Substrate damage and incorporation of sapphire into barium hexaferrite films deposited by aerosol deposition

Ranjit, Smriti; Law, Ka Ming; Budhathoki, Sujan; Allred, Jared M.; Rosenberg, Richard A.; Park, Dong‐Soo; Johnson, Scooter; Hauser, Adam J.

doi:10.1111/jace.16864

Title: Substrate damage and incorporation of sapphire into barium hexaferrite films deposited by aerosol deposition

Journal Article · 20 October 2019 · Journal of the American Ceramic Society

DOI: https://doi.org/10.1111/jace.16864 · OSTI ID:1582015

Ranjit, Smriti ^[1]; Law, Ka Ming ^[1]; Budhathoki, Sujan ^[1]; Allred, Jared M. ^[1]; Rosenberg, Richard A. ^[2]; Park, Dong‐Soo ^[3];

^[4];

^[1]

Univ. of Alabama, Tuscaloosa, AL (United States)
Argonne National Lab. (ANL), Lemont, IL (United States)
Korean Inst. of Materials Science, Changwon (Korea)
Naval Research Lab., Washington, D.C (United States)

Barium Hexaferrite (BaM) grown on sapphire substrate by aerosol deposition is investigated in a subtractive wedge series to determine the extent of energetic substrate damage and indentation. Energy dispersive x-ray spectroscopy (EDS) mapping reveals Al₂O₃ particulates ejected from the substrate surface during growth. The concentration of particles is higher at the substrate-film interface but persists throughout the 6 mu m thick film. An estimate of the indentation depth (similar to 600 nm) was agreed upon using two EDS techniques (line scan analysis and substrate surface reconstruction by areal integration). X-ray diffraction patterns show peak polycrystalline Al₂O₃ intensity in 1.5 mu m thick wedges and a decrease at higher thicknesses, confirming that Al₂O₃ particulate density decreases further from the substrate. Here, magnetic characterization showed decreased magnetic moment compared to bulk and thickness dependence consistent with the fractional increase of Al₂O₃ content in the films. X-ray absorption at the Fe L₃ edge suggests a reduction of material close to the surface, but this reduction appears secondary in magnitude to the effect of damage from deposition.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1582015

Journal Information:: Journal of the American Ceramic Society, Vol. 103, Issue 3; ISSN 0002-7820

Publisher:: American Ceramic SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 1 work

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