Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism

doi:10.1039/D0CE00114G

This content will become publicly available on January 1, 2021

Title: Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism

Abstract

Size and shape-controlled synthesis of gibbsite nanoplates via an additive-free two-step route.

Authors:

Wang, Suyun ^[1];

^[2];

^[2]; Zhang, Hailin ^[2]; Pearce, Carolyn I. ^[3];

^[2]; Clark, Sue B. ^[4];

^[5];

^[2]

Physical & Computational Sciences Directorate; Pacific Northwest National Laboratory; Washington 99354; USA; School of Chemical Engineering
Physical & Computational Sciences Directorate; Pacific Northwest National Laboratory; Washington 99354; USA
Energy & Environment Directorate; Pacific Northwest National Laboratory; Richland; USA
Energy & Environment Directorate; Pacific Northwest National Laboratory; Richland; USA; The Voiland School of Chemical and Biological Engineering
School of Chemical Engineering; Nanjing University of Science and Technology; Nanjing 210094; China

Publication Date:: 2020-01-01

Research Org.:: Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)

OSTI Identifier:: 1605596

Alternate Identifier(s):: OSTI ID: 1605615

Report Number(s):: [PNNL-SA-150680]
[Journal ID: ISSN 1466-8033; CRECF4]

Grant/Contract Number:: [DE-AC05-76RL01830]

Resource Type:: Accepted Manuscript

Journal Name:: CrystEngComm

Additional Journal Information:: [Journal Name: CrystEngComm]; Journal ID: ISSN 1466-8033

Country of Publication:: United States

Language:: English

Citation Formats


                    Wang, Suyun, Zhang, Xin, Graham, Trent R., Zhang, Hailin, Pearce, Carolyn I., Wang, Zheming, Clark, Sue B., Jiang, Wei, and Rosso, Kevin M. Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism.  United States: N. p., 2020. 
        Web.  doi:10.1039/D0CE00114G.

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                    Wang, Suyun, Zhang, Xin, Graham, Trent R., Zhang, Hailin, Pearce, Carolyn I., Wang, Zheming, Clark, Sue B., Jiang, Wei, & Rosso, Kevin M. Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism.  United States.  doi:10.1039/D0CE00114G.

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                    Wang, Suyun, Zhang, Xin, Graham, Trent R., Zhang, Hailin, Pearce, Carolyn I., Wang, Zheming, Clark, Sue B., Jiang, Wei, and Rosso, Kevin M. Wed .  
        "Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism".  United States.  doi:10.1039/D0CE00114G.

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@article{osti_1605596,

  title        = {Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism},

  author       = {Wang, Suyun and Zhang, Xin and Graham, Trent R. and Zhang, Hailin and Pearce, Carolyn I. and Wang, Zheming and Clark, Sue B. and Jiang, Wei and Rosso, Kevin M.},

  abstractNote = {Size and shape-controlled synthesis of gibbsite nanoplates via an additive-free two-step route.},

  doi          = {10.1039/D0CE00114G},

  journal      = {CrystEngComm},

  number       = ,

  volume       = ,

  place        = {United States},

  year         = {2020},

  month        = {1}

}

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DOI: 10.1039/D0CE00114G

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This content will become publicly available on January 1, 2021

Title: Two-step route to size and shape controlled gibbsite nanoplates and the crystal growth mechanism

Abstract

Citation Formats

Synthesis and Characterization of Gibbsite Nanostructures journal, February 2008

Electronic response of aluminum-bearing minerals journal, July 2018

Synthesis of submicron gibbsite platelets by organic-free hydrothermal crystallization process journal, June 2006

Seeded growth of monodisperse gibbsite platelets to adjustable sizes journal, December 2005

Boehmite and Gibbsite Nanoplates for the Synthesis of Advanced Alumina Products journal, November 2018

Atomic force microscopy study of the growth mechanism of gibbsite crystals journal, January 2004

Characterization of aluminum hydroxide (Al(OH)3) for use as a porogenic agent in castable ceramics journal, February 2015

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Evidence for dawsonite in Hanford high-level nuclear waste tanks journal, March 2012

Radiolytic stability of gibbsite and boehmite with adsorbed water journal, April 2018

Effects of Ionic Strength, Salt, and pH on Aggregation of Boehmite Nanocrystals: Tumbler Small-Angle Neutron and X-ray Scattering and Imaging Analysis journal, October 2018

Transformation of Gibbsite to Boehmite in Caustic Aqueous Solution at Hydrothermal Conditions journal, August 2019

