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Title: High-pressure nuclear inelastic scattering with backscattering monochromatization

Abstract

The capability to perform high-pressure low-temperature nuclear inelastic scattering on125Te and121Sb with a sapphire backscattering monochromator is presented. This technique was applied to measure nuclear inelastic scattering in TeO2at pressures up to 10 GPa and temperatures down to 25 K. The evaluated partial Te densities of phonon states were compared with theoretical calculations and with Raman scattering measured under the same conditions. The high-pressure cell developed in this work can also be used for other techniques at pressures up to at least 100 GPa.

Authors:
 [1];  [1];  [2];  [1];  [1];  [1]; ORCiD logo [3]; ORCiD logo [3]; ORCiD logo [3];  [2]; ORCiD logo [3]
  1. Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
  2. Forschungszentrum Jülich GmbH, Jülich (Germany)
  3. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1560474
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Synchrotron Radiation (Online)
Additional Journal Information:
Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 26; Journal Issue: 5; Journal ID: ISSN 1600-5775
Publisher:
International Union of Crystallography
Country of Publication:
United States
Language:
English
Subject:
73 NUCLEAR PHYSICS AND RADIATION PHYSICS; nuclear inelastic scattering; high pressure; backscattering; nuclear resonance scattering; density of phonon states

Citation Formats

Sergueev, Ilya, Glazyrin, Konstantin, Herrmann, Markus G., Alexeev, Pavel, Wille, Hans -Christian, Leupold, Olaf, May, Andrew F., Pandey, Tribhuwan, Lindsay, Lucas R., Friese, Karen, and Hermann, Raphael P. High-pressure nuclear inelastic scattering with backscattering monochromatization. United States: N. p., 2019. Web. https://doi.org/10.1107/S1600577519008853.
Sergueev, Ilya, Glazyrin, Konstantin, Herrmann, Markus G., Alexeev, Pavel, Wille, Hans -Christian, Leupold, Olaf, May, Andrew F., Pandey, Tribhuwan, Lindsay, Lucas R., Friese, Karen, & Hermann, Raphael P. High-pressure nuclear inelastic scattering with backscattering monochromatization. United States. https://doi.org/10.1107/S1600577519008853
Sergueev, Ilya, Glazyrin, Konstantin, Herrmann, Markus G., Alexeev, Pavel, Wille, Hans -Christian, Leupold, Olaf, May, Andrew F., Pandey, Tribhuwan, Lindsay, Lucas R., Friese, Karen, and Hermann, Raphael P. Fri . "High-pressure nuclear inelastic scattering with backscattering monochromatization". United States. https://doi.org/10.1107/S1600577519008853. https://www.osti.gov/servlets/purl/1560474.
@article{osti_1560474,
title = {High-pressure nuclear inelastic scattering with backscattering monochromatization},
author = {Sergueev, Ilya and Glazyrin, Konstantin and Herrmann, Markus G. and Alexeev, Pavel and Wille, Hans -Christian and Leupold, Olaf and May, Andrew F. and Pandey, Tribhuwan and Lindsay, Lucas R. and Friese, Karen and Hermann, Raphael P.},
abstractNote = {The capability to perform high-pressure low-temperature nuclear inelastic scattering on125Te and121Sb with a sapphire backscattering monochromator is presented. This technique was applied to measure nuclear inelastic scattering in TeO2at pressures up to 10 GPa and temperatures down to 25 K. The evaluated partial Te densities of phonon states were compared with theoretical calculations and with Raman scattering measured under the same conditions. The high-pressure cell developed in this work can also be used for other techniques at pressures up to at least 100 GPa.},
doi = {10.1107/S1600577519008853},
journal = {Journal of Synchrotron Radiation (Online)},
number = 5,
volume = 26,
place = {United States},
year = {2019},
month = {8}
}

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129 Xe nuclear resonance scattering on solid Xe and 129 Xe clathrate hydrate
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From ultrasoft pseudopotentials to the projector augmented-wave method
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Density of phonon states in superconducting FeSe as a function of temperature and pressure
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Raman study of pressure-induced phase transitions in paratellurite (TeO 2 )
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Phonon Density of States Measured by Inelastic Nuclear Resonant Scattering
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Polymorphism and compression of TeO2 at high pressure
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Structure and order parameters in the pressure-induced continuous transition in Te O 2
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Refinement of the Structure of alpha-TeO2.
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The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III
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Thermochemical Ranking and Dynamic Stability of TeO 2 Polymorphs from Ab Initio Theory
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Rocking curve imaging of high quality sapphire crystals in backscattering geometry
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    Works referencing / citing this record:

    Polymorphism and compression of TeO2 at high pressure
    journal, January 1987


    Refinement of the Structure of alpha-TeO2.
    journal, January 1968


    Phonon Density of States Measured by Inelastic Nuclear Resonant Scattering
    journal, May 1995


    Phase-Change Materials: Vibrational Softening upon Crystallization and Its Impact on Thermal Properties
    journal, April 2011

