Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication
Abstract
Neutron scattering is one of the most useful methods of studying the structure of matter, with applications to biomedical, structural, magnetic and energy-related materials. Neutron-scattering instruments are installed around research reactors or accelerator-based neutron sources, and neutron guides are critical components of these facilities. They are neutron-transport optical devices consisting of state-of-the-art mirrors often tens of meters long. Here we demonstrate a novel fabrication method of all-metallic neutron guides and axisymmetric mirrors by electroplating from precision mandrels. The process allows for the fabrication of single-piece all-metal guides of prismatic and axisymmetric shapes. We also demonstrate supermirror guides and axisymmetric focusing supermirrors produced with the same technology. We present the fabrication and tests of the multilayer-coated replicated guides and optic and show that the mandrel is reproduced with high fidelity and reliability. Such supermirror optics will provide game-changing improvements in neutron techniques.
- Authors:
-
- Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)
- Harvard-Smithsonian Center for Astrophysics, Cambridge, MA (United States)
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
- Dawn Research, Huntsville, AL (United States)
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Dawn Research, Huntsville, AL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- Contributing Org.:
- Oak Ridge National Laboratory's Spallation Neutron Source
- OSTI Identifier:
- 1630490
- Alternate Identifier(s):
- OSTI ID: 1774063
- Grant/Contract Number:
- AC05-00OR22725; SC0011507; SC0017098
- Resource Type:
- Accepted Manuscript
- Journal Name:
- MRS Advances
- Additional Journal Information:
- Journal Volume: 5; Journal Issue: 29-30; Journal ID: ISSN 2059-8521
- Publisher:
- Materials Research Society (MRS)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 47 OTHER INSTRUMENTATION
Citation Formats
Khaykovich, Boris, Romaine, S., Ames, A., Bruni, R., Ambaye, Haile Arena, Glavic, Arthur, Lauter, Valeria, and Engelhaupt, D. Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication. United States: N. p., 2020.
Web. doi:10.1557/adv.2020.142.
Khaykovich, Boris, Romaine, S., Ames, A., Bruni, R., Ambaye, Haile Arena, Glavic, Arthur, Lauter, Valeria, & Engelhaupt, D. Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication. United States. https://doi.org/10.1557/adv.2020.142
Khaykovich, Boris, Romaine, S., Ames, A., Bruni, R., Ambaye, Haile Arena, Glavic, Arthur, Lauter, Valeria, and Engelhaupt, D. Sun .
"Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication". United States. https://doi.org/10.1557/adv.2020.142. https://www.osti.gov/servlets/purl/1630490.
@article{osti_1630490,
title = {Fabrication and testing of high-performance all-metal neutron guides and axisymmetric mirrors by electrochemical replication},
author = {Khaykovich, Boris and Romaine, S. and Ames, A. and Bruni, R. and Ambaye, Haile Arena and Glavic, Arthur and Lauter, Valeria and Engelhaupt, D.},
abstractNote = {Neutron scattering is one of the most useful methods of studying the structure of matter, with applications to biomedical, structural, magnetic and energy-related materials. Neutron-scattering instruments are installed around research reactors or accelerator-based neutron sources, and neutron guides are critical components of these facilities. They are neutron-transport optical devices consisting of state-of-the-art mirrors often tens of meters long. Here we demonstrate a novel fabrication method of all-metallic neutron guides and axisymmetric mirrors by electroplating from precision mandrels. The process allows for the fabrication of single-piece all-metal guides of prismatic and axisymmetric shapes. We also demonstrate supermirror guides and axisymmetric focusing supermirrors produced with the same technology. We present the fabrication and tests of the multilayer-coated replicated guides and optic and show that the mandrel is reproduced with high fidelity and reliability. Such supermirror optics will provide game-changing improvements in neutron techniques.},
doi = {10.1557/adv.2020.142},
journal = {MRS Advances},
number = 29-30,
volume = 5,
place = {United States},
year = {Sun Sep 27 00:00:00 EDT 2020},
month = {Sun Sep 27 00:00:00 EDT 2020}
}
Works referenced in this record:
The use of neutron optical devices on beam-hole experiments on beam-hole experiments
journal, July 1963
- Maier-Leibnitz, H.; Springer, T.
- Journal of Nuclear Energy. Parts A/B. Reactor Science and Technology, Vol. 17, Issue 4-5
New concepts for neutron instrumentation
journal, February 2008
- Böni, P.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 586, Issue 1
High Performance Supermirrors on Metallic Substrates
journal, November 2010
- Schanzer, C.; Böni, P.; Schneider, M.
