Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films

Galy, Tiphaine; Marszewski, Michal; King, Sophia; Yan, Yan; Tolbert, Sarah H.; Pilon, Laurent

doi:10.1016/j.micromeso.2019.109677

Title: Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films

Authors:

Galy, Tiphaine;

; King, Sophia; Yan, Yan; Tolbert, Sarah H.;

Publication Date:: 2020-01-01

Sponsoring Org.:: USDOE Advanced Research Projects Agency - Energy (ARPA-E)

OSTI Identifier:: 1560755

Resource Type:: Publisher's Accepted Manuscript

Journal Name:: Microporous and Mesoporous Materials

Additional Journal Information:: Journal Name: Microporous and Mesoporous Materials Journal Volume: 291 Journal Issue: C; Journal ID: ISSN 1387-1811

Publisher:: Elsevier

Country of Publication:: France

Language:: English

Citation Formats


                    Galy, Tiphaine, Marszewski, Michal, King, Sophia, Yan, Yan, Tolbert, Sarah H., and Pilon, Laurent. Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films.  France: N. p., 2020. 
Web.  doi:10.1016/j.micromeso.2019.109677.

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                    Galy, Tiphaine, Marszewski, Michal, King, Sophia, Yan, Yan, Tolbert, Sarah H., & Pilon, Laurent. Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films.  France.  https://doi.org/10.1016/j.micromeso.2019.109677

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                    Galy, Tiphaine, Marszewski, Michal, King, Sophia, Yan, Yan, Tolbert, Sarah H., and Pilon, Laurent. Wed .  
"Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films".  France.  https://doi.org/10.1016/j.micromeso.2019.109677.

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@article{osti_1560755,

  title        = {Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films},

  author       = {Galy, Tiphaine and Marszewski, Michal and King, Sophia and Yan, Yan and Tolbert, Sarah H. and Pilon, Laurent},

  abstractNote = {},

  doi          = {10.1016/j.micromeso.2019.109677},

  journal      = {Microporous and Mesoporous Materials},

  number       = C,

  volume       = 291,

  place        = {France},

  year         = {2020},

  month        = {1}

}

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https://doi.org/10.1016/j.micromeso.2019.109677

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Title: Comparing methods for measuring thickness, refractive index, and porosity of mesoporous thin films

Citation Formats

Physisorption of gases, with special reference to the evaluation of surface area and pore size distribution (IUPAC Technical Report) journal, October 2015

pH-Dependent Structure and Properties of TiO 2 /SiO 2 Nanoparticle Multilayer Thin Films journal, March 2007

Processing dependent thermal conductivity of nanoporous silica xerogel films journal, March 2002

Non-destructive characterisation of porous low-k dielectric films journal, October 2002

Ueber die Refractionsconstante journal, January 1880

Design of hierarchically meso–macroporous tetragonal ZrO2 thin films with tunable thickness by spin-coating via sol–gel template route journal, February 2013

Sol–gel derived porous silica films journal, January 1999

Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas journal, August 1999

Control of pore size and condensation rate of cubic mesoporous silica thin films using a swelling agent journal, March 2005

Low- k Periodic Mesoporous Organosilica with Air Walls: POSS-PMO journal, November 2011

Guided wave sensing of polyelectrolyte multilayers journal, March 2006

Evaporation-Induced Self-Assembly: Nanostructures Made Easy journal, May 1999

Templating Nanoporosity in Thin-Film Dielectric Insulators journal, September 1998

Ueber die Beziehung zwischen der Fortpflanzungsgeschwindigkeit des Lichtes und der Körperdichte journal, January 1880

Porous silica materials as low-k dielectrics for electronic and optical interconnects journal, November 2001

Fabrication of Ordered Mesoporous Thin Films for Optical Waveguiding and Interferometric Chemical Sensing journal, June 2006

Ultralow-k Dielectrics Made by Supercritical Foaming of Thin Polymer Films journal, August 2002

Determination of Porosity of TiO[sub 2] Films from Reflection Spectra journal, January 2002

