Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography

Jiang, Zhang; Strzalka, Joseph W.; Walko, Donald A.; Wang, Jin

doi:10.1038/s41467-020-16980-5

Title: Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography

Abstract

Fluorescence from an excited atom propagates as an outgoing spherical wave until it is scattered by inhomogeneities or other atoms nearby. An anisotropic intensity pattern, known as the fluorescence hologram, is created when this scattered wave interferes with the freely propagating wave. X-ray fluorescence holography focuses on holograms generated from crystals and gives information about their local atomic structures. Likewise, a waveguide can also generate fluorescence holograms as a result of the establishment of X-ray standing waves. We therefrom introduce the concept of X-ray waveguide fluorescence holography, where a nanostructured thin film by itself is an optical waveguide thus turning this holographic technique into an in-situ and time-resolved imaging probe for nanostructures in the film. A model-free reconstruction method was developed based on the dynamical theory. The performance of X-ray waveguide fluorescence holography is experimentally compared to conventional forward scattering techniques for thin films such as reflectivity and grazing-incidence small

Authors:

;

; Walko, Donald A.; Wang, Jin

Publication Date:: Wed Jun 24 00:00:00 EDT 2020

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1634846

Alternate Identifier(s):: OSTI ID: 1647006; OSTI ID: 1656866

Grant/Contract Number:: AC02-06CH11357

Resource Type:: Published Article

Journal Name:: Nature Communications

Additional Journal Information:: Journal Name: Nature Communications Journal Volume: 11 Journal Issue: 1; Journal ID: ISSN 2041-1723

Publisher:: Nature Publishing Group

Country of Publication:: United Kingdom

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Jiang, Zhang, Strzalka, Joseph W., Walko, Donald A., and Wang, Jin. Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography.  United Kingdom: N. p., 2020. 
Web.  doi:10.1038/s41467-020-16980-5.

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                    Jiang, Zhang, Strzalka, Joseph W., Walko, Donald A., & Wang, Jin. Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography.  United Kingdom.  https://doi.org/10.1038/s41467-020-16980-5

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                    Jiang, Zhang, Strzalka, Joseph W., Walko, Donald A., and Wang, Jin. Wed .  
"Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography".  United Kingdom.  https://doi.org/10.1038/s41467-020-16980-5.

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@article{osti_1634846,

  title        = {Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography},

  author       = {Jiang, Zhang and Strzalka, Joseph W. and Walko, Donald A. and Wang, Jin},

  abstractNote = {Fluorescence from an excited atom propagates as an outgoing spherical wave until it is scattered by inhomogeneities or other atoms nearby. An anisotropic intensity pattern, known as the fluorescence hologram, is created when this scattered wave interferes with the freely propagating wave. X-ray fluorescence holography focuses on holograms generated from crystals and gives information about their local atomic structures. Likewise, a waveguide can also generate fluorescence holograms as a result of the establishment of X-ray standing waves. We therefrom introduce the concept of X-ray waveguide fluorescence holography, where a nanostructured thin film by itself is an optical waveguide thus turning this holographic technique into an in-situ and time-resolved imaging probe for nanostructures in the film. A model-free reconstruction method was developed based on the dynamical theory. The performance of X-ray waveguide fluorescence holography is experimentally compared to conventional forward scattering techniques for thin films such as reflectivity and grazing-incidence small},

  doi          = {10.1038/s41467-020-16980-5},

  journal      = {Nature Communications},

  number       = 1,

  volume       = 11,

  place        = {United Kingdom},

  year         = {Wed Jun 24 00:00:00 EDT 2020},

  month        = {Wed Jun 24 00:00:00 EDT 2020}

}

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Fig. 1: Schematics of X-ray fluorescence holography (XFH) operation modes. a In the normal XFH mode¹, an emitting atom (i.e. emitter) gives out a spherically outgoing X-ray fluorescence wave. An object wave is formed when this outgoing wave is scattered by a nearby atom (i.e. scatterer) and then interferes withmore »

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Similar Records

Title: Reconstruction of evolving nanostructures in ultrathin films with X-ray waveguide fluorescence holography

Abstract

Citation Formats

Figures / Tables:

Advanced grazing-incidence techniques for modern soft-matter materials analysis journal, January 2015

Glancing-incidence and glancing-takeoff x-ray fluorescence analysis of Ni-GaAs interface reactions journal, March 2000

Morphologies of discontinuous gold films on amorphous polymer substrates journal, November 1992

Resonance-enhanced x-rays in thin films: a structure probe for membranes and surface layers journal, October 1992

Experimental phase determination of the structure factor from Kossel line profile journal, March 2016

Enhancement of X-ray fluorescence intensity from an ultra-thin sandwiched layer at grazing-emission angles journal, December 1999

Model-independent determination of the surface scattering-length-density profile from specular reflectivity data journal, April 1992

Element sensitive reconstruction of nanostructured surfaces with finite elements and grazing incidence soft X-ray fluorescence journal, January 2018

Laboratory Setup for Scanning-Free Grazing Emission X-ray Fluorescence journal, January 2017

X-ray standing waves at a reflecting mirror surface journal, March 1989

Depth-Resolved X-ray Absorption Spectroscopy by Means of Grazing Emission X-ray Fluorescence journal, July 2015

Surface Studies of Solids by Total Reflection of X-Rays journal, July 1954

Combined evaluation of grazing incidence X-ray fluorescence and X-ray reflectivity data for improved profiling of ultra-shallow depth distributions journal, September 2014

Structural studies of membranes and surface layers up to 1,000 Å thick using X-ray standing waves journal, December 1991

Photon cross sections from 1 keV to 100 MeV for elements Z=1 to Z=100 journal, June 1970

Removing multiple scattering and twin images from holographic images journal, November 1991

Scanning-free grazing emission x-ray fluorescence by means of an angular dispersive arrangement with a two-dimensional position-sensitive area detector journal, December 2013

Dynamics of Polymer/Metal Nanocomposite Films at Short Times As Studied by X-ray Standing Waves journal, November 2004

Characterization of ultra-shallow aluminum implants in silicon by grazing incidence and grazing emission X-ray fluorescence spectroscopy journal, January 2012

Fluorescent X-ray interference from a protein monolayer journal, January 1994

X-ray and neutron scattering from rough surfaces journal, August 1988

X-ray divergent-beam (Kossel) technique: A review journal, March 2011

X-ray fluorescence holography: Going beyond the diffraction limit journal, January 2003

Perturbation to the resonance modes by gold nanoparticles in a thin-film-based x-ray waveguide journal, April 2006

X-ray standing waves: a molecular yardstick for biological membranes journal, September 1988

Depth profiling of low energy ion implantations in Si and Ge by means of micro-focused grazing emission X-ray fluorescence and grazing incidence X-ray fluorescence journal, January 2015

Multiple-Energy X-Ray Holography: Atomic Images of Hematite (F e 2 O 3 ) journal, April 1996

X-ray holography with atomic resolution journal, March 1996

Waveguide-enhanced grazing-incidence small-angle x-ray scattering of buried nanostructures in thin films journal, August 2011

Three-dimensional atomic-arrangement reconstruction from an Auger-electron hologram journal, February 2007

X-Ray Evanescent-Wave Absorption and Emission journal, January 1983

Real-Time Evolution of the Distribution of Nanoparticles in an Ultrathin-Polymer-Film-Based Waveguide journal, April 2005

X-Ray Scattering from Soft-Matter Thin Films book, January 1999

Application of spline functions to the correction of resolution errors in small-angle scattering journal, June 1971

X-ray fluorescence induced by standing waves in the grazing-incidence and grazing-exit modes: study of the Mg–Co–Zr system journal, September 2015

Kossel diffraction in perfect crystals: X-ray standing waves in reverse journal, March 1995

The interference theory of ideal paracrystals journal, September 1952

Diffuse-double layer at a membrane-aqueous interface measured with x-ray standing waves journal, April 1990

A new approach for three-dimensional atomic-image reconstruction from a single-energy photoelectron hologram journal, January 2004

Observation of ultralow-level Al impurities on a silicon surface by high-resolution grazing emission x-ray fluorescence excited by synchrotron radiation journal, September 2009

Advanced grazing-incidence techniques for modern soft-matter materials analysis
journal, January 2015

