Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction
Abstract
Synchrotron X-ray radiation Laue diffraction is a widely used diagnostic technique for characterizing the microstructure of materials. An exciting feature of this technique is that comparable numbers of reflections can be measured several orders of magnitude faster than using monochromatic methods. This makes polychromatic beam diffraction a powerful tool for time-resolved microstructural studies, critical for understanding pressure-induced phase transition mechanisms, by in situ and in operando measurements. The current status of this technique, including experimental routines and data analysis, is presented along with some case studies. The new experimental setup at the High-Pressure Collaborative Access Team (HPCAT) facility at the Advanced Photon Source, specifically dedicated for in situ and in operando microstructural studies by Laue diffraction under high pressure, is presented.
- Authors:
-
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States); Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division
- OSTI Identifier:
- 1581777
- Grant/Contract Number:
- AC02-06CH11357; AC52-07NA27344
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Crystals
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 12; Journal ID: ISSN 2073-4352
- Publisher:
- MDPI
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Laue diffraction; high pressure; mechanisms of phase transitions
Citation Formats
Popov, Dmitry, Velisavljevic, Nenad, and Somayazulu, Maddury. Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction. United States: N. p., 2019.
Web. doi:10.3390/cryst9120672.
Popov, Dmitry, Velisavljevic, Nenad, & Somayazulu, Maddury. Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction. United States. https://doi.org/10.3390/cryst9120672
Popov, Dmitry, Velisavljevic, Nenad, and Somayazulu, Maddury. Sat .
"Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction". United States. https://doi.org/10.3390/cryst9120672. https://www.osti.gov/servlets/purl/1581777.
@article{osti_1581777,
title = {Mechanisms of Pressure-Induced Phase Transitions by Real-Time Laue Diffraction},
author = {Popov, Dmitry and Velisavljevic, Nenad and Somayazulu, Maddury},
abstractNote = {Synchrotron X-ray radiation Laue diffraction is a widely used diagnostic technique for characterizing the microstructure of materials. An exciting feature of this technique is that comparable numbers of reflections can be measured several orders of magnitude faster than using monochromatic methods. This makes polychromatic beam diffraction a powerful tool for time-resolved microstructural studies, critical for understanding pressure-induced phase transition mechanisms, by in situ and in operando measurements. The current status of this technique, including experimental routines and data analysis, is presented along with some case studies. The new experimental setup at the High-Pressure Collaborative Access Team (HPCAT) facility at the Advanced Photon Source, specifically dedicated for in situ and in operando microstructural studies by Laue diffraction under high pressure, is presented.},
doi = {10.3390/cryst9120672},
journal = {Crystals},
number = 12,
volume = 9,
place = {United States},
year = {Sat Dec 14 00:00:00 EST 2019},
month = {Sat Dec 14 00:00:00 EST 2019}
}
Web of Science
Works referenced in this record:
A superbend X-ray microdiffraction beamline at the advanced light source
journal, October 2009
- Tamura, N.; Kunz, M.; Chen, K.
- Materials Science and Engineering: A, Vol. 524, Issue 1-2
The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team
journal, July 2015
- Hrubiak, Rostislav; Sinogeikin, Stanislav; Rod, Eric
- Review of Scientific Instruments, Vol. 86, Issue 7
Kinetics of intracrystalline olivine–ringwoodite transformation
journal, September 2000
- Kerschhofer, L.; Rubie, D. C.; Sharp, T. G.
- Physics of the Earth and Planetary Interiors, Vol. 121, Issue 1-2
DIOPTAS : a program for reduction of two-dimensional X-ray diffraction data and data exploration
journal, May 2015
- Prescher, Clemens; Prakapenka, Vitali B.
- High Pressure Research, Vol. 35, Issue 3
Tutorial on x-ray microLaue diffraction
journal, November 2009
- Ice, Gene E.; Pang, Judy W. L.
- Materials Characterization, Vol. 60, Issue 11
A new white beam x-ray microdiffraction setup on the BM32 beamline at the European Synchrotron Radiation Facility
journal, March 2011
- Ulrich, O.; Biquard, X.; Bleuet, P.
- Review of Scientific Instruments, Vol. 82, Issue 3
High-pressure studies with x-rays using diamond anvil cells
journal, November 2016
- Shen, Guoyin; Mao, Ho Kwang
- Reports on Progress in Physics, Vol. 80, Issue 1
Automated indexing for texture and strain measurement with broad-bandpass x-ray microbeams
journal, November 1999
- Chung, Jin-Seok; Ice, Gene E.
- Journal of Applied Physics, Vol. 86, Issue 9
The kinetics of cubic boron nitride formation in the system BN-Mg2N2
journal, September 1988
- Lorenz, Helmar; Lorenz, Bernd; K�hne, Ulrich
- Journal of Materials Science, Vol. 23, Issue 9
Real time study of grain enlargement in zirconium under room-temperature compression across the α to ω phase transition
journal, October 2019
- Popov, Dmitry; Velisavljevic, Nenad; Liu, Wenjun
- Scientific Reports, Vol. 9, Issue 1
Mechanisms of transformation and deformation in Mg1.8Fe0.2SiO4 olivine and wadsleyite under non-hydrostatic stress
journal, May 1998
- Dupas-Bruzek, Catherine; Sharp, Thomas G.; Rubie, David C.
- Physics of the Earth and Planetary Interiors, Vol. 108, Issue 1
Progress of in situ synchrotron X-ray diffraction studies on the mechanical behavior of materials at small scales
journal, May 2018
- Cornelius, Thomas W.; Thomas, Olivier
- Progress in Materials Science, Vol. 94
Fly scan apparatus for high pressure research using diamond anvil cells
journal, January 2019
- Smith, Jesse S.; Rod, Eric A.; Shen, Guoyin
- Review of Scientific Instruments, Vol. 90, Issue 1
Two-dimensional detector software: From real detector to idealised image or two-theta scan
journal, January 1996
- Hammersley, A. P.; Svensson, S. O.; Hanfland, M.
- High Pressure Research, Vol. 14, Issue 4-6, p. 235-248
Effects of interstitial impurities on the high pressure martensitic α to ω structural transformation and grain growth in zirconium
journal, March 2011
- Velisavljevic, Nenad; Chesnut, Gary N.; Stevens, Lewis L.
- Journal of Physics: Condensed Matter, Vol. 23, Issue 12
High pressure Laue diffraction and its application to study microstructural changes during the α → β phase transition in Si
journal, July 2015
- Popov, D.; Park, C.; Kenney-Benson, C.
- Review of Scientific Instruments, Vol. 86, Issue 7
Multiscale twin hierarchy in NiMnGa shape memory alloys with Fe and Cu
journal, April 2015
- Barabash, Rozaliya I.; Barabash, Oleg M.; Popov, Dmitry
- Acta Materialia, Vol. 87