Resonant inelastic X-ray scattering using a miniature dispersive Rowland refocusing spectrometer

Ditter, Alexander S.; Holden, William M.; Cary, Samantha K.; Mocko, Veronika; Latimer, Matthew J.; Nelson, Erik J.; Kozimor, Stosh A.; Seidler, Gerald T.

doi:10.1107/s1600577520001022

Title: Resonant inelastic X-ray scattering using a miniature dispersive Rowland refocusing spectrometer

Journal Article · 20 February 2020 · Journal of Synchrotron Radiation (Online)

DOI: https://doi.org/10.1107/s1600577520001022 · OSTI ID:1608487

^[1]; Holden, William M. ^[2];

^[3];

^[3]; Latimer, Matthew J. ^[4]; Nelson, Erik J. ^[4];

^[3];

^[2]

Univ. of Washington, Seattle, WA (United States); Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Univ. of Washington, Seattle, WA (United States)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
SLAC National Accelerator Lab., Menlo Park, CA (United States)

X-ray absorption spectroscopy (XAS) beamlines worldwide are steadily increasing their emphasis on full photon-in/photon-out spectroscopies, such as resonant inelastic X-ray scattering (RIXS), resonant X-ray emission spectroscopy (RXES) and high energy resolution fluorescence detection XAS (HERFD-XAS). In such cases, each beamline must match the choice of emission spectrometer to the scientific mission of its users. Previous work has recently reported a miniature tender X-ray spectrometer using a dispersive Rowland refocusing (DRR) geometry that functions with high energy resolution even with a large X-ray spot size on the sample. This instrument has been used in the laboratory in multiple studies of non-resonant X-ray emission spectroscopy using a conventional X-ray tube, though only for preliminary measurements at a low-intensity microfocus synchrotron beamline. This paper reports an extensive study of the performance of a miniature DRR spectrometer at an unfocused wiggler beamline, where the incident monochromatic flux allows for resonant studies which are impossible in the laboratory. Here, the results support the broader use of the present design and also suggest that the DRR method with an unfocused beam could have important applications for materials with low radiation damage thresholds and that would not survive analysis on focused beamlines.

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Research Organization:: SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE Office of Science (SC), Biological and Environmental Research (BER); National Inst. of Health

Grant/Contract Number:: 89233218CNA000001; AC02-76SF00515; SC0016251

OSTI ID:: 1608487

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 27, Issue 2; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 5 works

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