Glancing-incidence and glancing-takeoff x-ray fluorescence analysis of Ni-GaAs interface reactions
journal, March 2000

Morphologies of discontinuous gold films on amorphous polymer substrates
journal, November 1992

Resonance-enhanced x-rays in thin films: a structure probe for membranes and surface layers
journal, October 1992

Experimental phase determination of the structure factor from Kossel line profile
journal, March 2016

Enhancement of X-ray fluorescence intensity from an ultra-thin sandwiched layer at grazing-emission angles
journal, December 1999

Model-independent determination of the surface scattering-length-density profile from specular reflectivity data
journal, April 1992

Element sensitive reconstruction of nanostructured surfaces with finite elements and grazing incidence soft X-ray fluorescence
journal, January 2018

Laboratory Setup for Scanning-Free Grazing Emission X-ray Fluorescence
journal, January 2017

X-ray standing waves at a reflecting mirror surface
journal, March 1989

Depth-Resolved X-ray Absorption Spectroscopy by Means of Grazing Emission X-ray Fluorescence
journal, July 2015

Surface Studies of Solids by Total Reflection of X-Rays
journal, July 1954

Combined evaluation of grazing incidence X-ray fluorescence and X-ray reflectivity data for improved profiling of ultra-shallow depth distributions
journal, September 2014

Structural studies of membranes and surface layers up to 1,000 Å thick using X-ray standing waves
journal, December 1991

Photon cross sections from 1 keV to 100 MeV for elements Z=1 to Z=100
journal, June 1970

Removing multiple scattering and twin images from holographic images
journal, November 1991

Scanning-free grazing emission x-ray fluorescence by means of an angular dispersive arrangement with a two-dimensional position-sensitive area detector
journal, December 2013

Dynamics of Polymer/Metal Nanocomposite Films at Short Times As Studied by X-ray Standing Waves
journal, November 2004

Characterization of ultra-shallow aluminum implants in silicon by grazing incidence and grazing emission X-ray fluorescence spectroscopy
journal, January 2012

Fluorescent X-ray interference from a protein monolayer
journal, January 1994

X-ray and neutron scattering from rough surfaces
journal, August 1988

X-ray divergent-beam (Kossel) technique: A review
journal, March 2011

X-ray fluorescence holography: Going beyond the diffraction limit
journal, January 2003

Perturbation to the resonance modes by gold nanoparticles in a thin-film-based x-ray waveguide
journal, April 2006

X-ray standing waves: a molecular yardstick for biological membranes
journal, September 1988

Depth profiling of low energy ion implantations in Si and Ge by means of micro-focused grazing emission X-ray fluorescence and grazing incidence X-ray fluorescence
journal, January 2015

Multiple-Energy X-Ray Holography: Atomic Images of Hematite (F $e_{2}$ $O_{3}$ )
journal, April 1996

X-ray holography with atomic resolution
journal, March 1996

Waveguide-enhanced grazing-incidence small-angle x-ray scattering of buried nanostructures in thin films
journal, August 2011

Three-dimensional atomic-arrangement reconstruction from an Auger-electron hologram
journal, February 2007

X-Ray Evanescent-Wave Absorption and Emission
journal, January 1983

Real-Time Evolution of the Distribution of Nanoparticles in an Ultrathin-Polymer-Film-Based Waveguide
journal, April 2005

X-Ray Scattering from Soft-Matter Thin Films
book, January 1999

Application of spline functions to the correction of resolution errors in small-angle scattering
journal, June 1971

X-ray fluorescence induced by standing waves in the grazing-incidence and grazing-exit modes: study of the Mg–Co–Zr system
journal, September 2015

Kossel diffraction in perfect crystals: X-ray standing waves in reverse
journal, March 1995

The interference theory of ideal paracrystals
journal, September 1952

Diffuse-double layer at a membrane-aqueous interface measured with x-ray standing waves
journal, April 1990

A new approach for three-dimensional atomic-image reconstruction from a single-energy photoelectron hologram
journal, January 2004

Observation of ultralow-level Al impurities on a silicon surface by high-resolution grazing emission x-ray fluorescence excited by synchrotron radiation
journal, September 2009