Spectrally tunable infrared plasmonic F,Sn:In2O3 nanocrystal cubes

Cho, Shin Hum; Roccapriore, Kevin M.; Dass, Chandriker Kavir; Ghosh, Sandeep; Choi, Junho; Noh, Jungchul; Reimnitz, Lauren C.; Heo, Sungyeon; Kim, Kihoon; Xie, Karen; Korgel, Brian A.; Li, Xiaoqin; Hendrickson, Joshua R.; Hachtel, Jordan A.; Milliron, Delia J.

doi:10.1063/1.5139050

Title: Spectrally tunable infrared plasmonic F,Sn:In₂O₃ nanocrystal cubes

Journal Article · 06 January 2020 · Journal of Chemical Physics

DOI: https://doi.org/10.1063/1.5139050 · OSTI ID:1720250

^[1];

^[2]; Dass, Chandriker Kavir ^[3]; Ghosh, Sandeep ^[1]; Choi, Junho ^[1]; Noh, Jungchul ^[1]; Reimnitz, Lauren C. ^[1]; Heo, Sungyeon ^[4]; Kim, Kihoon ^[1]; Xie, Karen ^[1]; Korgel, Brian A. ^[1]; Li, Xiaoqin ^[1]; Hendrickson, Joshua R. ^[5];

^[2];

^[1]

Univ. of Texas, Austin, TX (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Air Force Research Lab. (AFRL), Wright-Patterson AFB, OH (United States); KBRwyle, Beavercreek, OH (United States)
Univ. of Texas, Austin, TX (United States); Princeton Univ., NJ (United States)
Air Force Research Lab. (AFRL), Wright-Patterson AFB, OH (United States)

A synthetic challenge in faceted metal oxide nanocrystals (NCs) is realizing tunable localized surface plasmon resonance (LSPR) near-field response in the infrared (IR). Cube-shaped nanoparticles of noble metals exhibit LSPR spectral tunability limited to visible spectral range. In this work, we describe the colloidal synthesis of fluorine, tin codoped indium oxide (F,Sn:In₂O₃) NC cubes with tunable IR range LSPR for around 10 nm particle sizes. Free carrier concentration is tuned through controlled Sn dopant incorporation, where Sn is an aliovalent n-type dopant in the In₂O₃ lattice. F shapes the NC morphology into cubes by functioning as a surfactant on the {100} crystallographic facets. Cube shaped F,Sn:In₂O₃ NCs exhibit narrow, shape-dependent multimodal LSPR due to corner, edge, and face centered modes. Monolayer NC arrays are fabricated through a liquid-air interface assembly, further demonstrating tunable LSPR response as NC film nanocavities that can heighten near-field enhancement (NFE). The tunable F,Sn:In₂O₃ NC near-field is coupled with PbS quantum dots, via the Purcell effect. The detuning frequency between the nanocavity and exciton is varied, resulting in IR near-field dependent enhanced exciton lifetime decay. LSPR near-field tunability is directly visualized through IR range scanning transmission electron microscopy-electron energy loss spectroscopy (STEM-EELS). STEM-EELS mapping of the spatially confined near-field in the F,Sn:In₂O₃ NC array interparticle gap demonstrates elevated NFE tunability in the arrays.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: Fulbright Program; National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); Welch Foundation

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1720250

Journal Information:: Journal of Chemical Physics, Journal Name: Journal of Chemical Physics Journal Issue: 1 Vol. 152; ISSN 0021-9606

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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