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Title: Coupling of NMR to ACOMP for Terpolymerization Monitoring and Control

Authors:
 [1];  [1];  [1];  [2]; ORCiD logo [1]
  1. Department of Physics and Engineering PhysicsTulane University New Orleans LA 70118 USA
  2. Fluence Analytics 1078 South Gayoso Street New Orleans LA 70125 USA
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1573421
Grant/Contract Number:  
DE EE0005776
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Macromolecular Reaction Engineering
Additional Journal Information:
Journal Name: Macromolecular Reaction Engineering Journal Volume: 13 Journal Issue: 6; Journal ID: ISSN 1862-832X
Publisher:
Wiley Blackwell (John Wiley & Sons)
Country of Publication:
Germany
Language:
English

Citation Formats

McAfee, Terry, Jarand, Curtis W., Zekoski, Thomas, Montgomery, Rick, and Reed, Wayne F. Coupling of NMR to ACOMP for Terpolymerization Monitoring and Control. Germany: N. p., 2019. Web. doi:10.1002/mren.201900039.
McAfee, Terry, Jarand, Curtis W., Zekoski, Thomas, Montgomery, Rick, & Reed, Wayne F. Coupling of NMR to ACOMP for Terpolymerization Monitoring and Control. Germany. doi:10.1002/mren.201900039.
McAfee, Terry, Jarand, Curtis W., Zekoski, Thomas, Montgomery, Rick, and Reed, Wayne F. Thu . "Coupling of NMR to ACOMP for Terpolymerization Monitoring and Control". Germany. doi:10.1002/mren.201900039.
@article{osti_1573421,
title = {Coupling of NMR to ACOMP for Terpolymerization Monitoring and Control},
author = {McAfee, Terry and Jarand, Curtis W. and Zekoski, Thomas and Montgomery, Rick and Reed, Wayne F.},
abstractNote = {},
doi = {10.1002/mren.201900039},
journal = {Macromolecular Reaction Engineering},
number = 6,
volume = 13,
place = {Germany},
year = {2019},
month = {11}
}

Journal Article:
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Works referenced in this record:

Inferential Conversion and Composition Monitoring via Microcalorimetric Measurements in Emulsion Terpolymerization
journal, December 2007

  • Srour, M. H.; Gomes, Vincent G.; Altarawneh, I. S.
  • Polymer-Plastics Technology and Engineering, Vol. 47, Issue 1
  • DOI: 10.1080/03602550701575946

Automatic Control of Polymer Molecular Weight during Synthesis
journal, September 2016


Polymer Composition Control in Emulsion Co- and Terpolymerizations
journal, March 2002

  • Othman, Nida; Févotte, Gilles; McKenna, Timothy F.
  • Industrial & Engineering Chemistry Research, Vol. 41, Issue 5
  • DOI: 10.1021/ie0101994

Online model-based control of an emulsion terpolymerisation process
journal, May 2009

  • Srour, M. H.; Gomes, Vincent G.; Altarawneh, I. S.
  • Chemical Engineering Science, Vol. 64, Issue 9
  • DOI: 10.1016/j.ces.2009.01.044

Macromol. Chem. Phys. 1/2018
journal, January 2018

  • Haenelt, Taida Gil; Abetz, Clarissa; Abetz, Volker
  • Macromolecular Chemistry and Physics, Vol. 219, Issue 1
  • DOI: 10.1002/macp.201870001

Mathematical modeling of diffusion-controlled free-radical terpolymerization reactions
journal, January 2003

  • Keramopoulos, Anastasios; Kiparissides, Costas
  • Journal of Applied Polymer Science, Vol. 88, Issue 1
  • DOI: 10.1002/app.11619

Terpolymerization monitoring with ATR-FTIR spectroscopy: Terpolymerization Monitoring
journal, April 2001

  • Hua, Hong; Dubé, Marc A.
  • Journal of Polymer Science Part A: Polymer Chemistry, Vol. 39, Issue 11
  • DOI: 10.1002/pola.1164

Online Optimal Feedback Control of Polymerization Reactors: Application to Polymerization of Acrylamide–Water–Potassium Persulfate (KPS) System
journal, June 2017

