Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly
Abstract
Mesoporous FexOy and Pt@FexOy have proven promising performance in catalysis. Yet, current methods usually use wet chemistry, which poses several drawbacks. Here, we introduce a simple process of mechanochemical assembly between an iron salt and a triblock copolymer in the solid state that can not only directly form abundant mesopores into FexOy, but also enable a high dispersion of Pt species at the nm or sub-nm scale. In this regard, mesoporous FexOy and Pt@FexOy catalysts with high surface areas (up to 149 m2 g-1) and narrow pore size distributions (~5 nm) can be obtained in a solvent-free and rapid (0.5 h) way. The kinetic energy and frictional heating of ball milling are expected to promote the interaction and diffusion between iron precursors and surfactants, while the solvent-free feature confines their assembly to the mesophase of the P123 copolymer. Moreover, these Pt@FexOy catalysts provide good activity in the total oxidation of propylene and CO.
- Authors:
-
[2];
[4]
- East China Normal Univ., Shanghai (China)
- Shanghai Jiao Tong Univ. (China)
- Univ. of Tennessee, Knoxville, TN (United States)
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Brookhaven National Lab. (BNL), Upton, NY (United States)
- Publication Date:
- Research Org.:
- Brookhaven National Lab. (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division; National Natural Science Foundation of China (NNSFC)
- OSTI Identifier:
- 1570676
- Report Number(s):
- BNL-212200-2019-JAAM
Journal ID: ISSN 2044-4753; CSTAGD
- Grant/Contract Number:
- SC0012704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Catalysis Science and Technology
- Additional Journal Information:
- Journal Volume: 9; Journal Issue: 15; Journal ID: ISSN 2044-4753
- Publisher:
- Royal Society of Chemistry
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE
Citation Formats
Zhou, Min, Zhao, Jiahua, Zhang, Pengfei, Chen, Nanqing, and Yang, Shize. Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly. United States: N. p., 2019.
Web. doi:10.1039/C9CY00970A.
Zhou, Min, Zhao, Jiahua, Zhang, Pengfei, Chen, Nanqing, & Yang, Shize. Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly. United States. doi:10.1039/C9CY00970A.
Zhou, Min, Zhao, Jiahua, Zhang, Pengfei, Chen, Nanqing, and Yang, Shize. Mon .
"Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly". United States. doi:10.1039/C9CY00970A. https://www.osti.gov/servlets/purl/1570676.
@article{osti_1570676,
title = {Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly},
author = {Zhou, Min and Zhao, Jiahua and Zhang, Pengfei and Chen, Nanqing and Yang, Shize},
abstractNote = {Mesoporous FexOy and Pt@FexOy have proven promising performance in catalysis. Yet, current methods usually use wet chemistry, which poses several drawbacks. Here, we introduce a simple process of mechanochemical assembly between an iron salt and a triblock copolymer in the solid state that can not only directly form abundant mesopores into FexOy, but also enable a high dispersion of Pt species at the nm or sub-nm scale. In this regard, mesoporous FexOy and Pt@FexOy catalysts with high surface areas (up to 149 m2 g-1) and narrow pore size distributions (~5 nm) can be obtained in a solvent-free and rapid (0.5 h) way. The kinetic energy and frictional heating of ball milling are expected to promote the interaction and diffusion between iron precursors and surfactants, while the solvent-free feature confines their assembly to the mesophase of the P123 copolymer. Moreover, these Pt@FexOy catalysts provide good activity in the total oxidation of propylene and CO.},
doi = {10.1039/C9CY00970A},
journal = {Catalysis Science and Technology},
number = 15,
volume = 9,
place = {United States},
year = {2019},
month = {7}
}
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Facile Synthesis of Highly Porous Metal Oxides by Mechanochemical Nanocasting
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Works referencing / citing this record:
Nanocasting: A Versatile Strategy for Creating Nanostructured Porous Materials
journal, July 2006
- Lu, A. -H.; Schüth, F.
