An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

Immoor, Julia; Marquardt, H.; Miyagi, L.; Speziale, S.; Merkel, S.; Schwark, I.; Ehnes, A.; Liermann, H. -P.

doi:10.1063/1.5143293

Title: An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

Abstract

We present an improved setup for the experimental study of deformation of solids at simultaneous high pressures and temperatures by radial x-ray diffraction. This technique employs a graphite resistive heated Mao–Bell type diamond anvil cell for radial x-ray diffraction in combination with a water-cooled vacuum chamber. The new chamber has been developed by the sample environment group at PETRA III and implemented at the Extreme Conditions Beamline P02.2 at PETRA III, DESY (Hamburg, Germany). Here, we discuss applications of the new setup to study deformation of a variety of materials, including ferropericlase, calcium perovskite, bridgmanite, and tantalum carbide, at high-pressure/temperature.

Authors:

^[1];

^[2];

^[3];

^[4];

^[5]; Schwark, I. ^[6]; Ehnes, A. ^[6];

^[6]

Univ. of Bayreuth (Germany)
Univ. of Oxford (United Kingdom)
Univ. of Utah, Salt Lake City, UT (United States)
German Research Center for Geosciences GFZ, Potsdam (Germany)
Univ. Lille (France)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

Publication Date:: Tue Apr 28 00:00:00 EDT 2020

Research Org.:: George Washington Univ., Washington, DC (United States); Univ. of Illinois, Chicago, IL (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA), Office of Defense Programs (DP); German Science Foundation; National Science Foundation (NSF); EU Framework Programme for Research and Innovation

OSTI Identifier:: 1801157

Alternate Identifier(s):: OSTI ID: 1824202

Grant/Contract Number:: NA0003858; MA4534/3-1; MA4534/4-1; EAR-1344579; EAR-1654687; 730872; NA0003975

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 91; Journal Issue: 4; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 47 OTHER INSTRUMENTATION; Instruments & Instrumentation; Physics; Ceramics; Diamond anvil cells; X-ray diffraction; Rheological properties; Perovskites; High pressure instruments

Citation Formats


                    Immoor, Julia, Marquardt, H., Miyagi, L., Speziale, S., Merkel, S., Schwark, I., Ehnes, A., and Liermann, H. -P. An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell.  United States: N. p., 2020. 
Web.  doi:10.1063/1.5143293.

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                    Immoor, Julia, Marquardt, H., Miyagi, L., Speziale, S., Merkel, S., Schwark, I., Ehnes, A., & Liermann, H. -P. An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell.  United States.  https://doi.org/10.1063/1.5143293

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                    Immoor, Julia, Marquardt, H., Miyagi, L., Speziale, S., Merkel, S., Schwark, I., Ehnes, A., and Liermann, H. -P. Tue .  
"An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell".  United States.  https://doi.org/10.1063/1.5143293.  https://www.osti.gov/servlets/purl/1801157.

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@article{osti_1801157,

  title        = {An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell},

  author       = {Immoor, Julia and Marquardt, H. and Miyagi, L. and Speziale, S. and Merkel, S. and Schwark, I. and Ehnes, A. and Liermann, H. -P.},

  abstractNote = {We present an improved setup for the experimental study of deformation of solids at simultaneous high pressures and temperatures by radial x-ray diffraction. This technique employs a graphite resistive heated Mao–Bell type diamond anvil cell for radial x-ray diffraction in combination with a water-cooled vacuum chamber. The new chamber has been developed by the sample environment group at PETRA III and implemented at the Extreme Conditions Beamline P02.2 at PETRA III, DESY (Hamburg, Germany). Here, we discuss applications of the new setup to study deformation of a variety of materials, including ferropericlase, calcium perovskite, bridgmanite, and tantalum carbide, at high-pressure/temperature.},

  doi          = {10.1063/1.5143293},

  journal      = {Review of Scientific Instruments},

  number       = 4,

  volume       = 91,

  place        = {United States},

  year         = {Tue Apr 28 00:00:00 EDT 2020},

  month        = {Tue Apr 28 00:00:00 EDT 2020}

}

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Title: An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

Abstract

Citation Formats

Evaluating post-perovskite as a cause of D′′ anisotropy in regions of palaeosubduction journal, December 2012

