Title: Mild hydrothermal synthesis of potassium uranyl phosphates with layered and framework structures

Journal Article · · Journal of Solid State Chemistry
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Sponsoring Organization:
USDOE
OSTI ID:
1787926
Journal Information:
Journal of Solid State Chemistry, Journal Name: Journal of Solid State Chemistry Journal Issue: C Vol. 301; ISSN 0022-4596
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English

References (39)

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Crystal Structures of Three Framework Alkali Metal Uranyl Phosphate Hydrates journal August 2002
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Fluorescence spectroscopy of U(VI)-silicates and U(VI)-contaminated Hanford sediment journal March 2005
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Structures and syntheses of layered and framework amine-bearing uranyl phosphate and uranyl arsenates journal August 2004
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Crystal chemistry of anhydrous Li uranyl phosphates and arsenates. II. Tubular fragments and cation–cation interactions in the 3D framework structures of Li6[(UO2)12(PO4)8(P4O13)], Li5[(UO2)13(AsO4)9(As2O7)], Li[(UO2)4(AsO4)3] and Li3[(UO2)7(AsO4)5O)] journal November 2009
Synthesis, structure, and spectroscopic characterization of three uranyl phosphates with unique structural units journal December 2012
Copper uranyl phosphate and arsenate incorporating an organic ligand with a pillared layer structure: [Cu(4,4′-bpy)(UO2)0.5(HPO4)(H2PO4)]·H2O and [Cu(4,4′-bpy)(UO2)0.5(HAsO4)(H2AsO4)]·1.5H2O journal January 2013
Crystal Growth and Structure Characterization of Three Layered Uranyl Phosphates and Their Relation to the Phosphuranylite Family journal December 2018
Hierarchical Materials as Tailored Nuclear Waste Forms: A Perspective journal June 2018
Flux versus Hydrothermal Growth: Polymorphism of A 2 (UO 2 )Si 2 O 6 (A = Rb, Cs) journal January 2017
Observation of an Unusual Uranyl Cation–Cation Interaction in the Strongly Fluorescent Layered Uranyl Phosphates Rb 6 [(UO 2 ) 7 O 4 (PO 4 ) 4 ] and Cs 6 [(UO 2 ) 7 O 4 (PO 4 ) 4 ] journal December 2017
A Family of Layered Phosphates Crystallizing in a Rare Geometrical Isomer of the Phosphuranylite Topology: Synthesis, Characterization, and Computational Modeling of A 4 [(UO 2 ) 3 O 2 (PO 4 ) 2 ] (A = Alkali Metal) Exhibiting Intralayer Ion Exchange journal March 2018
Overstepping Löwenstein’s Rule—A Route to Unique Aluminophosphate Frameworks with Three-Dimensional Salt-Inclusion and Ion-Exchange Properties journal December 2018
Syntheses, Structures, and Comparisons of Thallium Uranium Phosphites, Mixed Phosphate-Phosphites, and Phosphate journal March 2013
Observation of Multiple Crystal-to-Crystal Transitions in a New Reduced Vanadium Oxalate Hybrid Material, Ba 3 [(VO) 2 (C 2 O 4 ) 5 (H 2 O) 6 ]·(H 2 O) 3 , Prepared via a Mild, Two-Step Hydrothermal Method journal August 2014
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A New Uranium(VI) Monophosphate with a Layered Structure:  Ba 3 [UO 2 (PO 4 )(PO 3 (OH))] 2 · x H 2 O ( x ≈ 0.4) journal November 1998
Influence of Phosphate and Silica on U(VI) Precipitation from Acidic and Neutralized Wastewaters journal May 2014
An Unprecedented Uranyl Phosphate Framework in the Structure of [(UO 2 ) 3 (PO 4 )O(OH)(H 2 O) 2 ](H 2 O) journal March 2004
Syntheses, Structures, and Ion-Exchange Properties of the Three-Dimensional Framework Uranyl Gallium Phosphates, Cs 4 [(UO 2 ) 2 (GaOH) 2 (PO 4 ) 4 ]·H 2 O and Cs[UO 2 Ga(PO 4 ) 2 ] journal January 2005
General Route to Three-Dimensional Framework Uranyl Transition Metal Phosphates with Atypical Structural Motifs:  The Case Examples of Cs 2 {(UO 2 ) 4 [Co(H 2 O) 2 ] 2 (HPO 4 )(PO 4 ) 4 } and Cs 3+ x [(UO 2 ) 3 CuH 4 - x (PO 4 ) 5 ]·H 2 O journal March 2006
Cation−Cation Interactions in Sr 5 (UO 2 ) 20 (UO 6 ) 2 O 16 (OH) 6 (H 2 O) 6 and Cs(UO 2 ) 9 U 3 O 16 (OH) 5 journal November 2006
Synthesis and Structural and Magnetic Characterization of {[(phen) 2 Ni] 2 (μ-P 2 O 7 )}·27H 2 O and {[(phen) 2 Mn] 2 (μ-P 2 O 7 )}·13H 2 O:  Rare Examples of Coordination Complexes with the Pyrophosphate Ligand journal August 2007
Polymerization and Depolymerization Phenomena in Phosphate–Metaphosphate Systems at Higher Temperatures. Condensation Reactions Involving the Potassium Hydrogen Orthophosphates journal January 1952
Organically templated layered uranium(VI) phosphates: hydrothermal syntheses and structures of [NHEt3][(UO2)2(PO4)(HPO4)] and [NPr4][(UO2)3(PO4)(HPO4)2] journal January 1998
The novel open-framework uranium silicates Na2(UO2)(Si4O10)·2.1H2O (USH-1) and RbNa(UO2)(Si2O6)·H2O (USH-3) journal January 2002
Hydrothermal synthesis and structures of the new open-framework uranyl silicates Rb4(UO2)2(Si8O20) (USH-2Rb), Rb2(UO2)(Si2O6)·H2O (USH-4Rb) and A2(UO2)(Si2O6)·0.5H2O (USH-5A; A = Rb, Cs) journal December 2002
Exfoliation of crystals journal September 2018
Single-crystal structure validation with the program PLATON journal January 2003
OLEX2 : a complete structure solution, refinement and analysis program journal January 2009
A short history of SHELX journal December 2007
Bond-valence parameters obtained from a systematic analysis of the Inorganic Crystal Structure Database journal August 1985
SHELXT – Integrated space-group and crystal-structure determination journal January 2015
Synthesis and study of potassium uranates K2U6O19 and K2U4O13·2.2H2O journal November 2015
Observation of the Same New Sheet Topology in Both the Layered Uranyl Oxide-Phosphate Cs11[(UO2)12(PO4)3O13] and the Layered Uranyl Oxyfluoride-Phosphate Rb11[(UO2)12(PO4)3O12F2] Prepared by Flux Crystal Growth journal August 2019
A Revised and Expanded Structure Hierarchy of Natural and Synthetic Hexavalent Uranium Compounds journal January 2016

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