skip to main content
DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor

Abstract

Liquid-phase synthesis of Ni 2 P in different flow types.

Authors:
ORCiD logo [1];  [1];  [1];  [1];  [1];  [1]
  1. Fujian Engineering Research Center of Advanced Manufacturing Technology for Specialty Chemicals, & Fujian Key Laboratory of Advanced Manufacturing Technology for Specialty Chemicals, College of Chemical Engineering, Fuzhou University, Fuzhou
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1630353
Grant/Contract Number:  
FG02-963414669
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Reaction Chemistry & Engineering
Additional Journal Information:
Journal Name: Reaction Chemistry & Engineering Journal Volume: 5 Journal Issue: 6; Journal ID: ISSN 2058-9883
Publisher:
Royal Society of Chemistry (RSC)
Country of Publication:
United Kingdom
Language:
English

Citation Formats

Zheng, Huidong, Li, Donglin, Chen, Jingjing, Liu, Jie, Yan, Zuoyi, and Oyama, S. Ted. Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor. United Kingdom: N. p., 2020. Web. doi:10.1039/D0RE00010H.
Zheng, Huidong, Li, Donglin, Chen, Jingjing, Liu, Jie, Yan, Zuoyi, & Oyama, S. Ted. Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor. United Kingdom. doi:https://doi.org/10.1039/D0RE00010H
Zheng, Huidong, Li, Donglin, Chen, Jingjing, Liu, Jie, Yan, Zuoyi, and Oyama, S. Ted. Tue . "Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor". United Kingdom. doi:https://doi.org/10.1039/D0RE00010H.
@article{osti_1630353,
title = {Continuous liquid-phase synthesis of nickel phosphide nanoparticles in a helically coiled tube reactor},
author = {Zheng, Huidong and Li, Donglin and Chen, Jingjing and Liu, Jie and Yan, Zuoyi and Oyama, S. Ted},
abstractNote = {Liquid-phase synthesis of Ni 2 P in different flow types.},
doi = {10.1039/D0RE00010H},
journal = {Reaction Chemistry & Engineering},
number = 6,
volume = 5,
place = {United Kingdom},
year = {2020},
month = {6}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
DOI: https://doi.org/10.1039/D0RE00010H

Save / Share:

Works referenced in this record:

Rational Design of Nickel Phosphide Hydrodesulfurization Catalysts: Controlling Particle Size and Preventing Sintering
journal, March 2013

  • Layan Savithra, Galbokka H.; Muthuswamy, Elayaraja; Bowker, Richard H.
  • Chemistry of Materials, Vol. 25, Issue 6
  • DOI: 10.1021/cm302680j

Magnetic properties of CoP alloys electrodeposited at room temperature
journal, April 2005


Heat-Transfer Performance of a Liquid−Liquid Microdispersed System
journal, December 2008

  • Wang, Kai; Lu, Yangcheng; Shao, Huawei
  • Industrial & Engineering Chemistry Research, Vol. 47, Issue 23
  • DOI: 10.1021/ie8005484

Microstructure evaluation and strengthening mechanism of Ni–P–W alloy coatings
journal, January 2004


A novel method for preparing an active nickel phosphide catalyst for HDS of dibenzothiophene
journal, April 2009

  • Cecilia, J. A.; Infantes-Molina, A.; Rodríguez-Castellón, E.
  • Journal of Catalysis, Vol. 263, Issue 1
  • DOI: 10.1016/j.jcat.2009.02.013

Formation mechanisms of Ni2P nanocrystals using XANES and EXAFS spectroscopy
journal, February 2011

  • Seo, Hye-Ryun; Cho, Kye-Sung; Lee, Yong-Kul
  • Materials Science and Engineering: B, Vol. 176, Issue 2
  • DOI: 10.1016/j.mseb.2010.10.013

A Facile Molecular Precursor Route to Metal Phosphide Nanoparticles and Their Evaluation as Hydrodeoxygenation Catalysts
journal, November 2015

  • Habas, Susan E.; Baddour, Frederick G.; Ruddy, Daniel A.
  • Chemistry of Materials, Vol. 27, Issue 22, p. 7580-7592
  • DOI: 10.1021/acs.chemmater.5b02140

Synthesis, characterization and properties of hollow nickel phosphide nanospheres
journal, September 2006


Studies of the synthesis of transition metal phosphides and their activity in the hydrodeoxygenation of a biofuel model compound
journal, October 2012


Toward continuous and scalable production of colloidal nanocrystals by switching from batch to droplet reactors
journal, January 2015

  • Niu, Guangda; Ruditskiy, Aleksey; Vara, Madeline
  • Chemical Society Reviews, Vol. 44, Issue 16
  • DOI: 10.1039/C5CS00049A

Segmented Flow Reactors for Nanocrystal Synthesis
journal, November 2012


Alternative synthesis of bulk and supported nickel phosphide from the thermal decomposition of hypophosphites
journal, April 2009


Solvent-controlled syntheses of Ni12P5 and Ni2P nanocrystals and photocatalytic property comparison
journal, December 2011

  • Mi, Kai; Ni, Yonghong; Hong, Jianming
  • Journal of Physics and Chemistry of Solids, Vol. 72, Issue 12
  • DOI: 10.1016/j.jpcs.2011.08.028

Mesomixing scale controlling and its effect on micromixing performance
journal, July 2007