    • Matsunaga, Toshiyuki; Yamada, Noboru; Kojima, Rie
    • Advanced Functional Materials, Vol. 21, Issue 12
    • DOI: 10.1002/adfm.201002274

    Quadrupole splitting and isomer shifts in Te oxides investigated using nuclear forward scattering
    journal, January 2014

    • Klobes, Benedikt; Barrier, Nicolas; Vertruyen, Benedicte
    • Hyperfine Interactions, Vol. 226, Issue 1-3
    • DOI: 10.1007/s10751-013-0993-4

    The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III
    journal, June 2015

    • Liermann, H. -P.; Konôpková, Z.; Morgenroth, W.
    • Journal of Synchrotron Radiation, Vol. 22, Issue 4
    • DOI: 10.1107/s1600577515005937

    Observation of Nuclear Resonant Scattering Accompanied by Phonon Excitation Using Synchrotron Radiation
    journal, May 1995


    Lattice dynamics and structure of GeTe, SnTe and PbTe
    journal, December 2012

    • Bauer Pereira, Paula; Sergueev, Ilya; Gorsse, Stéphane
    • physica status solidi (b), Vol. 250, Issue 7
    • DOI: 10.1002/pssb.201248412

    Nuclear resonant scattering at high pressure and high temperature
    journal, December 2004


    A compact membrane-driven diamond anvil cell and cryostat system for nuclear resonant scattering at high pressure and low temperature
    journal, December 2017

    • Zhao, J. Y.; Bi, W.; Sinogeikin, S.
    • Review of Scientific Instruments, Vol. 88, Issue 12
    • DOI: 10.1063/1.4999787

    Rocking curve imaging of high quality sapphire crystals in backscattering geometry
    journal, January 2017

    • Jafari, A.; Sergueev, I.; Bessas, D.
    • Journal of Applied Physics, Vol. 121, Issue 4
    • DOI: 10.1063/1.4974106

    Thermochemical Ranking and Dynamic Stability of TeO 2 Polymorphs from Ab Initio Theory
    journal, January 2014

    • Deringer, Volker L.; Stoffel, Ralf P.; Dronskowski, Richard
    • Crystal Growth & Design, Vol. 14, Issue 2
    • DOI: 10.1021/cg401822g

    Raman study of pressure-induced phase transitions in paratellurite (TeO 2 )
    journal, May 1992


    Elasticity and lattice dynamics of enstatite at high pressure: ELASTICITY AND LATTICE DYNAMICS OF EN87
    journal, August 2013

    • Zhang, Dongzhou; Jackson, Jennifer M.; Chen, Bin
    • Journal of Geophysical Research: Solid Earth, Vol. 118, Issue 8
    • DOI: 10.1002/jgrb.50303

    Nuclear resonant scattering at PETRA III : Brillant opportunities for nano – and extreme condition science
    journal, March 2010


    121 Sb and 125 Te nuclear inelastic scattering in Sb 2 Te 3 under high pressure
    journal, November 2014


    Phase-change materials for rewriteable data storage
    journal, November 2007

    • Wuttig, Matthias; Yamada, Noboru
    • Nature Materials, Vol. 6, Issue 11
    • DOI: 10.1038/nmat2009

    The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III
    journal, February 2016


    The crystal structure and absolute optical chirality of paratellurite, α-TeO 2
    journal, September 1988


    From ultrasoft pseudopotentials to the projector augmented-wave method
    journal, January 1999


    Nuclear resonant forward scattering of synchrotron radiation from 121 Sb at 37.13 keV
    journal, April 2006


    The Crystal Structure of Tellurite (TeO2).
    journal, January 1940

    • Ito, T.; Sawada, H.
    • Zeitschrift für Kristallographie - Crystalline Materials, Vol. 102, Issue 1-6
    • DOI: 10.1524/zkri.1940.102.1.13

    Complex thermoelectric materials
    journal, February 2008

    • Snyder, G. Jeffrey; Toberer, Eric S.
    • Nature Materials, Vol. 7, Issue 2, p. 105-114
    • DOI: 10.1038/nmat2090

    129 Xe nuclear resonance scattering on solid Xe and 129 Xe clathrate hydrate
    journal, August 2013


    Restoring the Density-Gradient Expansion for Exchange in Solids and Surfaces
    journal, April 2008


    High-pressure nuclear inelastic scattering with backscattering monochromatization
    text, January 2019

    • Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G.
    • Deutsches Elektronen-Synchrotron, DESY, Hamburg
    • DOI: 10.3204/pubdb-2019-03277

    First principles phonon calculations in materials science
    journal, November 2015


    Projector augmented-wave method
    journal, December 1994


    Nuclear resonant inelastic X-ray scattering at high pressure and low temperature
    journal, April 2015


    Nuclear forward and inelastic spectroscopy on 125 Te and Sb 2 125 Te 3
    journal, September 2010


    Efficiency of ab-initio total energy calculations for metals and semiconductors using a plane-wave basis set
    journal, July 1996