The role of recrystallization in the preferred orientation of olivine journal, June 1988

Ab initio study of the high-pressure behavior of CaSiO3 perovskite text, January 2005

Deformation experiment at P–T conditions of the mantle transition zone using D-DIA apparatus journal, November 2010

Ferropericlase Control of Lower Mantle Rheology : Impact of Phase Morphology text, January 2020

Anisotropy in the deep Earth journal, August 2017

Flow laws for rocks containing two non-linear viscous phases: A phenomenological approach journal, March 1994

Ab initio molecular dynamics study of Ca Si O 3 perovskite at P − T conditions of Earth’s lower mantle journal, May 2006

Shear deformation of bridgmanite and magnesiowustite aggregates at lower mantle conditions journal, December 2015

The deformation-DIA: A new apparatus for high temperature triaxial deformation to pressures up to 15 GPa journal, June 2003

Diamond anvil cell deformation of CaSiO3 perovskite up to 49GPa journal, May 2009

Toward an internally consistent pressure scale journal, May 2007

Ferropericlase Control of Lower Mantle Rheology: Impact of Phase Morphology journal, January 2020

Slab stagnation in the shallow lower mantle linked to an increase in mantle viscosity journal, March 2015

Phase transition in CaSiO3 perovskite journal, August 2007

Superplasticity in Earth's Lower Mantle: Evidence from Seismic Anisotropy and Rock Physics journal, October 1995

Non-cubic crystal symmetry of CaSiO3 perovskite up to 18 GPa and 1600 K journal, May 2009

Mantle Convection and Plate Tectonics: Toward an Integrated Physical and Chemical Theory journal, June 2000

The equation of state of TaC0.99 by X-ray diffraction in radial scattering geometry to 32 GPa and 1073 K journal, September 2019

Deformation of (Mg,Fe)SiO3 Post-Perovskite and D'' Anisotropy journal, June 2007

Two-phase deformation of lower mantle mineral analogs journal, December 2016

Deformation of polycrystalline MgO at pressures of the lower mantle: DEFORMATION OF MgO AT HIGH PRESSURE journal, November 2002

In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K text, January 2013

Combined resistive and laser heating technique for in situ radial X-ray diffraction in the diamond anvil cell at high pressure and temperature journal, February 2013

High-pressure rotational deformation apparatus to 15 GPa journal, November 2001

Deformation of lower-mantle ferropericlase (Mg,Fe)O across the electronic spin transition journal, April 2009

A cubic boron nitride gasket for diamond-anvil experiments journal, May 2008

Mantle dynamics inferred from the crystallographic preferred orientation of bridgmanite journal, October 2016

X-ray transparent gasket for diamond anvil cell high pressure experiments journal, April 2005

Elastic Shear Anisotropy of Ferropericlase in Earth's Lower Mantle journal, April 2009

Experimental method for in situ determination of material textures at simultaneous high pressure and high temperature by means of radial diffraction in the diamond anvil cell journal, October 2009

Rheology of the Upper Mantle: A Synthesis journal, May 1993

A convection model to explain anisotropy of the inner core journal, March 2000

Texture development and elastic stresses in magnesiowűstite at high pressure journal, January 2006

Rheology of the lower mantle journal, January 1981

Some mineral physics constraints on the rheology and geothermal structure of Earth’s lower mantle journal, April 2001

Seismic anisotropy in the mantle transition zone induced by shear deformation of wadsleyite journal, March 2013

In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K journal, August 2013

Ab initio study of the high-pressure behavior of CaSiO3 perovskite journal, May 2005

Evidence for {100}<011> slip in ferropericlase in Earth's lower mantle from high-pressure/high-temperature experiments journal, May 2018

In situ laser heating and radial synchrotron x-ray diffraction in a diamond anvil cell journal, June 2007

Note: Modified anvil design for improved reliability in DT-Cup experiments journal, December 2017

High-pressure, high-temperature deformation of CaGeO 3 (perovskite)±MgO aggregates: Implications for multiphase rheology of the lower mantle : DEFORMATION OF TWO-PHASE AGGREGATES journal, September 2013

Evaluating post-perovskite as a cause of D′′ anisotropy in regions of palaeosubduction
journal, December 2012

