Nanoscale imaging of the full strain tensor of specific dislocations extracted from a bulk sample

Hofmann, Felix; Phillips, Nicholas W.; Das, Suchandrima; Karamched, Phani; Hughes, Gareth M.; Douglas, James O.; Cha, Wonsuk; Liu, Wenjun

doi:10.1103/PhysRevMaterials.4.013801

Title: Nanoscale imaging of the full strain tensor of specific dislocations extracted from a bulk sample

Journal Article · 14 January 2020 · Physical Review Materials

DOI: https://doi.org/10.1103/PhysRevMaterials.4.013801 · OSTI ID:1616753

^[1];

^[1]; Das, Suchandrima ^[1]; Karamched, Phani ^[2]; Hughes, Gareth M. ^[2]; Douglas, James O. ^[2]; Cha, Wonsuk ^[3]; Liu, Wenjun ^[3]

Univ. of Oxford (United Kingdom). Dept. of Engineering Science
Univ. of Oxford (United Kingdom). Dept. of Materials
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Lattice defects play a key role in determining the properties of crystalline materials. Probing the three-dimensional (3D) lattice strains that govern their interactions remains a challenge. Bragg coherent diffraction imaging (BCDI) allows strain to be measured with nanoscale 3D resolution. However, it is currently limited to materials that form microcrystals. In this work, we introduce a technique that allows the manufacture of BCDI samples from bulk materials. Using tungsten as an example, we show that focused ion-beam machining can be used to extract, from macroscopic crystals, micron-sized BCDI samples containing specific preselected defects. To interpret the experimental data, we develop a displacement-gradient-based analysis for multireflection BCDI. This provides accurate recovery of the full lattice strain tensor from samples containing multiple dislocations. These capabilities open the door to BCDI as a microscopy tool for studying complex real-world materials.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: European Research Council (ERC); European Union - Horizon 2020 Research and Innovation Programme; Engineering and Physical Sciences Research Council (EPSRC); Leverhulme Trust; USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1616753

Journal Information:: Physical Review Materials, Vol. 4, Issue 1; ISSN 2475-9953

Publisher:: American Physical Society (APS)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 31 works

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