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Title: Operando measurement of lattice strain in internal combustion engine components by neutron diffraction

Abstract

Engineering neutron diffraction can nondestructively and noninvasively probe stress, strain, temperature, and phase evolutions deep within bulk materials. In this work, we demonstrate operando lattice strain measurement of internal combustion engine components by neutron diffraction. A modified commercial generator engine was mounted in the VULCAN diffractometer at the Spallation Neutron Source, and the lattice strains in both the cylinder block and head were measured under static nonfiring conditions as well as steady state and cyclic transient operation. The dynamic temporal response of the lattice strain change during transient operation was resolved in two locations by asynchronous stroboscopic neutron diffraction. We demonstrated that operando neutron measurements can allow for understanding of how materials behave throughout operational engineering devices. This study opens a pathway for the industrial and academic communities to better understand the complexities of material behavior during the operation of internal combustion engines and other real-scale devices and systems and to leverage techniques developed here for future investigations of numerous new platforms and alloys.

Authors:
ORCiD logo [1];  [2]; ORCiD logo [2]; ORCiD logo [1];  [3];  [4]; ORCiD logo [5];  [6]; ORCiD logo [2]
  1. Energy Science and Technology Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 37831,
  2. Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 37831,
  3. Physical Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 37831,, Department of Materials Science and Engineering, The University of Tennessee, Knoxville, TN 37996,
  4. Physical Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 37831,, The Bredesen Center for Interdisciplinary Research and Graduate Education, The University of Tennessee, Knoxville, TN 37996,
  5. Eck Industries, Inc., Manitowoc, WI 54220,
  6. Physical Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 37831,, US Navy, Washington, DC 20350
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC); USDOE Office of Energy Efficiency and Renewable Energy (EERE)
OSTI Identifier:
1742079
Alternate Identifier(s):
OSTI ID: 1787233; OSTI ID: 1808407
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Published Article
Journal Name:
Proceedings of the National Academy of Sciences of the United States of America
Additional Journal Information:
Journal Name: Proceedings of the National Academy of Sciences of the United States of America Journal Volume: 117 Journal Issue: 52; Journal ID: ISSN 0027-8424
Publisher:
Proceedings of the National Academy of Sciences
Country of Publication:
United States
Language:
English
Subject:
72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS; neutron diffraction; operando; in situ; internal combustion engine; time-resolved

Citation Formats

Wissink, Martin L., Chen, Yan, Frost, Matthew J., Curran, Scott J., Rios, Orlando, Sims, Zachary C., Weiss, David, Stromme, Eric T., and An, Ke. Operando measurement of lattice strain in internal combustion engine components by neutron diffraction. United States: N. p., 2020. Web. doi:10.1073/pnas.2012960117.
Wissink, Martin L., Chen, Yan, Frost, Matthew J., Curran, Scott J., Rios, Orlando, Sims, Zachary C., Weiss, David, Stromme, Eric T., & An, Ke. Operando measurement of lattice strain in internal combustion engine components by neutron diffraction. United States. https://doi.org/10.1073/pnas.2012960117
Wissink, Martin L., Chen, Yan, Frost, Matthew J., Curran, Scott J., Rios, Orlando, Sims, Zachary C., Weiss, David, Stromme, Eric T., and An, Ke. Mon . "Operando measurement of lattice strain in internal combustion engine components by neutron diffraction". United States. https://doi.org/10.1073/pnas.2012960117.
@article{osti_1742079,
title = {Operando measurement of lattice strain in internal combustion engine components by neutron diffraction},
author = {Wissink, Martin L. and Chen, Yan and Frost, Matthew J. and Curran, Scott J. and Rios, Orlando and Sims, Zachary C. and Weiss, David and Stromme, Eric T. and An, Ke},
abstractNote = {Engineering neutron diffraction can nondestructively and noninvasively probe stress, strain, temperature, and phase evolutions deep within bulk materials. In this work, we demonstrate operando lattice strain measurement of internal combustion engine components by neutron diffraction. A modified commercial generator engine was mounted in the VULCAN diffractometer at the Spallation Neutron Source, and the lattice strains in both the cylinder block and head were measured under static nonfiring conditions as well as steady state and cyclic transient operation. The dynamic temporal response of the lattice strain change during transient operation was resolved in two locations by asynchronous stroboscopic neutron diffraction. We demonstrated that operando neutron measurements can allow for understanding of how materials behave throughout operational engineering devices. This study opens a pathway for the industrial and academic communities to better understand the complexities of material behavior during the operation of internal combustion engines and other real-scale devices and systems and to leverage techniques developed here for future investigations of numerous new platforms and alloys.},
doi = {10.1073/pnas.2012960117},
journal = {Proceedings of the National Academy of Sciences of the United States of America},
number = 52,
volume = 117,
place = {United States},
year = {Mon Dec 21 00:00:00 EST 2020},
month = {Mon Dec 21 00:00:00 EST 2020}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1073/pnas.2012960117