- Advanced Materials, Vol. 18, Issue 14
Mesoporous Mn2O3 and Mn3O4 with Crystalline Walls
journal, November 2007
- Jiao, F.; Harrison, A.; Hill, A. H.
- Advanced Materials, Vol. 19, Issue 22
Soluble Porous Coordination Polymers by Mechanochemistry: From Metal-Containing Films/Membranes to Active Catalysts for Aerobic Oxidation
journal, November 2014
- Zhang, Pengfei; Li, Haiying; Veith, Gabriel M.
- Advanced Materials, Vol. 27, Issue 2
Solvent-Free Self-Assembly to the Synthesis of Nitrogen-Doped Ordered Mesoporous Polymers for Highly Selective Capture and Conversion of CO 2
journal, May 2017
- Liu, Fujian; Huang, Kuan; Wu, Qin
- Advanced Materials, Vol. 29, Issue 27
Chemical solvent in chemical solvent: A class of hybrid materials for effective capture of CO 2
journal, September 2017
- Chen, Feng-Feng; Huang, Kuan; Fan, Jie-Ping
- AIChE Journal, Vol. 64, Issue 2
High Reactivity of Metal-Organic Frameworks under Grinding Conditions: Parallels with Organic Molecular Materials
journal, April 2010
- Yuan, Wenbing; Friščić, Tomislav; Apperley, David
- Angewandte Chemie, Vol. 122, Issue 23
Crystal-to-Crystal Phase Transition in Self-Assembled Mesoporous Iron Oxide Films
journal, January 2006
- Brezesinski, Torsten; Groenewolt, Matthijs; Antonietti, Markus
- Angewandte Chemie International Edition, Vol. 45, Issue 5, p. 781-784
Pharmaceutical Nano-Cocrystals: Sonochemical Synthesis by Solvent Selection and Use of a Surfactant
journal, September 2010
- Sander, John R. G.; Bučar, Dejan-Krešimir; Henry, Rodger F.
- Angewandte Chemie International Edition, Vol. 49, Issue 40
Rapid Room-Temperature Synthesis of Zeolitic Imidazolate Frameworks by Using Mechanochemistry
journal, November 2010
- Beldon, Patrick J.; Fábián, László; Stein, Robin S.
- Angewandte Chemie International Edition, Vol. 49, Issue 50
Solvent-Free Synthesis of Silicoaluminophosphate Zeolites
journal, July 2013
- Jin, Yinying; Sun, Qi; Qi, Guodong
- Angewandte Chemie International Edition, Vol. 52, Issue 35
Charged Porous Polymers using a Solid CO Cross-Coupling Reaction
journal, July 2015
- Zhang, Pengfei; Jiang, Xueguang; Wan, Shun
- Chemistry - A European Journal, Vol. 21, Issue 37
Controllable Synthesis of Mesoporous Iron Oxide Nanoparticle Assemblies for Chemoselective Catalytic Reduction of Nitroarenes
journal, February 2016
- Papadas, Ioannis T.; Fountoulaki, Stella; Lykakis, Ioannis N.
- Chemistry - A European Journal, Vol. 22, Issue 13
Ultrathin Coating of Confined Pt Nanocatalysts by Atomic Layer Deposition for Enhanced Catalytic Performance in Hydrogenation Reactions
journal, May 2016
- Wang, Meihua; Gao, Zhe; Zhang, Bin
- Chemistry - A European Journal, Vol. 22, Issue 25
Solvent-Free Mechanochemical Synthesis of Nitrogen-Doped Nanoporous Carbon for Electrochemical Energy Storage
journal, May 2017
- Schneidermann, Christina; Jäckel, Nicolas; Oswald, Steffen
- ChemSusChem, Vol. 10, Issue 11
Mesoporous Metallic Cells: Design of Uniformly Sized Hollow Mesoporous Pt-Ru Particles with Tunable Shell Thicknesses
journal, December 2012
- Ataee-Esfahani, Hamed; Liu, Jian; Hu, Ming
- Small, Vol. 9, Issue 7
Evaporation-Induced Coating of Hydrous Ruthenium Oxide on Mesoporous Silica Nanoparticles to Develop High-Performance Supercapacitors
journal, March 2013
- Huang, Hou-Sheng; Chang, Kuo-Hsin; Suzuki, Norihiro
- Small, Vol. 9, Issue 15
Some Difficult Challenges for the Synthesis of Nanoporous Materials
journal, October 2010
- Morris, Russell E.