  • Ghadipasha, Navid; Zhu, Wenbo; Romagnoli, Jose A.
  • Industrial & Engineering Chemistry Research, Vol. 56, Issue 25
  • DOI: 10.1021/acs.iecr.7b01074

Thermoresponsive gels based on ABC triblock copolymers: effect of the length of the PEG side group
journal, January 2016

  • Constantinou, A. P.; Georgiou, T. K.
  • Polymer Chemistry, Vol. 7, Issue 11
  • DOI: 10.1039/C5PY02072G

High solids content emulsion terpolymerization of vinyl acetate, methyl methacrylate and butyl acrylate. II. Open loop composition control
journal, July 1994

  • Urretabizkaia, Agustín; Arzamendi, Gurutze; Unzué, María J.
  • Journal of Polymer Science Part A: Polymer Chemistry, Vol. 32, Issue 9
  • DOI: 10.1002/pola.1994.080320920

Determination of Molecular Mass during Online Monitoring of Copolymerization Reactions
journal, October 2007

  • Enohnyaket, Pascal; Kreft, Tomasz; Alb, Alina M.
  • Macromolecules, Vol. 40, Issue 22
  • DOI: 10.1021/ma0717338

Automatic, simultaneous control of polymer composition and molecular weight during free radical copolymer synthesis
journal, January 2018


The Scattering of Light and the Radial Distribution Function of High Polymer Solutions
journal, December 1948

  • Zimm, Bruno H.
  • The Journal of Chemical Physics, Vol. 16, Issue 12
  • DOI: 10.1063/1.1746738

Poly(N-vinyl-2-pyrrolidone-maleic anhydride-styrene) grafted terpolymer: Synthesis, characterization, and bactericidal property evaluation against E. coli and S. epidermidis
journal, July 2017

  • Ajithkumar, M. P.; Yashoda, M. P.; Prasannakumar, S.
  • Journal of Macromolecular Science, Part A, Vol. 54, Issue 7
  • DOI: 10.1080/10601325.2017.1320753

Evolution of Composition, Molar Mass, and Conductivity during the Free Radical Copolymerization of Polyelectrolytes
journal, July 2007

  • Alb, Alina M.; Paril, Ahmet; Çatalgil-Giz, Huceste
  • The Journal of Physical Chemistry B, Vol. 111, Issue 29
  • DOI: 10.1021/jp0688299

Light-Scattering Studies of Copolymers: i. Effect of Heterogeneity of Chain Composition on the Molecular Weight
journal, December 1958

  • Bushuk, W.; Benoit, H.
  • Canadian Journal of Chemistry, Vol. 36, Issue 12
  • DOI: 10.1139/v58-235

Synthesis and photovoltaic properties of three different types of terpolymers
journal, January 2017

  • Uddin, Mohammad Afsar; An, Na Gyeong; Li, Yuxiang
  • Materials Chemistry Frontiers, Vol. 1, Issue 6
  • DOI: 10.1039/C6QM00267F

On-Line Monitoring of Emulsion Terpolymerization Processes
journal, November 2001

  • Othman, Nida; Févotte, Gilles; McKenna, Timothy F.
  • Polymer Reaction Engineering, Vol. 9, Issue 4
  • DOI: 10.1081/PRE-100107510

Synthesis and characterization of SSS/HAM/AA terpolymer as a fluid loss additive for oil well cement: Research Article
journal, February 2018

  • Wu, Jing; Li, Ming; Zhang, Aili
  • Journal of Applied Polymer Science, Vol. 135, Issue 22
  • DOI: 10.1002/app.46266

Batch separation studies for the removal of heavy metal ions using a chelating terpolymer: Synthesis, characterization and isotherm models
journal, September 2013


Infrared process monitoring of conjugated linoleic acid/styrene/butyl acrylate bulk and emulsion terpolymerization
journal, March 2016

  • Roberge, Stéphane; Dubé, Marc A.
  • Journal of Applied Polymer Science, Vol. 133, Issue 26
  • DOI: 10.1002/app.43574

Emulsion co- and terpolymerization of styrene, methyl methacrylate and methyl acrylate. II. Control of emulsion terpolymer microstructure with optimal addition profiles
journal, April 1996


Copolymers in dilute solution. I. Preliminary results for styrene-methyl methacrylate
journal, April 1955