Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding
Abstract
Recent advancements in the severe plastic deformation process called accumulative roll bonding (ARB) can help to address the long‐standing need for manufacturing lightweight, high‐strength Mg sheet materials. However, the fabrication of Mg alloy‐based laminates via ARB remains a challenge due to the intrinsically poor formability of Mg. Herein, it is shown that Mg‐based composite laminates with refined layers can be fabricated via several room‐temperature ARB cycles with appropriate intermediate annealing and alloy selection. The final laminates made here consist of equal volume fractions of a dilute Mg–Zn–Mn–Ca alloy phase and a pure Nb phase with fine 150 μm layer thicknesses. Deformation texture evolution in both phases within the composite is analyzed via neutron diffraction measurements taken at different stages in the process. The analysis suggests that the annealing step recrystallizes the Mg‐alloy phase. It is also shown that for both phases, the stabilized deformation textures within the composite correspond to the classic stable textures of the individual constituents. Polycrystal texture modeling implies that {10–12} <‐1011> extension twinning developed in the Mg alloy during rolling.
- Authors:
-
[4];
[4];
[4];
- Univ. of California, Santa Barbara, CA (United States). Dept. of Materials Engineering
- Univ. of New Hampshire, Durham, NH (United States). College of Engineering and Physical Sciences
- Univ. of Minnesota, Minneapolis, MN (United States). Dept. of Chemical Engineering and Materials Science
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- nanoMAG LLC, Livonia, MI (United States)
- Publication Date:
- Research Org.:
- Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC). Basic Energy Sciences (BES) (SC-22); USDOE
- OSTI Identifier:
- 1566117
- Alternate Identifier(s):
- OSTI ID: 1558817
- Report Number(s):
- LA-UR-19-25330
Journal ID: ISSN 1438-1656
- Grant/Contract Number:
- 89233218CNA000001; FWP 06SCPE401
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Advanced Engineering Materials
- Additional Journal Information:
- Journal Volume: 22; Journal Issue: 1; Journal ID: ISSN 1438-1656
- Publisher:
- Wiley
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; accumulative roll bonding; interfaces; Mg-alloys; recrystallization; textures
Citation Formats
Leu, Brandon, Savage, Daniel J, Wang, Jiaxiang, Alam, Md Ershadul, Mara, Nathan A, Mariyappan, Arul Kumar, Carpenter, John S., Vogel, Sven C., Knezevic, Marko, Decker, Ray, and Beyerlein, Irene. Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding. United States: N. p., 2019.
Web. doi:10.1002/adem.201900673.
Leu, Brandon, Savage, Daniel J, Wang, Jiaxiang, Alam, Md Ershadul, Mara, Nathan A, Mariyappan, Arul Kumar, Carpenter, John S., Vogel, Sven C., Knezevic, Marko, Decker, Ray, & Beyerlein, Irene. Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding. United States. https://doi.org/10.1002/adem.201900673
Leu, Brandon, Savage, Daniel J, Wang, Jiaxiang, Alam, Md Ershadul, Mara, Nathan A, Mariyappan, Arul Kumar, Carpenter, John S., Vogel, Sven C., Knezevic, Marko, Decker, Ray, and Beyerlein, Irene. Tue .
"Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding". United States. https://doi.org/10.1002/adem.201900673. https://www.osti.gov/servlets/purl/1566117.
@article{osti_1566117,
title = {Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding},
author = {Leu, Brandon and Savage, Daniel J and Wang, Jiaxiang and Alam, Md Ershadul and Mara, Nathan A and Mariyappan, Arul Kumar and Carpenter, John S. and Vogel, Sven C. and Knezevic, Marko and Decker, Ray and Beyerlein, Irene},
abstractNote = {Recent advancements in the severe plastic deformation process called accumulative roll bonding (ARB) can help to address the long‐standing need for manufacturing lightweight, high‐strength Mg sheet materials. However, the fabrication of Mg alloy‐based laminates via ARB remains a challenge due to the intrinsically poor formability of Mg. Herein, it is shown that Mg‐based composite laminates with refined layers can be fabricated via several room‐temperature ARB cycles with appropriate intermediate annealing and alloy selection. The final laminates made here consist of equal volume fractions of a dilute Mg–Zn–Mn–Ca alloy phase and a pure Nb phase with fine 150 μm layer thicknesses. Deformation texture evolution in both phases within the composite is analyzed via neutron diffraction measurements taken at different stages in the process. The analysis suggests that the annealing step recrystallizes the Mg‐alloy phase. It is also shown that for both phases, the stabilized deformation textures within the composite correspond to the classic stable textures of the individual constituents. Polycrystal texture modeling implies that {10–12} <‐1011> extension twinning developed in the Mg alloy during rolling.},
doi = {10.1002/adem.201900673},
journal = {Advanced Engineering Materials},
number = 1,
volume = 22,
place = {United States},
year = {Tue Jul 23 00:00:00 EDT 2019},
month = {Tue Jul 23 00:00:00 EDT 2019}
}
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Figure 1: (a) Electron Back Scatter Diffraction (EBSD) orientation maps and corresponding pole figure showing the initial microstructure of the annealed Mg-alloy. The colors in the orientation map indicate the orientation of the ND sample direction with respect to the grain orientations. (b) Mg- alloy stress-strain response for compression alongmore »
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