Multi-step synthesis of nanoparticles performed on millisecond time scale in a microfluidic droplet-based system
journal, January 2004

  • Shestopalov, Ilya; Tice, Joshua D.; Ismagilov, Rustem F.
  • Lab on a Chip, Vol. 4, Issue 4
  • DOI: 10.1039/b403378g

Comparison of phosphide catalysts prepared by temperature-programmed reduction and liquid-phase methods in the hydrodeoxygenation of 2-methylfuran
journal, November 2017


Production of titania nanoparticles by using a new microreactor assembled with same axle dual pipe
journal, August 2004

  • Takagi, Michiya; Maki, Taisuke; Miyahara, Minoru
  • Chemical Engineering Journal, Vol. 101, Issue 1-3
  • DOI: 10.1016/j.cej.2003.11.011

The residence time distribution for ideal laminar flow in helical tube
journal, July 1971


A comparative study on the crystallization behavior of electroless NiP and NiCuP deposits
journal, December 2001


Controlled synthesis and characterization of nickel phosphide nanocrystal
journal, June 2007


A general approach to the synthesis of metal phosphide catalysts
journal, February 2014


Generalized Synthesis of Metal Phosphide Nanorods via Thermal Decomposition of Continuously Delivered Metal−Phosphine Complexes Using a Syringe Pump
journal, June 2005

  • Park, Jongnam; Koo, Bonil; Yoon, Ki Youl
  • Journal of the American Chemical Society, Vol. 127, Issue 23
  • DOI: 10.1021/ja0427496

Liquid–liquid two-phase mass transfer in the T-junction microchannels
journal, January 2007

  • Zhao, Yuchao; Chen, Guangwen; Yuan, Quan
  • AIChE Journal, Vol. 53, Issue 12
  • DOI: 10.1002/aic.11333

Two-Phase Flow in a Coiled Tube. Pressure Drop, Holdup, and Liquid Phase Axial Mixing
journal, January 1966

  • Rippel, G. R.; Eidt, C. M.; Jordan, H. B.
  • Industrial & Engineering Chemistry Process Design and Development, Vol. 5, Issue 1
  • DOI: 10.1021/i260017a007

Synthetic Levers Enabling Independent Control of Phase, Size, and Morphology in Nickel Phosphide Nanoparticles
journal, February 2011

  • Muthuswamy, Elayaraja; Savithra, Galbokka H. Layan; Brock, Stephanie L.
  • ACS Nano, Vol. 5, Issue 3, p. 2402-2411
  • DOI: 10.1021/nn1033357

Synthesis of transition-metal phosphides from oxidic precursors by reduction in hydrogen plasma
journal, June 2009


Active phase of a nickel phosphide (Ni2P) catalyst supported on KUSY zeolite for the hydrodesulfurization of 4,6-DMDBT
journal, April 2007


Synthesis, Characterization, and Hydrotreating Activity of Several Iron Group Transition Metal Phosphides
journal, June 2002

  • Wang, Xianqin; Clark, Paul; Oyama, S. Ted
  • Journal of Catalysis, Vol. 208, Issue 2
  • DOI: 10.1006/jcat.2002.3604

Gas–liquid and liquid–liquid mass transfer in microstructured reactors
journal, September 2011

  • Kashid, Madhvanand N.; Renken, Albert; Kiwi-Minsker, Lioubov
  • Chemical Engineering Science, Vol. 66, Issue 17
  • DOI: 10.1016/j.ces.2011.05.015

Developing a Millifluidic Platform for the Synthesis of Ultrasmall Nanoclusters: Ultrasmall Copper Nanoclusters as a Case Study
journal, February 2012


Controlled Design of Phase- and Size-Tunable Monodisperse Ni 2 P Nanoparticles in a Phosphonium-Based Ionic Liquid through Response Surface Methodology
journal, February 2019


Axial Dispersion and Heat Transfer in a Milli/Microstructured Coiled Flow Inverter for Narrow Residence Time Distribution at Laminar Flow
journal, April 2015

  • Kurt, Safa Kutup; Gelhausen, Marius Gerrit; Kockmann, Norbert
  • Chemical Engineering & Technology, Vol. 38, Issue 7
  • DOI: 10.1002/ceat.201400515

New synthesis method for nickel phosphide hydrotreating catalysts
journal, January 2005

  • Yang, Shaofeng; Prins, Roel
  • Chemical Communications, Issue 33
  • DOI: 10.1039/b507940c

Transport and reaction in microscale segmented gas–liquid flow
journal, January 2004

  • Günther, Axel; Khan, Saif A.; Thalmann, Martina
  • Lab Chip, Vol. 4, Issue 4
  • DOI: 10.1039/B403982C

Flow boiling heat transfer in two-phase micro-channel heat sinks––I. Experimental investigation and assessment of correlation methods
journal, July 2003


A mathematical model of a slurry reactor for the direct synthesis of hydrogen peroxide
journal, January 2019

  • Pizzetti, Fabio; Granata, Vittoria M. A.; Riva, Umberto
  • Reaction Chemistry & Engineering, Vol. 4, Issue 12
  • DOI: 10.1039/C9RE00309F

Formation of Hollow Ni 2 P Nanoparticles Based on the Nanoscale Kirkendall Effect
journal, January 2007

  • Chiang, Ray-Kuang; Chiang, Ray-Tung
  • Inorganic Chemistry, Vol. 46, Issue 2
  • DOI: 10.1021/ic061846s