DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Variation of elastic mechanical properties with texture, porosity, and defect characteristics in laser powder bed fusion 316L stainless steel

Abstract

Elastic mechanical properties of 316 L stainless steel samples fabricated using laser powder bed fusion were studied non-destructively through resonant ultrasound spectroscopy. Samples in five different conditions were obtained by varying the laser power from 103 W (the highest density condition) to 68 W (the lowest density condition) at constant laser speed, producing samples with a volume energy density in the 24.5-16.5 J/mm(3) range and volumetric porosity in the 0.1-10% range. The observed elastic mechanical properties are discussed taking into consideration the bulk texture developed and quantitative pore characteristics studied using high-energy high-resolution synchrotron X-ray diffraction and X-ray computed micro-tomography, respectively. Furthermore, empirical exponential relationships are provided to express the functional dependence of Young's and shear moduli with porosity.

Authors:
 [1];  [2];  [1];  [2];  [1];  [3];  [3];  [4]
  1. Y-12 National Security Complex, Oak Ridge, TN (United States)
  2. Univ. of Tennessee, Knoxville, TN (United States)
  3. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
  4. Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Publication Date:
Research Org.:
Brookhaven National Laboratory (BNL), Upton, NY (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA)
OSTI Identifier:
1570662
Alternate Identifier(s):
OSTI ID: 1630422; OSTI ID: 2325414
Report Number(s):
BNL-212142-2019-JAAM
Journal ID: ISSN 0921-5093; TRN: US2001364
Grant/Contract Number:  
SC0012704; AC02-06CH11357
Resource Type:
Accepted Manuscript
Journal Name:
Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
Additional Journal Information:
Journal Volume: 763; Journal Issue: C; Journal ID: ISSN 0921-5093
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Resonant ultrasound spectroscopy (RUS); Elastic mechanical properties; X-ray synchrotron micro-tomography and diffraction; Porosity and texture; Stainless steel; Laser powder bed fusion

Citation Formats

Garlea, E., Choo, H., Sluss, C. C., Koehler, M. R., Bridges, R. L., Xiao, Xianghui, Ren, Y., and Jared, B. H. Variation of elastic mechanical properties with texture, porosity, and defect characteristics in laser powder bed fusion 316L stainless steel. United States: N. p., 2019. Web. doi:10.1016/j.msea.2019.138032.
Garlea, E., Choo, H., Sluss, C. C., Koehler, M. R., Bridges, R. L., Xiao, Xianghui, Ren, Y., & Jared, B. H. Variation of elastic mechanical properties with texture, porosity, and defect characteristics in laser powder bed fusion 316L stainless steel. United States. https://doi.org/10.1016/j.msea.2019.138032
Garlea, E., Choo, H., Sluss, C. C., Koehler, M. R., Bridges, R. L., Xiao, Xianghui, Ren, Y., and Jared, B. H. Mon . "Variation of elastic mechanical properties with texture, porosity, and defect characteristics in laser powder bed fusion 316L stainless steel". United States. https://doi.org/10.1016/j.msea.2019.138032. https://www.osti.gov/servlets/purl/1570662.
@article{osti_1570662,
title = {Variation of elastic mechanical properties with texture, porosity, and defect characteristics in laser powder bed fusion 316L stainless steel},
author = {Garlea, E. and Choo, H. and Sluss, C. C. and Koehler, M. R. and Bridges, R. L. and Xiao, Xianghui and Ren, Y. and Jared, B. H.},
abstractNote = {Elastic mechanical properties of 316 L stainless steel samples fabricated using laser powder bed fusion were studied non-destructively through resonant ultrasound spectroscopy. Samples in five different conditions were obtained by varying the laser power from 103 W (the highest density condition) to 68 W (the lowest density condition) at constant laser speed, producing samples with a volume energy density in the 24.5-16.5 J/mm(3) range and volumetric porosity in the 0.1-10% range. The observed elastic mechanical properties are discussed taking into consideration the bulk texture developed and quantitative pore characteristics studied using high-energy high-resolution synchrotron X-ray diffraction and X-ray computed micro-tomography, respectively. Furthermore, empirical exponential relationships are provided to express the functional dependence of Young's and shear moduli with porosity.},
doi = {10.1016/j.msea.2019.138032},
journal = {Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing},
number = C,
volume = 763,
place = {United States},
year = {Mon Jun 17 00:00:00 EDT 2019},
month = {Mon Jun 17 00:00:00 EDT 2019}
}

Journal Article:

Citation Metrics:
Cited by: 34 works
Citation information provided by
Web of Science

Save / Share:

Works referenced in this record:

Metal Additive Manufacturing: A Review
journal, April 2014


Additive manufacturing of metallic components – Process, structure and properties
journal, March 2018


Modeling of Powder Bed Manufacturing Defects
journal, September 2017

  • Mindt, H. -W.; Desmaison, O.; Megahed, M.
  • Journal of Materials Engineering and Performance, Vol. 27, Issue 1
  • DOI: 10.1007/s11665-017-2874-5

Additive manufacturing of metals
journal, September 2016


The Origin of Microstructural Diversity, Texture, and Mechanical Properties in Electron Beam Melted Ti-6Al-4V
journal, August 2010

