New reflections on hard X-ray photon-in/photon-out spectroscopy
Abstract
Analysis of the electronic structure and local coordination of an element is an important aspect in the study of the chemical and physical properties of materials. This is particularly relevant at the nanoscale where new phases of matter may emerge below a critical size. X-ray emission spectroscopy (XES) at synchrotron radiation sources and free electron lasers has enriched the field of X-ray spectroscopy. Additionally, the spectroscopic techniques derived from the combination of X-ray absorption and emission spectroscopy (XAS–XES), such as resonant inelastic X-ray scattering (RIXS) and high energy resolution fluorescence detected (HERFD) XAS, are an ideal tool for the study of nanomaterials. New installations and beamline upgrades now often include wavelength dispersive instruments for the analysis of the emitted X-rays. With the growing use of XAS–XES, scientists are learning about the possibilities and pitfalls. We discuss some experimental aspects, assess the feasibility of measuring weak fluorescence lines in dilute, radiation sensitive samples, and present new experimental approaches for studying magnetic properties of colloidal nanoparticles directly in the liquid phase.
- Authors:
-
- European Synchrotron Radiation Facility (ESRF), Grenoble (France)
- Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
- Publication Date:
- Research Org.:
- Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC)
- OSTI Identifier:
- 1782156
- Alternate Identifier(s):
- OSTI ID: 1643720
- Grant/Contract Number:
- AC02-05CH11231
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nanoscale
- Additional Journal Information:
- Journal Volume: 12; Journal Issue: 30; Journal ID: ISSN 2040-3364
- Publisher:
- Royal Society of Chemistry
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Lafuerza, Sara, Retegan, Marius, Detlefs, Blanka, Chatterjee, Ruchira, Yachandra, Vittal, Yano, Junko, and Glatzel, Pieter. New reflections on hard X-ray photon-in/photon-out spectroscopy. United States: N. p., 2020.
Web. doi:10.1039/d0nr01983f.
Lafuerza, Sara, Retegan, Marius, Detlefs, Blanka, Chatterjee, Ruchira, Yachandra, Vittal, Yano, Junko, & Glatzel, Pieter. New reflections on hard X-ray photon-in/photon-out spectroscopy. United States. https://doi.org/10.1039/d0nr01983f
Lafuerza, Sara, Retegan, Marius, Detlefs, Blanka, Chatterjee, Ruchira, Yachandra, Vittal, Yano, Junko, and Glatzel, Pieter. Fri .
"New reflections on hard X-ray photon-in/photon-out spectroscopy". United States. https://doi.org/10.1039/d0nr01983f. https://www.osti.gov/servlets/purl/1782156.
@article{osti_1782156,
title = {New reflections on hard X-ray photon-in/photon-out spectroscopy},
author = {Lafuerza, Sara and Retegan, Marius and Detlefs, Blanka and Chatterjee, Ruchira and Yachandra, Vittal and Yano, Junko and Glatzel, Pieter},
abstractNote = {Analysis of the electronic structure and local coordination of an element is an important aspect in the study of the chemical and physical properties of materials. This is particularly relevant at the nanoscale where new phases of matter may emerge below a critical size. X-ray emission spectroscopy (XES) at synchrotron radiation sources and free electron lasers has enriched the field of X-ray spectroscopy. Additionally, the spectroscopic techniques derived from the combination of X-ray absorption and emission spectroscopy (XAS–XES), such as resonant inelastic X-ray scattering (RIXS) and high energy resolution fluorescence detected (HERFD) XAS, are an ideal tool for the study of nanomaterials. New installations and beamline upgrades now often include wavelength dispersive instruments for the analysis of the emitted X-rays. With the growing use of XAS–XES, scientists are learning about the possibilities and pitfalls. We discuss some experimental aspects, assess the feasibility of measuring weak fluorescence lines in dilute, radiation sensitive samples, and present new experimental approaches for studying magnetic properties of colloidal nanoparticles directly in the liquid phase.},
doi = {10.1039/d0nr01983f},
journal = {Nanoscale},
number = 30,
volume = 12,
place = {United States},
year = {Fri Jul 17 00:00:00 EDT 2020},
month = {Fri Jul 17 00:00:00 EDT 2020}
}
Web of Science
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