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Title: Improving microstructural quantification in FIB/SEM nanotomography

Authors:
; ; ; ;
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1549711
Grant/Contract Number:  
DGE1322106; DEFE0009084
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Ultramicroscopy
Additional Journal Information:
Journal Name: Ultramicroscopy Journal Volume: 184 Journal Issue: PA; Journal ID: ISSN 0304-3991
Publisher:
Elsevier
Country of Publication:
Netherlands
Language:
English

Citation Formats

Taillon, Joshua A., Pellegrinelli, Christopher, Huang, Yi-Lin, Wachsman, Eric D., and Salamanca-Riba, Lourdes G. Improving microstructural quantification in FIB/SEM nanotomography. Netherlands: N. p., 2018. Web. doi:10.1016/j.ultramic.2017.07.017.
Taillon, Joshua A., Pellegrinelli, Christopher, Huang, Yi-Lin, Wachsman, Eric D., & Salamanca-Riba, Lourdes G. Improving microstructural quantification in FIB/SEM nanotomography. Netherlands. https://doi.org/10.1016/j.ultramic.2017.07.017
Taillon, Joshua A., Pellegrinelli, Christopher, Huang, Yi-Lin, Wachsman, Eric D., and Salamanca-Riba, Lourdes G. Mon . "Improving microstructural quantification in FIB/SEM nanotomography". Netherlands. https://doi.org/10.1016/j.ultramic.2017.07.017.
@article{osti_1549711,
title = {Improving microstructural quantification in FIB/SEM nanotomography},
author = {Taillon, Joshua A. and Pellegrinelli, Christopher and Huang, Yi-Lin and Wachsman, Eric D. and Salamanca-Riba, Lourdes G.},
abstractNote = {},
doi = {10.1016/j.ultramic.2017.07.017},
journal = {Ultramicroscopy},
number = PA,
volume = 184,
place = {Netherlands},
year = {Mon Jan 01 00:00:00 EST 2018},
month = {Mon Jan 01 00:00:00 EST 2018}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1016/j.ultramic.2017.07.017

Citation Metrics:
Cited by: 24 works
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Works referenced in this record:

Image-based characterization of cement pore structure using wood’s metal intrusion
journal, December 1998


Three-Dimensional Reconstruction of Porous LSCF Cathodes
journal, January 2007

  • Gostovic, D.; Smith, J. R.; Kundinger, D. P.
  • Electrochemical and Solid-State Letters, Vol. 10, Issue 12
  • DOI: 10.1149/1.2794672

The relationship between overpotential and the three phase boundary length
journal, July 1996


Quantitative relationships between microstructure and effective transport properties based on virtual materials testing
journal, February 2014

  • Gaiselmann, Gerd; Neumann, Matthias; Schmidt, Volker
  • AIChE Journal, Vol. 60, Issue 6
  • DOI: 10.1002/aic.14416

Reconstruction of porous electrodes by FIB/SEM for detailed microstructure modeling
journal, September 2011


FIB-Nanotomography of Particulate Systems—Part I: Particle Shape and Topology of Interfaces
journal, August 2006


High-resolution three-dimensional reconstruction: A combined scanning electron microscope and focused ion-beam approach
journal, January 2006

  • Bansal, R. K.; Kubis, A.; Hull, R.
  • Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures, Vol. 24, Issue 2
  • DOI: 10.1116/1.2167987

Evaluation of the relationship between cathode microstructure and electrochemical behavior for SOFCs
journal, February 2009


3D determination of grain shape in a FeAl-based nanocomposite by 3D FIB tomography
journal, October 2001


Polarization Effects in Intermediate Temperature, Anode-Supported Solid Oxide Fuel Cells
journal, January 1999

  • Kim, Jai-Woh
  • Journal of The Electrochemical Society, Vol. 146, Issue 1
  • DOI: 10.1149/1.1391566

3D Microstructural characterization of a solid oxide fuel cell anode reconstructed by focused ion beam tomography
journal, September 2011


Three Dimensional Microstructural Characterization of Cathode Degradation in SOFCs Using FIB/SEM and TEM
journal, August 2015

  • Taillon, Joshua; Pellegrinelli, Christopher; Huang, Yilin
  • Microscopy and Microanalysis, Vol. 21, Issue S3
  • DOI: 10.1017/S1431927615011587

Practical methods for measuring the tortuosity of porous materials from binary or gray-tone tomographic reconstructions
journal, August 2009

  • Gommes, Cedric J.; Bons, Anton-Jan; Blacher, Silvia
  • AIChE Journal, Vol. 55, Issue 8
  • DOI: 10.1002/aic.11812

Quantification of double-layer Ni/YSZ fuel cell anodes from focused ion beam tomography data
journal, January 2014


Advancing FIB assisted 3D EBSD using a static sample setup
journal, February 2016


Three-dimensional reconstruction of a solid-oxide fuel-cell anode
journal, June 2006