Unraveling Gibbsite Transformation Pathways into LiAl-LDH in Concentrated Lithium Hydroxide journal, September 2019

Review of the Scientific Understanding of Radioactive Waste at the U.S. DOE Hanford Site journal, January 2018

Fast Synthesis of Gibbsite Nanoplates and Process Optimization using Box-Behnken Experimental Design journal, October 2017

The surface chemistry of Bayer process solids: a review journal, January 1999

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Pressure Induced Nanoparticle Phase Behavior, Property, and Applications journal, April 2019

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Fast Synthesis and Size Control of Gibbsite Nanoplatelets, Their Pseudomorphic Dehydroxylation, and Efficient Dye Adsorption journal, September 2013

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Nanogibbsite: Synthesis and characterization journal, December 2010

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In Situ 27 Al NMR Spectroscopy of Aluminate in Sodium Hydroxide Solutions above and below Saturation with Respect to Gibbsite journal, July 2018

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Review on alumina trihydrate precipitation mechanisms and effect of Bayer impurities on hydrate particle growth rate journal, December 2013

Precipitation of spherical boehmite from concentrated sodium aluminate solution by adding gibbsite as seed journal, July 2017

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journal, February 2008

Electronic response of aluminum-bearing minerals
journal, July 2018

Synthesis of submicron gibbsite platelets by organic-free hydrothermal crystallization process
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Seeded growth of monodisperse gibbsite platelets to adjustable sizes
journal, December 2005

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Characterization of aluminum hydroxide (Al(OH)3) for use as a porogenic agent in castable ceramics
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Purification of Al(OH)3 synthesized by Bayer process for preparation of high purity alumina as sapphire raw material
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Evidence for dawsonite in Hanford high-level nuclear waste tanks
journal, March 2012

Radiolytic stability of gibbsite and boehmite with adsorbed water
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Effects of Ionic Strength, Salt, and pH on Aggregation of Boehmite Nanocrystals: Tumbler Small-Angle Neutron and X-ray Scattering and Imaging Analysis
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Transformation of Gibbsite to Boehmite in Caustic Aqueous Solution at Hydrothermal Conditions
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Surface morphology and crystal growth mechanism of gibbsite in industrial Bayer liquors
journal, August 2005

Direct observation of the growth of gibbsite crystals by atomic force microscopy
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Revisiting the Growth Mechanism of Hierarchical Semiconductor Nanostructures: The Role of Secondary Nucleation in Branch Formation
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Fast Synthesis and Size Control of Gibbsite Nanoplatelets, Their Pseudomorphic Dehydroxylation, and Efficient Dye Adsorption
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Tailored mesoporous alumina prepared from different aluminum alkoxide precursors
journal, January 2007

Sedimentation and Phase Transitions of Colloidal Gibbsite Platelets
journal, November 2005

Protonation and Charging of Nanosized Gibbsite (α-Al(OH) ₃ ) Particles in Aqueous Suspension
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Multinuclear studies of aluminium compounds
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journal, May 2016

Solid-state aluminium-27 nuclear magnetic resonance chemical shift and quadrupole coupling data for condensed AlO ₄ tetrahedra
journal, January 1986

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Chemical bond change of gibbsite and fumed silica mixture during mechanical activation
journal, October 2012

In Situ ²⁷ Al NMR Spectroscopy of Aluminate in Sodium Hydroxide Solutions above and below Saturation with Respect to Gibbsite
journal, July 2018

Calcination products of gibbsite studied by X-ray diffraction, XPS and solid-state NMR
journal, July 2014

Transitions in Al Coordination during Gibbsite Crystallization Using High-Field ²⁷ Al and ²³ Na MAS NMR Spectroscopy
journal, November 2017

Multiple-Quantum and Cross-Polarized ²⁷ Al MAS NMR of Mechanically Treated Mixtures of Kaolinite and Gibbsite
journal, July 2000

Review on alumina trihydrate precipitation mechanisms and effect of Bayer impurities on hydrate particle growth rate
journal, December 2013

Precipitation of spherical boehmite from concentrated sodium aluminate solution by adding gibbsite as seed
journal, July 2017

Mechanisms of Nucleation and Growth of Nanoparticles in Solution
journal, July 2014

Nucleation and Growth Kinetics from LaMer Burst Data
journal, October 2017

Shape-Controlled Synthesis of Metal Nanostructures: The Case of Palladium
journal, September 2007

Metal oxide nanoparticles: synthesis, characterization and application
journal, February 2006

Shape control of inorganic nanoparticles from solution
journal, January 2016