Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles

Diao, Jiecheng; Shi, Xiaowen; Assefa, Tadesse A.; Wu, Longlong; Suzana, Ana F.; Nunes, Daniel S.; Batey, Darren; Cipiccia, Silvia; Rau, Christoph; Harder, Ross J.; Cha, Wonsuk; Robinson, Ian K.

doi:10.1103/physrevmaterials.4.106001

Title: Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles

Abstract

In this work, ferroelastic domain walls inside BaTiO3 (BTO) tetragonal nanocrystals are distinguished by Bragg peak position and studied with Bragg coherent x-ray diffraction imaging (BCDI). Convergence-related features of the BCDI method for strongly phased objects are reported. A ferroelastic domain wall inside a BTO crystal has been tracked and imaged across the tetragonal-cubic phase transition and proves to be reversible. The linear relationship of relative displacement between two twin domains with temperature is measured and shows a different slope for heating and cooling, while the tetragonality reproduces well over temperature changes in both directions. An edge dislocation is also observed and found to annihilate when heating the crystal close to the phase transition temperature.

Authors:

^[1]; Shi, Xiaowen ^[2];

^[3];

^[3]; Nunes, Daniel S. ^[1]; Batey, Darren ^[2]; Cipiccia, Silvia ^[2]; Rau, Christoph ^[2];

^[4];

^[5]

Univ. College London (United Kingdom). London Centre for Nanotechnology
Science and Technology Facilities Council (STFC), Oxford (United Kingdom). Diamond Light Source, Ltd.
Brookhaven National Lab. (BNL), Upton, NY (United States)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Univ. College London (United Kingdom). London Centre for Nanotechnology; Brookhaven National Lab. (BNL), Upton, NY (United States)

Publication Date:: 2020-10-27

Research Org.:: Brookhaven National Lab. (BNL), Upton, NY (United States); Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES); National Science Foundation (NSF); China Scholarship Council (CSC)

OSTI Identifier:: 1661637

Alternate Identifier(s):: OSTI ID: 1779070

Report Number(s):: BNL-216378-2020-JAAM
Journal ID: ISSN 2475-9953; TRN: US2203607

Grant/Contract Number:: SC0012704; EP/I022562/1; AC02-06CH11357; DMR-9724294

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review Materials

Additional Journal Information:: Journal Volume: 4; Journal Issue: 10; Journal ID: ISSN 2475-9953

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY

Citation Formats


                    Diao, Jiecheng, Shi, Xiaowen, Assefa, Tadesse A., Wu, Longlong, Suzana, Ana F., Nunes, Daniel S., Batey, Darren, Cipiccia, Silvia, Rau, Christoph, Harder, Ross J., Cha, Wonsuk, and Robinson, Ian K.. Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles.  United States: N. p., 2020. 
Web.  doi:10.1103/physrevmaterials.4.106001.

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                    Diao, Jiecheng, Shi, Xiaowen, Assefa, Tadesse A., Wu, Longlong, Suzana, Ana F., Nunes, Daniel S., Batey, Darren, Cipiccia, Silvia, Rau, Christoph, Harder, Ross J., Cha, Wonsuk, & Robinson, Ian K.. Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles.  United States.  https://doi.org/10.1103/physrevmaterials.4.106001

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                    Diao, Jiecheng, Shi, Xiaowen, Assefa, Tadesse A., Wu, Longlong, Suzana, Ana F., Nunes, Daniel S., Batey, Darren, Cipiccia, Silvia, Rau, Christoph, Harder, Ross J., Cha, Wonsuk, and Robinson, Ian K.. Tue .  
"Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles".  United States.  https://doi.org/10.1103/physrevmaterials.4.106001.  https://www.osti.gov/servlets/purl/1661637.

