Impact of Drying on Meso- and Nanoscale Structures of Citrus Fiber: A Study by SFG, ATR-IR, XRD, and DLS

Makarem, Mohamadamin; Kim, Hyojung; Emami, Parinaz; Melendez, Jesus; Steinbach, Adam; Lipkie, Tristan; Deleris, Isabelle; Desmet, Christina; Wallecan, Jöel; Kim, Seong H.

doi:10.1021/acs.iecr.9b06194

Title: Impact of Drying on Meso- and Nanoscale Structures of Citrus Fiber: A Study by SFG, ATR-IR, XRD, and DLS

Journal Article · 27 January 2020 · Industrial and Engineering Chemistry Research

DOI: https://doi.org/10.1021/acs.iecr.9b06194 · OSTI ID:1634826

^[1]; Kim, Hyojung ^[2]; Emami, Parinaz ^[2]; Melendez, Jesus ^[2]; Steinbach, Adam ^[3]; Lipkie, Tristan ^[3]; Deleris, Isabelle ^[3]; Desmet, Christina ^[3]; Wallecan, Jöel ^[3];

^[2]

Pennsylvania State Univ., University Park, PA (United States); The Pennsylvania State University
Pennsylvania State Univ., University Park, PA (United States)
Cargill Research and Development, Plymouth, MN (United States)

Citrus fibers are a sidestream of the pectin extraction process from citrus peel. This sidestream can be converted into a functional ingredient through a shear-induced homogenization process. One technical challenge with this material is that dehydration and subsequent rehydration result in reduction of viscosity compared to the original product. In this study, various drying methods were compared with never-dried fibers to investigate the structural changes underlying the viscosity loss. Infrared and X-ray diffraction analyses confirmed no changes in chemical composition and crystalline structure of citrus fibers. Here, the dynamic light scattering and sum frequency generation analyses of citrus fiber suspension showed that the rehydration process could not fully disperse aggregated fibers, which appears to be the main cause for the viscosity loss.

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Research Organization:: Energy Frontier Research Centers (EFRC) (United States). Center for Lignocellulose Structure and Formation (CLSF); Pennsylvania State Univ., University Park, PA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

Grant/Contract Number:: SC0001090

OSTI ID:: 1634826

Journal Information:: Industrial and Engineering Chemistry Research, Journal Name: Industrial and Engineering Chemistry Research Journal Issue: 7 Vol. 59; ISSN 0888-5885

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

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Title: Impact of Drying on Meso- and Nanoscale Structures of Citrus Fiber: A Study by SFG, ATR-IR, XRD, and DLS

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