  • Al-Bermani, S. S.; Blackmore, M. L.; Zhang, W.
  • Metallurgical and Materials Transactions A, Vol. 41, Issue 13
  • DOI: 10.1007/s11661-010-0397-x

Effect of build geometry on the β-grain structure and texture in additive manufacture of Ti6Al4V by selective electron beam melting
journal, October 2013


A study of the microstructural evolution during selective laser melting of Ti–6Al–4V
journal, May 2010


Investigation into the effect of process parameters on microstructural and physical properties of 316L stainless steel parts by selective laser melting
journal, September 2014

  • Cherry, J. A.; Davies, H. M.; Mehmood, S.
  • The International Journal of Advanced Manufacturing Technology, Vol. 76, Issue 5-8
  • DOI: 10.1007/s00170-014-6297-2

Effect of laser power on defect, texture, and microstructure of a laser powder bed fusion processed 316L stainless steel
journal, February 2019


Young’s modulus and volume porosity relationships for additive manufacturing applications
journal, April 2013

  • Choren, J. A.; Heinrich, S. M.; Silver-Thorn, M. B.
  • Journal of Materials Science, Vol. 48, Issue 15
  • DOI: 10.1007/s10853-013-7237-5

Elastic Properties of Model Porous Ceramics
journal, December 2000


Metal Additive Manufacturing: A Review of Mechanical Properties
journal, July 2016


Mechanical behavior of additive manufactured, powder-bed laser-fused materials
journal, January 2016


Effects of hot isostatic pressing on the elastic modulus and tensile properties of 316L parts made by powder bed laser fusion
journal, May 2017


Microstructure and mechanical behavior of porous sintered steels
journal, January 2005


The study of the laser parameters and environment variables effect on mechanical properties of high compact parts elaborated by selective laser melting 316L powder
journal, November 2013

  • Zhang, Baicheng; Dembinski, Lucas; Coddet, Christian
  • Materials Science and Engineering: A, Vol. 584
  • DOI: 10.1016/j.msea.2013.06.055

Comparison of different experimental techniques for determination of elastic properties of solids
journal, March 2004

  • Radovic, M.; Lara-Curzio, E.; Riester, L.
  • Materials Science and Engineering: A, Vol. 368, Issue 1-2
  • DOI: 10.1016/j.msea.2003.09.080

Temperature dependent elastic properties of γ-phase U – 8 wt% Mo
journal, March 2018


Porosity Measurements and Analysis for Metal Additive Manufacturing Process Control
journal, January 2014

  • Slotwinski, John A.; Garboczi, Edward J.; Hebenstreit, Keith M.
  • Journal of Research of the National Institute of Standards and Technology, Vol. 119
  • DOI: 10.6028/jres.119.019

Evaluation of defects in materials using resonant ultrasound spectroscopy
journal, December 2010


Rapid measurement of volumetric texture using resonant ultrasound spectroscopy
journal, December 2018


TomoPy: a framework for the analysis of synchrotron tomographic data
journal, August 2014

  • Gürsoy, Dogˇa; De Carlo, Francesco; Xiao, Xianghui
  • Journal of Synchrotron Radiation, Vol. 21, Issue 5
  • DOI: 10.1107/S1600577514013939

Fiji: an open-source platform for biological-image analysis
journal, June 2012

  • Schindelin, Johannes; Arganda-Carreras, Ignacio; Frise, Erwin
  • Nature Methods, Vol. 9, Issue 7
  • DOI: 10.1038/nmeth.2019

FIT2D : a multi-purpose data reduction, analysis and visualization program
journal, March 2016


Maud: a Rietveld analysis program designed for the internet and experiment integration
journal, August 2000

  • Lutterotti, L.
  • Acta Crystallographica Section A Foundations of Crystallography, Vol. 56, Issue s1
  • DOI: 10.1107/S0108767300021954

Texture Analysis with MTEX – Free and Open Source Software Toolbox
journal, February 2010


Ultrasonic characteristics of porous Pd42.5Cu30Ni7.5P20 glassy alloys
journal, October 2007

  • Fukuhara, Mikio; Wada, Takeshi; Inoue, Akihisa
  • Journal of Applied Physics, Vol. 102, Issue 8
  • DOI: 10.1063/1.2795684

Poisson's ratio of porous and microcracked solids: Theory and application to oxide superconductors
journal, November 1995

  • Dunn, Martin L.; Ledbetter, Hassel
  • Journal of Materials Research, Vol. 10, Issue 11
  • DOI: 10.1557/JMR.1995.2715

Elastic moduli for a class of porous materials
journal, February 1989

  • Zhao, Y. H.; Tandon, G. P.; Weng, G. J.
  • Acta Mechanica, Vol. 76, Issue 1-2
  • DOI: 10.1007/BF01175799

Works referencing / citing this record:

Forming, fracture and corrosion behaviour of stainless steel 202 sheet formed by single point incremental forming process
journal, November 2019

  • Vignesh, G.; Narayanan, C. Sathiya; Pandivelan, C.
  • Materials Research Express, Vol. 6, Issue 12
  • DOI: 10.1088/2053-1591/ab5606