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@article{osti_1661637,

  title        = {Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles},

  author       = {Diao, Jiecheng and Shi, Xiaowen and Assefa, Tadesse A. and Wu, Longlong and Suzana, Ana F. and Nunes, Daniel S. and Batey, Darren and Cipiccia, Silvia and Rau, Christoph and Harder, Ross J. and Cha, Wonsuk and Robinson, Ian K.},

  abstractNote = {In this work, ferroelastic domain walls inside BaTiO3 (BTO) tetragonal nanocrystals are distinguished by Bragg peak position and studied with Bragg coherent x-ray diffraction imaging (BCDI). Convergence-related features of the BCDI method for strongly phased objects are reported. A ferroelastic domain wall inside a BTO crystal has been tracked and imaged across the tetragonal-cubic phase transition and proves to be reversible. The linear relationship of relative displacement between two twin domains with temperature is measured and shows a different slope for heating and cooling, while the tetragonality reproduces well over temperature changes in both directions. An edge dislocation is also observed and found to annihilate when heating the crystal close to the phase transition temperature.},

  doi          = {10.1103/physrevmaterials.4.106001},

  journal      = {Physical Review Materials},

  number       = 10,

  volume       = 4,

  place        = {United States},

  year         = {2020},

  month        = {10}

}

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Title: Evolution of ferroelastic domain walls during phase transitions in barium titanate nanoparticles

Abstract

Citation Formats

An algorithm for Bragg coherent x-ray diffractive imaging of highly strained nanocrystals journal, January 2020

Inversion Domain Boundaries in GaN Wires Revealed by Coherent Bragg Imaging journal, September 2015

Tetragonal–cubic phase transition in BaTiO3 probed by resonant X-ray emission spectroscopy journal, April 2011

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New modalities of strain-control of ferroelectric thin films journal, May 2016

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The application of nanocrystalline BaTiO3-composite films as CO2-sensing layers journal, September 1999

Topological defect dynamics in operando battery nanoparticles journal, June 2015

Ferroelectricity at the Nanoscale: Local Polarization in Oxide Thin Films and Heterostructures journal, January 2004

Three-dimensional imaging of vortex structure in a ferroelectric nanoparticle driven by an electric field journal, August 2017

Development of an apparatus for Bragg coherent X-ray diffraction imaging, and its application to the three dimensional imaging of BaTiO 3 nano-crystals journal, August 2019

Ferroelectric Phase Transition in Individual Single-Crystalline BaTiO 3 Nanowires journal, April 2006

Coexistence of the Phonon and Relaxation Soft Modes in the Terahertz Dielectric Response of Tetragonal BaTiO 3 journal, October 2008

Interface Physics in Complex Oxide Heterostructures journal, March 2011

Phase retrieval algorithms: a comparison journal, January 1982

Character of Order-Disorder and Displacive Components in Barium Titanate journal, July 2004

Coherent X-Ray Diffraction Imaging and Characterization of Strain in Silicon-on-Insulator Nanostructures journal, June 2014

Scaling behavior of low-temperature orthorhombic domains in the prototypical high-temperature superconductor La 1.875 Ba 0.125 CuO 4 journal, February 2020

Domain wall nanoelectronics journal, February 2012

Recent Progress on BaTiO3-Based Piezoelectric Ceramics for Actuator Applications journal, July 2017

Scaling of domain periodicity with thickness measured in Ba Ti O 3 single crystal lamellae and comparison with other ferroics journal, July 2006

Ferroelectricity, Domain Structure, and Phase Transitions of Barium Titanate journal, July 1950

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Domain Bundle Boundaries in Single Crystal BaTiO 3 Lamellae: Searching for Naturally Forming Dipole Flux-Closure/Quadrupole Chains journal, October 2010

Crystal Structure and the Paraelectric-to-Ferroelectric Phase Transition of Nanoscale BaTiO 3 journal, June 2008

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An algorithm for Bragg coherent x-ray diffractive imaging of highly strained nanocrystals
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Inversion Domain Boundaries in GaN Wires Revealed by Coherent Bragg Imaging
journal, September 2015

Tetragonal–cubic phase transition in BaTiO3 probed by resonant X-ray emission spectroscopy
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Three-dimensional imaging of vortex structure in a ferroelectric nanoparticle driven by an electric field
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Development of an apparatus for Bragg coherent X-ray diffraction imaging, and its application to the three dimensional imaging of BaTiO ₃ nano-crystals
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Ferroelectric Phase Transition in Individual Single-Crystalline BaTiO ₃ Nanowires
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