The role of recrystallization in the preferred orientation of olivine
journal, June 1988

Ab initio study of the high-pressure behavior of CaSiO3 perovskite
text, January 2005

Deformation experiment at P–T conditions of the mantle transition zone using D-DIA apparatus
journal, November 2010

Ferropericlase Control of Lower Mantle Rheology : Impact of Phase Morphology
text, January 2020

Anisotropy in the deep Earth
journal, August 2017

Flow laws for rocks containing two non-linear viscous phases: A phenomenological approach
journal, March 1994

Ab initio molecular dynamics study of $Ca Si O_{3}$ perovskite at $P − T$ conditions of Earth’s lower mantle
journal, May 2006

Shear deformation of bridgmanite and magnesiowustite aggregates at lower mantle conditions
journal, December 2015

The deformation-DIA: A new apparatus for high temperature triaxial deformation to pressures up to 15 GPa
journal, June 2003

Diamond anvil cell deformation of CaSiO3 perovskite up to 49GPa
journal, May 2009

Toward an internally consistent pressure scale
journal, May 2007

Ferropericlase Control of Lower Mantle Rheology: Impact of Phase Morphology
journal, January 2020

Slab stagnation in the shallow lower mantle linked to an increase in mantle viscosity
journal, March 2015

Phase transition in CaSiO3 perovskite
journal, August 2007

Superplasticity in Earth's Lower Mantle: Evidence from Seismic Anisotropy and Rock Physics
journal, October 1995

Non-cubic crystal symmetry of CaSiO3 perovskite up to 18 GPa and 1600 K
journal, May 2009

Mantle Convection and Plate Tectonics: Toward an Integrated Physical and Chemical Theory
journal, June 2000

The equation of state of TaC0.99 by X-ray diffraction in radial scattering geometry to 32 GPa and 1073 K
journal, September 2019

Deformation of (Mg,Fe)SiO3 Post-Perovskite and D'' Anisotropy
journal, June 2007

Two-phase deformation of lower mantle mineral analogs
journal, December 2016

Deformation of polycrystalline MgO at pressures of the lower mantle: DEFORMATION OF MgO AT HIGH PRESSURE
journal, November 2002

In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K
text, January 2013

Combined resistive and laser heating technique for in situ radial X-ray diffraction in the diamond anvil cell at high pressure and temperature
journal, February 2013

High-pressure rotational deformation apparatus to 15 GPa
journal, November 2001

Deformation of lower-mantle ferropericlase (Mg,Fe)O across the electronic spin transition
journal, April 2009

A cubic boron nitride gasket for diamond-anvil experiments
journal, May 2008

Mantle dynamics inferred from the crystallographic preferred orientation of bridgmanite
journal, October 2016

X-ray transparent gasket for diamond anvil cell high pressure experiments
journal, April 2005

Elastic Shear Anisotropy of Ferropericlase in Earth's Lower Mantle
journal, April 2009

Experimental method for in situ determination of material textures at simultaneous high pressure and high temperature by means of radial diffraction in the diamond anvil cell
journal, October 2009

Rheology of the Upper Mantle: A Synthesis
journal, May 1993

A convection model to explain anisotropy of the inner core
journal, March 2000

Texture development and elastic stresses in magnesiowűstite at high pressure
journal, January 2006

Rheology of the lower mantle
journal, January 1981

Some mineral physics constraints on the rheology and geothermal structure of Earth’s lower mantle
journal, April 2001

Seismic anisotropy in the mantle transition zone induced by shear deformation of wadsleyite
journal, March 2013

In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K
journal, August 2013

Ab initio study of the high-pressure behavior of CaSiO3 perovskite
journal, May 2005

Evidence for {100}<011> slip in ferropericlase in Earth's lower mantle from high-pressure/high-temperature experiments
journal, May 2018

In situ laser heating and radial synchrotron x-ray diffraction in a diamond anvil cell
journal, June 2007

Note: Modified anvil design for improved reliability in DT-Cup experiments
journal, December 2017

High-pressure, high-temperature deformation of CaGeO ₃ (perovskite)±MgO aggregates: Implications for multiphase rheology of the lower mantle : DEFORMATION OF TWO-PHASE AGGREGATES
journal, September 2013