A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide

Spiekermann, Georg; Kupenko, Ilya; Petitgirard, Sylvain; Harder, Manuel; Nyrow, Alexander; Weis, Christopher; Albers, Christian; Biedermann, Nicole; Libon, Lélia; Sahle, Christoph J.; Cerantola, Valerio; Glazyrin, Konstantin; Konôpková, Zuzana; Sinmyo, Ryosuke; Morgenroth, Wolfgang; Sergueev, Ilya; Yavaş, Hasan; Dubrovinsky, Leonid; Tolan, Metin; Sternemann, Christian; Wilke, Max

doi:10.1107/s1600577519017041

Title: A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide

Journal Article · 13 February 2020 · Journal of Synchrotron Radiation (Online)

DOI: https://doi.org/10.1107/s1600577519017041 · OSTI ID:1608571

Spiekermann, Georg ^[1]; Kupenko, Ilya ^[2]; Petitgirard, Sylvain ^[3]; Harder, Manuel ^[4]; Nyrow, Alexander ^[5]; Weis, Christopher ^[5]; Albers, Christian ^[5]; Biedermann, Nicole ^[6]; Libon, Lélia ^[7];

^[8]; Cerantola, Valerio ^[9];

^[4]; Konôpková, Zuzana ^[9]; Sinmyo, Ryosuke ^[10]; Morgenroth, Wolfgang ^[11]; Sergueev, Ilya ^[4]; Yavaş, Hasan ^[12];

^[13]; Tolan, Metin ^[5];

^[5] more »

Univ. of Potsdam (Germany); Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); GFZ German Research Centre for Geosciences, Potsdam (Germany)
Univ. Munster (Germany)
ETH, Zurich (Switzerland)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
Technische Univ. Dortmund (Germany)
Univ. of Potsdam (Germany); European XFEL, Schenefeld (Germany)
Univ. of Potsdam (Germany)
The European Synchrotron (ESRF), Grenoble (France)
European XFEL, Schenefeld (Germany)
Meiji Univ., Kanagawa (Japan)
Univ. Frankfurt (Germany)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); SLAC National Accelerator Lab., Menlo Park, CA (United States)
Bayerisches Geoinstitut (BGI), Bayreuth (Germany)

A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers double-sided on-axis heating by a single laser source and zero attenuation of incoming X-rays other than by the high-pressure environment. A description of the system, which has been tested for pressures above 100 GPa and temperatures up to 3000 K, is given. The XES spectra of laser-heated Mg_0.67Fe_0.33O demonstrate the potential to map the iron spin state in the pressure–temperature range of the Earth's lower mantle, and the NIS spectra of laser-heated FeSi give access to the sound velocity of this candidate of a phase inside the Earth's core. This portable system represents one of the few bridges across the gap between laser heating and high-resolution X-ray spectroscopies with signal collection near 90°.

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Research Organization:: SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States)

Sponsoring Organization:: USDOE; Federal Ministry of Education and Research (BMBF); German Research Foundation (DFG)

Grant/Contract Number:: AC02-76SF00515; STE 1079/4-1; 05K16RFB; 05K10PEC; 05K13PE2; 05K16PE1

OSTI ID:: 1608571

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 27, Issue 2; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 9 works

Citation information provided by
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Title: A portable on-axis laser-heating system for near-90° X-ray spectroscopy: application to ferropericlase and iron silicide

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