Scattering and reflective properties of ordered mesoporous silica films journal, January 2005

Determination of pore size distribution in thin films by ellipsometric porosimetry journal, January 2000

Fundamentals of Mesostructuring Through Evaporation-Induced Self-Assembly journal, April 2004

Thermal conductivity of cubic and hexagonal mesoporous silica thin films journal, August 2009

Bruggeman effective medium approach for modelling optical properties of porous silicon: comparison with experiment journal, May 2007

Gas Adsorption Characterization of Ordered Organic−Inorganic Nanocomposite Materials journal, October 2001

Berechnung verschiedener physikalischer Konstanten von heterogenen Substanzen. I. Dielektrizitätskonstanten und Leitfähigkeiten der Mischkörper aus isotropen Substanzen journal, January 1935

Optical properties of thin films journal, March 1982

Fundamentals of sol-gel dip coating journal, June 1991

Fundamentals and applications of spectroscopic ellipsometry journal, January 2002

Adsorptive Characterization of the ZIF-68 Metal-Organic Framework: A Complex Structure with Amphiphilic Properties journal, July 2014

Effective optical properties of non-absorbing nanoporous thin films journal, February 2006

Characterization and simulation of microstructure and properties of EPS lightweight concrete journal, December 2007

Optical dispersion relations for amorphous semiconductors and amorphous dielectrics journal, November 1986

Optical Properties of Granular Silver and Gold Films journal, October 1973

Adsorption of Gases in Multimolecular Layers journal, February 1938

Maxwell Garnett rule for Dielectric Mixtures with Statistically Distributed Orientations of Inclusions journal, January 2009

Fabrication of highly uniform and porous MgF 2 anti-reflective coatings by polymer-based sol–gel processing on large-area glass substrates journal, November 2013

Enlarged Pore Size in Mesoporous Silica Films Templated by Pluronic F127: Use of Poloxamer Mixtures and Increased Template/SiO 2 Ratios in Materials Synthesized by Evaporation-Induced Self-Assembly journal, December 2014

The Determination of Pore Volume and Area Distributions in Porous Substances. I. Computations from Nitrogen Isotherms journal, January 1951

Porous Thin Films of Functionalized Mesoporous Silica Nanoparticles journal, November 2008

Optical Properties of Nanostructured Optical Materials journal, January 1996

Fabrication of Multilayered Nanoporous Poly(methyl silsesquioxane) journal, November 2002

Effects of Crystallinity in Spin-On Pure-Silica-Zeolite MFI Low-Dielectric-Constant Films journal, October 2004

Interspecimen Comparison of the Refractive Index of Fused Silica*,† journal, January 1965

Reflectance of surfactant-templated mesoporous silica thin films: Simulations versus experiments journal, February 2010

The Kelvin equation—a review journal, January 1972

Effective optical properties of highly ordered mesoporous thin films journal, February 2010

Novel Method of Preparation of Gold-Nanoparticle-Doped TiO2 and SiO2 Plasmonic Thin Films: Optical Characterization and Comparison with Maxwell-Garnett Modeling journal, July 2011

Physisorption of gases, with special reference to the evaluation of surface area and pore size distribution (IUPAC Technical Report)
journal, October 2015

pH-Dependent Structure and Properties of TiO ₂ /SiO ₂ Nanoparticle Multilayer Thin Films
journal, March 2007

Processing dependent thermal conductivity of nanoporous silica xerogel films
journal, March 2002

Non-destructive characterisation of porous low-k dielectric films
journal, October 2002

Ueber die Refractionsconstante
journal, January 1880

Design of hierarchically meso–macroporous tetragonal ZrO2 thin films with tunable thickness by spin-coating via sol–gel template route
journal, February 2013

Sol–gel derived porous silica films
journal, January 1999

Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas
journal, August 1999

Control of pore size and condensation rate of cubic mesoporous silica thin films using a swelling agent
journal, March 2005

Low- k Periodic Mesoporous Organosilica with Air Walls: POSS-PMO
journal, November 2011

