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Title: Effect of proton irradiation on anatase TiO2 nanotube anodes for lithium-ion batteries

Abstract

The role of defects in the charge transfer and transport properties of electrode materials for lithium-ion batteries has recently garnered increased interest. It is widely recognized that ion irradiation promotes the formation of defects within a crystalline solid. Among all ion species used for irradiation, protons are expected to create primarily simple Frenkel pair point defects without significantly changing the stoichiometry of the damaged region of the target material. This work investigates the effect of proton irradiation at varying temperatures on the electrochemical properties of anatase TiO2 nanotube (TiO2-NT) electrode for lithium-ion battery applications. Anatase TiO2-NTs are irradiated at both room temperature (25 degrees C) and 250 degrees C and compared with non-irradiated control specimens. Characterization by Raman spectroscopy and XRD suggests that the irradiation at both temperatures does not alter the long-range order of the nanotubes. However, high-resolution TEM reveals that defect clusters are formed upon irradiation and increase in size with increasing temperature. Both irradiated samples exhibit increased capacity and enhanced rate capability compared with the non-irradiated control, which can be explained by increased storage sites as well as improved Li+ diffusivity due to the presence of irradiation-induced defects. This study presents a unique perspective on pathways tomore » engineer functional nanostructured electrode materials by tailoring irradiation conditions.« less

Authors:
 [1];  [1];  [2]; ORCiD logo [3];  [1];  [3];  [4];  [1];  [1];  [5];  [2]; ORCiD logo [1]
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  1. Boise State Univ., ID (United States)
  2. Purdue Univ., West Lafayette, IN (United States)
  3. Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
  4. Argonne National Lab. (ANL), Lemont, IL (United States)
  5. Univ. of Utah, Salt Lake City, UT (United States)
Publication Date:
Research Org.:
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)
Sponsoring Org.:
USDOE Office of Science (SC). Basic Energy Sciences (BES) (SC-22); USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division
OSTI Identifier:
1558076
Alternate Identifier(s):
OSTI ID: 1566146
Report Number(s):
LA-UR-19-26408
Journal ID: ISSN 0022-2461
Grant/Contract Number:  
89233218CNA000001; AC52-06NA25396; AC04-94AL85000; DMR-1408949; DMR-1838604; DMR-1838605; AC02-06CH11357
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Materials Science
Additional Journal Information:
Journal Volume: 54; Journal Issue: 20; Journal ID: ISSN 0022-2461
Publisher:
Springer
Country of Publication:
United States
Language:
English
Subject:
25 ENERGY STORAGE; 36 MATERIALS SCIENCE; nanotube; proton irradiation; charge transfer and transport; defects; lithium-ion battery anode

Citation Formats

Smith, Kassiopeia A., Savva, Andreas I., Mao, Keyou S., Wang, Yongqiang, Tenne, Dmitri A., Chen, Di, Liu, Yuzi, Barnes, Pete, Deng, Changjian, Butt, Darryl P., Wharry, Janelle P., and Xiong, Hui. Effect of proton irradiation on anatase TiO2 nanotube anodes for lithium-ion batteries. United States: N. p., 2019. Web. doi:10.1007/s10853-019-03825-w.
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Smith, Kassiopeia A., Savva, Andreas I., Mao, Keyou S., Wang, Yongqiang, Tenne, Dmitri A., Chen, Di, Liu, Yuzi, Barnes, Pete, Deng, Changjian, Butt, Darryl P., Wharry, Janelle P., & Xiong, Hui. Effect of proton irradiation on anatase TiO2 nanotube anodes for lithium-ion batteries. United States. https://doi.org/10.1007/s10853-019-03825-w
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Smith, Kassiopeia A., Savva, Andreas I., Mao, Keyou S., Wang, Yongqiang, Tenne, Dmitri A., Chen, Di, Liu, Yuzi, Barnes, Pete, Deng, Changjian, Butt, Darryl P., Wharry, Janelle P., and Xiong, Hui. Thu . "Effect of proton irradiation on anatase TiO2 nanotube anodes for lithium-ion batteries". United States. https://doi.org/10.1007/s10853-019-03825-w. https://www.osti.gov/servlets/purl/1558076.
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@article{osti_1558076,
title = {Effect of proton irradiation on anatase TiO2 nanotube anodes for lithium-ion batteries},
author = {Smith, Kassiopeia A. and Savva, Andreas I. and Mao, Keyou S. and Wang, Yongqiang and Tenne, Dmitri A. and Chen, Di and Liu, Yuzi and Barnes, Pete and Deng, Changjian and Butt, Darryl P. and Wharry, Janelle P. and Xiong, Hui},
abstractNote = {The role of defects in the charge transfer and transport properties of electrode materials for lithium-ion batteries has recently garnered increased interest. It is widely recognized that ion irradiation promotes the formation of defects within a crystalline solid. Among all ion species used for irradiation, protons are expected to create primarily simple Frenkel pair point defects without significantly changing the stoichiometry of the damaged region of the target material. This work investigates the effect of proton irradiation at varying temperatures on the electrochemical properties of anatase TiO2 nanotube (TiO2-NT) electrode for lithium-ion battery applications. Anatase TiO2-NTs are irradiated at both room temperature (25 degrees C) and 250 degrees C and compared with non-irradiated control specimens. Characterization by Raman spectroscopy and XRD suggests that the irradiation at both temperatures does not alter the long-range order of the nanotubes. However, high-resolution TEM reveals that defect clusters are formed upon irradiation and increase in size with increasing temperature. Both irradiated samples exhibit increased capacity and enhanced rate capability compared with the non-irradiated control, which can be explained by increased storage sites as well as improved Li+ diffusivity due to the presence of irradiation-induced defects. This study presents a unique perspective on pathways to engineer functional nanostructured electrode materials by tailoring irradiation conditions.},
doi = {10.1007/s10853-019-03825-w},
journal = {Journal of Materials Science},
number = 20,
volume = 54,
place = {United States},
year = {2019},
month = {7}
}
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https://doi.org/10.1007/s10853-019-03825-w
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Cited by: 12 works
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Figures / Tables:

Figure 1 Figure 1: Damage depth profile of H+ ions on anatase TiO2 by SRIM calculation.
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