- Topics in Catalysis, Vol. 53, Issue 19-20
Synthesis of ordered mesoporous iron manganese bimetal oxides for arsenic removal from aqueous solutions
journal, December 2014
- Wen, Zhipan; Zhang, Yalei; Dai, Chaomeng
- Microporous and Mesoporous Materials, Vol. 200
Mechanochemical synthesis of metal–organic frameworks
journal, April 2019
- Chen, Dong; Zhao, Jiahua; Zhang, Pengfei
- Polyhedron, Vol. 162
Solid-state CTAB-assisted synthesis of mesoporous Fe3O4 and Au@Fe3O4 by mechanochemistry
journal, July 2019
- Zhao, Jiahua; Shu, Yuan; Zhang, Pengfei
- Chinese Journal of Catalysis, Vol. 40, Issue 7
Synthesis of Nanoporous Metals, Oxides, Carbides, and Sulfides: Beyond Nanocasting
journal, June 2016
- Luc, Wesley; Jiao, Feng
- Accounts of Chemical Research, Vol. 49, Issue 7
Protocol for the Nanocasting Method: Preparation of Ordered Mesoporous Metal Oxides
journal, September 2016
- Deng, Xiaohui; Chen, Kun; Tüysüz, Harun
- Chemistry of Materials, Vol. 29, Issue 1
Incorporating Rich Mesoporosity into a Ceria-Based Catalyst via Mechanochemistry
journal, August 2017
- Zhan, Wangcheng; Yang, Shize; Zhang, Pengfei
- Chemistry of Materials, Vol. 29, Issue 17
Facile Synthesis of Highly Porous Metal Oxides by Mechanochemical Nanocasting
journal, April 2018
- Xiao, Weiming; Yang, Shize; Zhang, Pengfei
- Chemistry of Materials, Vol. 30, Issue 9
Engineering Ordered and Nonordered Porous Noble Metal Nanostructures: Synthesis, Assembly, and Their Applications in Electrochemistry
journal, July 2015
- Zhu, Chengzhou; Du, Dan; Eychmüller, Alexander
- Chemical Reviews, Vol. 115, Issue 16
Synthesis of Mesoporous Iron Oxides by an Inverse Micelle Method and Their Application in the Degradation of Orange II under Visible Light at Neutral pH
journal, April 2015
- Jiang, Ting; Poyraz, Altug S.; Iyer, Aparna
- The Journal of Physical Chemistry C, Vol. 119, Issue 19
Mesoporous Iron Oxide Synthesized Using Poly(styrene- b -acrylic acid- b -ethylene glycol) Block Copolymer Micelles as Templates for Colorimetric and Electrochemical Detection of Glucose
journal, December 2017
- Tanaka, Shunsuke; Kaneti, Yusuf Valentino; Bhattacharjee, Ripon
- ACS Applied Materials & Interfaces, Vol. 10, Issue 1
Synthesis of Porous Polymeric Catalysts for the Conversion of Carbon Dioxide
journal, August 2018
- Huang, Kuan; Zhang, Jia-Yin; Liu, Fujian
- ACS Catalysis, Vol. 8, Issue 10
Synthesis of Hard Magnetic Ordered Mesoporous Co 3 O 4 /CoFe 2 O 4 Nanocomposites
journal, June 2012
- Tüysüz, Harun; Salabaş, Elena Lorena; Bill, Eckhard
- Chemistry of Materials, Vol. 24, Issue 13
Design of Ordered Mesoporous Composite Materials and Their Electrocatalytic Activities for Water Oxidation
journal, December 2013
- Grewe, Tobias; Deng, Xiaohui; Weidenthaler, Claudia