Guided wave sensing of polyelectrolyte multilayers
journal, March 2006

Evaporation-Induced Self-Assembly: Nanostructures Made Easy
journal, May 1999

Templating Nanoporosity in Thin-Film Dielectric Insulators
journal, September 1998

Ueber die Beziehung zwischen der Fortpflanzungsgeschwindigkeit des Lichtes und der Körperdichte
journal, January 1880

Porous silica materials as low-k dielectrics for electronic and optical interconnects
journal, November 2001

Fabrication of Ordered Mesoporous Thin Films for Optical Waveguiding and Interferometric Chemical Sensing
journal, June 2006

Ultralow-k Dielectrics Made by Supercritical Foaming of Thin Polymer Films
journal, August 2002

Determination of Porosity of TiO[sub 2] Films from Reflection Spectra
journal, January 2002

Scattering and reflective properties of ordered mesoporous silica films
journal, January 2005

Determination of pore size distribution in thin films by ellipsometric porosimetry
journal, January 2000

Fundamentals of Mesostructuring Through Evaporation-Induced Self-Assembly
journal, April 2004

Thermal conductivity of cubic and hexagonal mesoporous silica thin films
journal, August 2009

Bruggeman effective medium approach for modelling optical properties of porous silicon: comparison with experiment
journal, May 2007

Gas Adsorption Characterization of Ordered Organic−Inorganic Nanocomposite Materials
journal, October 2001

Berechnung verschiedener physikalischer Konstanten von heterogenen Substanzen. I. Dielektrizitätskonstanten und Leitfähigkeiten der Mischkörper aus isotropen Substanzen
journal, January 1935

Optical properties of thin films
journal, March 1982

Fundamentals of sol-gel dip coating
journal, June 1991

Fundamentals and applications of spectroscopic ellipsometry
journal, January 2002

Adsorptive Characterization of the ZIF-68 Metal-Organic Framework: A Complex Structure with Amphiphilic Properties
journal, July 2014

Effective optical properties of non-absorbing nanoporous thin films
journal, February 2006

Characterization and simulation of microstructure and properties of EPS lightweight concrete
journal, December 2007

Optical dispersion relations for amorphous semiconductors and amorphous dielectrics
journal, November 1986

Optical Properties of Granular Silver and Gold Films
journal, October 1973

Adsorption of Gases in Multimolecular Layers
journal, February 1938

Maxwell Garnett rule for Dielectric Mixtures with Statistically Distributed Orientations of Inclusions
journal, January 2009

Fabrication of highly uniform and porous MgF ₂ anti-reflective coatings by polymer-based sol–gel processing on large-area glass substrates
journal, November 2013

Enlarged Pore Size in Mesoporous Silica Films Templated by Pluronic F127: Use of Poloxamer Mixtures and Increased Template/SiO ₂ Ratios in Materials Synthesized by Evaporation-Induced Self-Assembly
journal, December 2014

The Determination of Pore Volume and Area Distributions in Porous Substances. I. Computations from Nitrogen Isotherms
journal, January 1951

Porous Thin Films of Functionalized Mesoporous Silica Nanoparticles
journal, November 2008

Optical Properties of Nanostructured Optical Materials
journal, January 1996

Fabrication of Multilayered Nanoporous Poly(methyl silsesquioxane)
journal, November 2002

Effects of Crystallinity in Spin-On Pure-Silica-Zeolite MFI Low-Dielectric-Constant Films
journal, October 2004

Interspecimen Comparison of the Refractive Index of Fused Silica*,†
journal, January 1965

Reflectance of surfactant-templated mesoporous silica thin films: Simulations versus experiments
journal, February 2010

The Kelvin equation—a review
journal, January 1972

Effective optical properties of highly ordered mesoporous thin films
journal, February 2010

Novel Method of Preparation of Gold-Nanoparticle-Doped TiO2 and SiO2 Plasmonic Thin Films: Optical Characterization and Comparison with Maxwell-Garnett Modeling
journal, July 2011