Spontaneous formation of nanoparticles on electrospun nanofibres

Radacsi, Norbert; Campos, Fernando Diaz; Chisholm, Calum R.  I.; Giapis, Konstantinos P.

doi:10.1038/s41467-018-07243-5

Title: Spontaneous formation of nanoparticles on electrospun nanofibres

Journal Article · 09 November 2018 · Nature Communications

DOI: https://doi.org/10.1038/s41467-018-07243-5 · OSTI ID:1613622

^[1]; Campos, Fernando Diaz ^[2]; Chisholm, Calum R. I. ^[2]; Giapis, Konstantinos P. ^[3]

California Institute of Technology (CalTech), Pasadena, CA (United States); Univ. of Edinburgh, Scotland (United Kingdom); DOE/OSTI
SAFCell, Inc., Pasadena, CA (United States)
California Institute of Technology (CalTech), Pasadena, CA (United States)

We report the spontaneous formation of nanoparticles on smooth nanofibres in a single-step electrospinning process, as an inexpensive and scalable method for producing high-surface-area composites. Layers of nanofibres, containing the proton conducting electrolyte, caesium dihydrogen phosphate, are deposited uniformly over large area substrates from clear solutions of the electrolyte mixed with polymers. Under certain conditions, the normally smooth nanofibres develop caesium dihydrogen phosphate nanoparticles in large numbers on their external surface. The nanoparticles appear to originate from the electrolyte within the fibres, which is transported to the outer surface after the fibres are deposited, as evidenced by cross-sectional imaging of the electrospun fibres. The presence of nanoparticles on the fibre surface yields composites with increased surface area of exposed electrolyte, which ultimately enhances electrocatalytic performance. Indeed, solid acid fuel cells fabricated with electrodes from processed nanofibre-nanoparticle composites, produced higher cell voltage as compared to fuel cells fabricated with state-of-the-art electrodes.

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Research Organization:: SAFCell, Inc., Pasadena, CA (United States)

Sponsoring Organization:: USDOE Advanced Research Projects Agency - Energy (ARPA-E)

Grant/Contract Number:: AR0000495

OSTI ID:: 1613622

Journal Information:: Nature Communications, Journal Name: Nature Communications Journal Issue: 1 Vol. 9; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Electrical conductivity and thermal stability of (1 − x)CsH2PO4/xSiP y O z (x = 0.2–0.7) composites Ponomareva, V. G.; Shutova, E. S.; Lavrova, G. V. Inorganic Materials, Vol. 44, Issue 9 https://doi.org/10.1134/S0020168508090185	journal	August 2008
Phase Relationship of CsH[sub 2]PO[sub 4]–CsPO[sub 3] System and Electrical Properties of CsPO[sub 3] Taninouchi, Yu-ki; Hatada, Naoyuki; Uda, Tetsuya Journal of The Electrochemical Society, Vol. 156, Issue 5 https://doi.org/10.1149/1.3086755	journal	January 2009
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Additional file 1 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577190	dataset	January 2020
Additional file 2 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577196	dataset	January 2020
Additional file 3 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577202	dataset	January 2020
Additional file 4 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577211	dataset	January 2020
Additional file 5 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577217.v1	dataset	January 2020
Additional file 6 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577220.v1	dataset	January 2020
Additional file 7 of Low-cost FDM 3D-printed modular electrospray/electrospinning setup for biomedical applications Huang, Jing; Koutsos, Vasileios; Radacsi, Norbert figshare https://doi.org/10.6084/m9.figshare.12577226	dataset	January 2020
Lightweight and flexible hybrid film based on delicate design of electrospun nanofibers for high-performance electromagnetic interference shielding Huang, Li; Li, Jianjun; Li, Yibin Nanoscale, Vol. 11, Issue 17 https://doi.org/10.1039/c9nr02102g	journal	January 2019
Development of biomimetic electrospun polymeric biomaterials for bone tissue engineering. A review Chahal, Sugandha; Kumar, Anuj; Hussian, Fathima Shahitha Jahir Journal of Biomaterials Science, Polymer Edition, Vol. 30, Issue 14 https://doi.org/10.1080/09205063.2019.1630699	journal	June 2019

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