- Journal of Physics: Conference Series, Vol. 251
Development of Wolter I x-ray optics by diamond turning and electrochemical replication
journal, October 1995
- Fawcett, Steven C.; Engelhaupt, Darell
- Precision Engineering, Vol. 17, Issue 4
From x-ray telescopes to neutron scattering: Using axisymmetric mirrors to focus a neutron beam
journal, March 2011
- Khaykovich, B.; Gubarev, M. V.; Bagdasarova, Y.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 631, Issue 1, p. 98-104
Demonstration of achromatic cold-neutron microscope utilizing axisymmetric focusing mirrors
journal, May 2013
- Liu, D.; Hussey, D.; Gubarev, M. V.
- Applied Physics Letters, Vol. 102, Issue 18
Response to “Comment on ‘Demonstration of achromatic cold-neutron microscope utilizing axisymmetric focusing mirrors’” [Appl. Phys. Lett. 103, 236101 (2013)]
journal, December 2013
- Liu, D.; Hussey, D. S.; Gubarev, M. V.
- Applied Physics Letters, Vol. 103, Issue 23
High-resolution neutron depolarization microscopy of the ferromagnetic transitions in Ni3Al and HgCr2Se4 under pressure
journal, April 2019
- Jorba, Pau; Schulz, Michael; Hussey, Daniel S.
- Journal of Magnetism and Magnetic Materials, Vol. 475
Demonstration of Focusing Wolter Mirrors for Neutron Phase and Magnetic Imaging
journal, March 2018
- Hussey, Daniel; Wen, Han; Wu, Huarui
- Journal of Imaging, Vol. 4, Issue 3
Wolter Mirrors for Neutron Imaging
journal, January 2017
- Wu, Huarui; Khaykovich, Boris; Wang, Xuewu
- Physics Procedia, Vol. 88
Axisymmetric grazing-incidence focusing optics for small-angle neutron scattering
journal, September 2012
- Liu, D.; Gubarev, M. V.; Resta, G.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 686
Demonstration of a novel focusing small-angle neutron scattering instrument equipped with axisymmetric mirrors
journal, September 2013
- Liu, Dazhi; Khaykovich, Boris; Gubarev, Mikhail V.
- Nature Communications, Vol. 4, Issue 1
Mandrel replication for hard x-ray optics using titanium nitride
conference, August 2009
- Romaine, S.; Boike, J.; Bruni, R.
- SPIE Optical Engineering + Applications, SPIE Proceedings
Improved release coatings for electroformed x-ray optics
conference, September 2011
- Romaine, S.; Boike, J.; Bruni, R.
- SPIE Optical Engineering + Applications, SPIE Proceedings
Development of soft and hard x-ray optics for astronomy
conference, November 2000
- Citterio, Oberto; Conconi, Paolo; Ghigo, Mauro
- International Symposium on Optical Science and Technology, SPIE Proceedings
New alloys for electroformed replicated x-ray optics
conference, November 2000
- Engelhaupt, Darell E.; Ramsey, Brian D.; O'Dell, Stephen L.
- International Symposium on Optical Science and Technology, SPIE Proceedings
Development of hard x-ray optics at MSFC
conference, March 2003
- Ramsey, Brian D.; Elsner, Ronald F.; Engelhaupt, Darell E.
- Astronomical Telescopes and Instrumentation, SPIE Proceedings
Discrete thin-film multilayer design for X-ray and neutron supermirrors
journal, February 1989
- Hayter, J. B.; Mook, H. A.
- Journal of Applied Crystallography, Vol. 22, Issue 1
Highlights from the magnetism reflectometer at the SNS
journal, September 2009
- Lauter, Valeria; Ambaye, Hailemariam; Goyette, Richard
- Physica B: Condensed Matter, Vol. 404, Issue 17, p. 2543-2546
IMD—Software for modeling the optical properties of multilayer films
journal, January 1998
- Windt, David L.
- Computers in Physics, Vol. 12, Issue 4
Techniques de diffusion des neutrons en incidence rasante pour les nanosciences
journal, January 2007
- Lauter-Pasyuk, V.
- École thématique de la Société Française de la Neutronique, Vol. 12
Anomalous Surface Reflection of X Rays
journal, September 1963
- Yoneda, Y.
- Physical Review, Vol. 131, Issue 5
A new generation of neutron-focusing optics
journal, February 2014
- Khaykovich, Boris; Liu, Dazhi; Moncton, David E.
- SPIE Newsroom