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Works referenced in this record:

VULCAN: A “hammer” for high-temperature materials research
journal, November 2019


Additively Manufactured Single-Use Molds and Reusable Patterns for Large Automotive and Hydroelectric Components
journal, October 2019

  • Henderson, Hunter B.; Stromme, Eric T.; Kesler, Michael S.
  • International Journal of Metalcasting, Vol. 14, Issue 2
  • DOI: 10.1007/s40962-019-00379-0

Analysis of pre-ignition to super-knock: Hotspot-induced deflagration to detonation
journal, March 2015


Introduction to the Characterization of Residual Stress by Neutron Diffraction
book, January 2005


EXPGUI , a graphical user interface for GSAS
journal, April 2001


PIND: High spatial resolution by pinhole neutron diffraction
journal, June 2018

  • Wu, Wei; Stoica, Alexandru D.; Berry, Kevin D.
  • Applied Physics Letters, Vol. 112, Issue 25
  • DOI: 10.1063/1.5026066

First In Situ Lattice Strains Measurements Under Load at VULCAN
journal, October 2010

  • An, Ke; Skorpenske, Harley D.; Stoica, Alexandru D.
  • Metallurgical and Materials Transactions A, Vol. 42, Issue 1
  • DOI: 10.1007/s11661-010-0495-9

A profile refinement method for nuclear and magnetic structures
journal, June 1969


Jet-Wall Interaction Effects on Diesel Combustion and Soot Formation
conference, April 2005

  • Pickett, Lyle M.; López, J. Javier
  • SAE 2005 World Congress & Exhibition, SAE Technical Paper Series
  • DOI: 10.4271/2005-01-0921

High performance aluminum–cerium alloys for high-temperature applications
journal, January 2017

  • Sims, Zachary C.; Rios, Orlando R.; Weiss, David
  • Materials Horizons, Vol. 4, Issue 6
  • DOI: 10.1039/C7MH00391A

RHEGAL: Resistive heating gas enclosure loadframe for in situ neutron scattering
journal, September 2018

  • An, Ke; Armitage, Douglas P.; Yu, Zhenzhen
  • Review of Scientific Instruments, Vol. 89, Issue 9
  • DOI: 10.1063/1.5033566

Event-based processing of neutron scattering data at the Spallation Neutron Source
journal, May 2018

  • Granroth, Garrett E.; An, Ke; Smith, Hillary L.
  • Journal of Applied Crystallography, Vol. 51, Issue 3
  • DOI: 10.1107/S1600576718004727

Bending Behavior of a Wrought Magnesium Alloy Investigated by the In Situ Pinhole Neutron Diffraction Method
journal, August 2018


Gasoline Wall Films and Spray/Wall Interaction Analyzed by Infrared Thermography
journal, April 2014

  • Schulz, Florian; Schmidt, Jürgen; Kufferath, Andreas
  • SAE International Journal of Engines, Vol. 7, Issue 3
  • DOI: 10.4271/2014-01-1446

Experimental Investigation of Fuel Impingement and Spray-Cooling on the Piston of a GDI Engine via Instantaneous Surface Temperature Measurements
journal, April 2014

  • Köpple, Fabian; Seboldt, Dimitri; Jochmann, Paul
  • SAE International Journal of Engines, Vol. 7, Issue 3
  • DOI: 10.4271/2014-01-1447