavior of Metals: (1959 Edward De Mille Campbell Memorial Lecture)
journal, November 2016

Effect of hydrogen on the mechanical properties of alloy 945X (UNS N09945) and influence of microstructural features
journal, January 2017

Microstructure and mechanical properties of Inconel 718 produced by selective laser melting: Sample orientation dependence and effects of post heat treatments
journal, January 2018

The effect of nanosized (Ti,Mo)C precipitates on hydrogen embrittlement of tempered lath martensitic steel
journal, August 2014

The advantage of grain refinement in the hydrogen embrittlement of Fe–18Mn–0.6C twinning-induced plasticity steel
journal, April 2015

High temperature oxidation of IN 718 manufactured by laser beam melting and electron beam melting: Effect of surface topography
journal, August 2018

Hydrogen compatibility of austenitic stainless steel tubing and orbital tube welds
journal, December 2014

Effect of Strain Rate on the Hydrogen Embrittlement Property of Ultra High-strength Low Alloy TRIP-aided Steel
journal, January 2018

Alloy 718 for Oilfield Applications
journal, February 2012

Effect of heat treatment on hydrogen-assisted fracture behavior of PH13-8Mo steel
journal, November 2017

Suppression of hydrogen embrittlement by formation of a stable austenite layer in metastable austenitic stainless steel
journal, November 2014

Effects of ferrite/pearlite alignment on the hydrogen permeation in a AISI 4130 steel
journal, November 1996

Dendritic microstructure and hot cracking of laser additive manufactured Inconel 718 under improved base cooling
journal, June 2016

Correlation of mechanical properties to microstructure in Inconel 718 fabricated by Direct Metal Laser Sintering
journal, January 2018

Mechanical properties and fracture behavior of hydrogen charged AHSS/UHSS grades at high- and low strain rate tests
journal, January 2014

Additive manufacturing of metals
journal, September 2016

Hydrogen-assisted failure in Ni-based superalloy 718 studied under in situ hydrogen charging: The role of localized deformation in crack propagation
journal, April 2017

Study of the effect of δ phase on hydrogen embrittlement of Inconel 718 by notch tensile tests
journal, February 2005

The role of localized deformation in hydrogen-assisted crack propagation in 21Cr–6Ni–9Mn stainless steel
journal, August 2009

Microstructures and mechanical behavior of Inconel 718 fabricated by selective laser melting
journal, March 2012

Decrease in hydrogen embrittlement sensitivity of INCONEL 718 by laser surface softening
journal, November 1996

Hydrogen-induced intergranular failure in nickel revisited
journal, April 2012

Hydrogen-assisted decohesion and localized plasticity in dual-phase steel
journal, May 2014

Effects of microstructure banding on hydrogen assisted fatigue crack growth in X65 pipeline steels
journal, January 2016

Additive layer manufacturing of titanium matrix composites using the direct metal deposition laser process
journal, November 2016

Rationalization of Microstructure Heterogeneity in INCONEL 718 Builds Made by the Direct Laser Additive Manufacturing Process
journal, June 2014

Variation of hardness, microstructure, and Laves phase distribution in direct laser deposited alloy 718 cuboids
journal, April 2017

Microstructure and directional fatigue behavior of Inconel 718 produced by selective laser melting
journal, January 2016

The behavior of sensitized 309S stainless steel in hydrogen
journal, June 1974

Hydrogen embrittlement behavior of Inconel 718 alloy at room temperature
journal, April 2019

Hydrogen diffusion coefficients through Inconel 718 in different metallurgical conditions
journal, March 2014

The microstructure and mechanical properties of deposited-IN718 by selective laser melting
journal, February 2012

Effect of temperature on hydrogen embrittlement susceptibility of alloy 718 in Light Water Reactor environment
journal, August 2017

Effects of precipitation phases on the hydrogen embrittlement sensitivity of Inconel 718
journal, January 2002

Microstructure and hardness studies of Inconel 718 manufactured by selective laser melting before and after solution heat treatment
journal, March 2017

Hydrogen embrittlement of AISI 4130 steel with an alternate ferrite/pearlite banded structure
journal, August 1991

Corrosion in the Oil and Gas Industry: An Increasing Challenge for Materials
journal, July 2013

Bending fatigue life characterisation of direct metal laser sintering nickel alloy 718: BENDING FATIGUE LIFE OF DIRECT METAL LASER SINTERING
journal, February 2015

Effect of heat treatment on the microstructure and mechanical properties of Inconel 718 processed by selective laser melting
journal, July 2015

An investigation of micro-mechanisms in hydrogen induced cracking in nickel-based superalloy 718
journal, April 2016

Effect of Microstructure and Alloy Chemistry on Hydrogen Embrittlement of Precipitation-Hardened Ni-Based Alloys
journal, February 2018

Selective laser melting additive manufactured Inconel 718 superalloy parts: High-temperature oxidation property and its mechanisms
journal, October 2014

Effect of microstructure on hydrogen diffusion and notch tensile strength of large steel forging
journal, March 2015

Effect of standard heat treatment on the microstructure and mechanical properties of selective laser melting manufactured Inconel 718 superalloy
journal, September 2015

Suppression of hydrogen-assisted fatigue crack growth in austenitic stainless steel by cavitation peening
journal, March 2012

Slow Strain Rate Testing for Hydrogen Embrittlement Susceptibility of Alloy 718 in Substitute Ocean Water
journal, April 2017

Multi-scale and spatially resolved hydrogen mapping in a Ni–Nb model alloy reveals the role of the δ phase in hydrogen embrittlement of alloy 718
journal, May 2016

Tensile mechanical properties and fracture behaviors of nickel-based superalloy 718 in the presence of hydrogen
journal, October 2018

Micro-and meso-structures and their influence on mechanical properties of selectively laser melted Ti-6Al-4V
journal, August 2018

Microstructure and Mechanical Properties of Inconel 718 Produced by SLM and Subsequent Heat Treatment
journal, July 2015

Anisotropy and heterogeneity of microstructure and mechanical properties in metal additive manufacturing: A critical review
journal, February 2018

Laves phase control of Inconel 718 alloy using quasi-continuous-wave laser additive manufacturing
journal, May 2017

The role of hydrogen in hydrogen embrittlement fracture of lath martensitic steel
journal, August 2012

On the microstructural and mechanical properties of post-treated additively manufactured Inconel 718 superalloy under quasi-static and cyclic loading
journal, July 2016

Study of the effect of hydrogen charging on the tensile properties and microstructure of four variant heat treatments of nickel alloy 718
journal, September 2017

Hydrogen-induced intergranular failure of iron
journal, May 2014

The dual role of shot peening in hydrogen-assisted cracking of PSB1080 high strength steel
journal, November 2016

Hydrogen assisted crack initiation and propagation in a nickel-based superalloy
journal, July 2016