Radiation furnace for synchrotron dark-field x-ray microscopy experiments
Abstract
We present a multi-purpose radiation furnace designed for x-ray experiments at synchrotrons. The furnace is optimized specifically for dark-field x-ray microscopy (DFXM) of crystalline materials at beamline ID06 of the European Synchrotron Radiation Facility. The furnace can reach temperatures above 1200 °C with a thermal stability better than 10 °C, with heating and cooling rates up to 30 K/s. The non-contact heating design enables samples to be heated either in air or in a controlled atmosphere contained within a capillary tube. The temperature was calibrated via the thermal expansion of an α-iron grain. Temperature profiles in the y and z axes were measured by scanning a thermocouple through the focal spot of the radiation furnace. In the current configuration of the beamline, this furnace can be used for DFXM, near-field x-ray topography, bright-field x-ray nanotomography, high-resolution reciprocal space mapping, and limited powder diffraction experiments. As a first application, we present a DFXM case study on isothermal heating of a commercially pure single crystal of aluminum.
- Publication Date:
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1633120
- Grant/Contract Number:
- AC52-07NA27344
- Resource Type:
- Publisher's Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Name: Review of Scientific Instruments Journal Volume: 91 Journal Issue: 6; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics
- Country of Publication:
- United States
- Language:
- English
Citation Formats
Yildirim, C., Vitoux, H., Dresselhaus-Marais, L. E., Steinmann, R., Watier, Y., Cook, P. K., Kutsal, M., and Detlefs, C. Radiation furnace for synchrotron dark-field x-ray microscopy experiments. United States: N. p., 2020.
Web. doi:10.1063/1.5141139.
Yildirim, C., Vitoux, H., Dresselhaus-Marais, L. E., Steinmann, R., Watier, Y., Cook, P. K., Kutsal, M., & Detlefs, C. Radiation furnace for synchrotron dark-field x-ray microscopy experiments. United States. https://doi.org/10.1063/1.5141139
Yildirim, C., Vitoux, H., Dresselhaus-Marais, L. E., Steinmann, R., Watier, Y., Cook, P. K., Kutsal, M., and Detlefs, C. Fri .
"Radiation furnace for synchrotron dark-field x-ray microscopy experiments". United States. https://doi.org/10.1063/1.5141139.
@article{osti_1633120,
title = {Radiation furnace for synchrotron dark-field x-ray microscopy experiments},
author = {Yildirim, C. and Vitoux, H. and Dresselhaus-Marais, L. E. and Steinmann, R. and Watier, Y. and Cook, P. K. and Kutsal, M. and Detlefs, C.},
abstractNote = {We present a multi-purpose radiation furnace designed for x-ray experiments at synchrotrons. The furnace is optimized specifically for dark-field x-ray microscopy (DFXM) of crystalline materials at beamline ID06 of the European Synchrotron Radiation Facility. The furnace can reach temperatures above 1200 °C with a thermal stability better than 10 °C, with heating and cooling rates up to 30 K/s. The non-contact heating design enables samples to be heated either in air or in a controlled atmosphere contained within a capillary tube. The temperature was calibrated via the thermal expansion of an α-iron grain. Temperature profiles in the y and z axes were measured by scanning a thermocouple through the focal spot of the radiation furnace. In the current configuration of the beamline, this furnace can be used for DFXM, near-field x-ray topography, bright-field x-ray nanotomography, high-resolution reciprocal space mapping, and limited powder diffraction experiments. As a first application, we present a DFXM case study on isothermal heating of a commercially pure single crystal of aluminum.},
doi = {10.1063/1.5141139},
journal = {Review of Scientific Instruments},
number = 6,
volume = 91,
place = {United States},
year = {Fri Jun 12 00:00:00 EDT 2020},
month = {Fri Jun 12 00:00:00 EDT 2020}
}
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