- Chemistry of Materials, Vol. 25, Issue 24
Green Routes for Synthesis of Zeolites
journal, November 2013
- Meng, Xiangju; Xiao, Feng-Shou
- Chemical Reviews, Vol. 114, Issue 2
Synthesis of Ordered Mesoporous Fe 3 O 4 and γ-Fe 2 O 3 with Crystalline Walls Using Post-Template Reduction/Oxidation
journal, October 2006
- Jiao, Feng; Jumas, Jean-Claude; Womes, Manfred
- Journal of the American Chemical Society, Vol. 128, Issue 39
Container Effect in Nanocasting Synthesis of Mesoporous Metal Oxides
journal, September 2011
- Sun, Xiaohong; Shi, Yifeng; Zhang, Peng
- Journal of the American Chemical Society, Vol. 133, Issue 37
Solvent-Free Synthesis of Zeolites from Solid Raw Materials
journal, September 2012
- Ren, Limin; Wu, Qinming; Yang, Chengguang
- Journal of the American Chemical Society, Vol. 134, Issue 37
Mechanochemical Synthesis of Chemically Stable Isoreticular Covalent Organic Frameworks
journal, March 2013
- Biswal, Bishnu P.; Chandra, Suman; Kandambeth, Sharath
- Journal of the American Chemical Society, Vol. 135, Issue 14
Synthetic Control of FePtM Nanorods (M = Cu, Ni) To Enhance the Oxygen Reduction Reaction
journal, May 2013
- Zhu, Huiyuan; Zhang, Sen; Guo, Shaojun
- Journal of the American Chemical Society, Vol. 135, Issue 19
Chemically Stable Multilayered Covalent Organic Nanosheets from Covalent Organic Frameworks via Mechanical Delamination
journal, November 2013
- Chandra, Suman; Kandambeth, Sharath; Biswal, Bishnu P.
- Journal of the American Chemical Society, Vol. 135, Issue 47
Solvent-Free Synthesis of Zeolites from Anhydrous Starting Raw Solids
journal, January 2015
- Wu, Qinming; Liu, Xiaolong; Zhu, Longfeng
- Journal of the American Chemical Society, Vol. 137, Issue 3
Evolution of Standing Mesochannels on Porous Anodic Alumina Substrates with Designed Conical Holes
journal, August 2008
- Yamauchi, Yusuke; Nagaura, Tomota; Ishikawa, Ayako
- Journal of the American Chemical Society, Vol. 130, Issue 31
Synthesis of Ordered Mesoporous NiO with Crystalline Walls and a Bimodal Pore Size Distribution
journal, April 2008
- Jiao, Feng; Hill, Adrian H.; Harrison, Andrew
- Journal of the American Chemical Society, Vol. 130, Issue 15
Pseudomorphic Transformation of Highly Ordered Mesoporous Co 3 O 4 to CoO via Reduction with Glycerol
journal, October 2008
- Tüysüz, Harun; Liu, Yong; Weidenthaler, Claudia
- Journal of the American Chemical Society, Vol. 130, Issue 43
Synthesis of Mesoporous Metal Oxide by the Thermal Decomposition of Oxalate Precursor
journal, February 2013
- Guo, Limin; Arafune, Hiroyuki; Teramae, Norio
- Langmuir, Vol. 29, Issue 13
Polymeric Micelle Assembly for Preparation of Large-Sized Mesoporous Metal Oxides with Various Compositions
journal, January 2014
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