  • Wilson, James R.; Kobsiriphat, Worawarit; Mendoza, Roberto
  • Nature Materials, Vol. 5, Issue 7
  • DOI: 10.1038/nmat1668

Non-Local Means Denoising
journal, January 2011


Three-dimensional chemical analysis of laser-welded NiTi–stainless steel wires using a dual-beam FIB
journal, May 2013


Solid Oxide Fuel Cell Ni–YSZ Anodes: Effect of Composition on Microstructure and Performance
journal, January 2008

  • Wilson, James R.; Barnett, Scott A.
  • Electrochemical and Solid-State Letters, Vol. 11, Issue 10
  • DOI: 10.1149/1.2960528

Numerical Assessment of SOFC Anode Polarization Based on Three-Dimensional Model Microstructure Reconstructed from FIB-SEM Images
journal, January 2010

  • Shikazono, Naoki; Kanno, Daisuke; Matsuzaki, Katsuhisa
  • Journal of The Electrochemical Society, Vol. 157, Issue 5
  • DOI: 10.1149/1.3330568

Quantitative three-dimensional microstructure of a solid oxide fuel cell cathode
journal, May 2009

  • Wilson, James R.; Duong, Anh T.; Gameiro, Marcio
  • Electrochemistry Communications, Vol. 11, Issue 5, p. 1052-1056
  • DOI: 10.1016/j.elecom.2009.03.010

Quantification of SOFC anode microstructure based on dual beam FIB-SEM technique
journal, February 2010


scikit-image: image processing in Python
journal, January 2014

  • van der Walt, Stéfan; Schönberger, Johannes L.; Nunez-Iglesias, Juan
  • PeerJ, Vol. 2
  • DOI: 10.7717/peerj.453

Watersheds in digital spaces: an efficient algorithm based on immersion simulations
journal, June 1991

  • Vincent, L.; Soille, P.
  • IEEE Transactions on Pattern Analysis and Machine Intelligence, Vol. 13, Issue 6
  • DOI: 10.1109/34.87344

Three-dimensional analysis of porous BaTiO3 ceramics using FIB nanotomography
journal, October 2004


Automated three-dimensional X-ray analysis using a dual-beam FIB
journal, August 2007


Computation of TPB length, surface area and pore size from numerical reconstruction of composite solid oxide fuel cell electrodes
journal, April 2009


Effect of Firing Temperature on LSM-YSZ Composite Cathodes: A Combined Three-Dimensional Microstructure and Impedance Spectroscopy Study
journal, January 2012

  • Scott Cronin, J.; Muangnapoh, Kullachate; Patterson, Zach
  • Journal of The Electrochemical Society, Vol. 159, Issue 4
  • DOI: 10.1149/2.053204jes

Predicting effective conductivities based on geometric microstructure characteristics
journal, January 2016

  • Stenzel, Ole; Pecho, Omar; Holzer, Lorenz
  • AIChE Journal, Vol. 62, Issue 5
  • DOI: 10.1002/aic.15160

Fiji: an open-source platform for biological-image analysis
journal, June 2012

  • Schindelin, Johannes; Arganda-Carreras, Ignacio; Frise, Erwin
  • Nature Methods, Vol. 9, Issue 7
  • DOI: 10.1038/nmeth.2019

Stripe and ring artifact removal with combined wavelet—Fourier filtering
journal, January 2009

  • Münch, Beat; Trtik, Pavel; Marone, Federica
  • Optics Express, Vol. 17, Issue 10
  • DOI: 10.1364/OE.17.008567

Durability Testing of Solid Oxide Cell Electrodes with Current Switching
journal, January 2012

  • Hughes, Gareth A.; Yakal-Kremski, Kyle; Call, Ann V.
  • Journal of The Electrochemical Society, Vol. 159, Issue 12
  • DOI: 10.1149/2.008301jes

Studies of Solid Oxide Fuel Cell Electrode Evolution Using 3D Tomography
journal, March 2013

  • Yakal-Kremski, K.; Cronin, J. S.; Chen-Wiegart, Y. -C. K.
  • Fuel Cells, Vol. 13, Issue 4
  • DOI: 10.1002/fuce.201200177

A survey on skeletonization algorithms and their applications
journal, June 2016


Morphological segmentation of FIB-SEM data of highly porous media: MORPHOLOGICAL SEGMENTATION OF FIB-SEM DATA OF HIGHLY POROUS MEDIA
journal, April 2013

  • Prill, T.; Schladitz, K.; Jeulin, D.
  • Journal of Microscopy, Vol. 250, Issue 2
  • DOI: 10.1111/jmi.12021

Three-Dimensional Analysis of Solid Oxide Fuel Cell Ni-YSZ Anode Interconnectivity
journal, January 2009

  • Wilson, James R.; Gameiro, Marcio; Mischaikow, Konstantin
  • Microscopy and Microanalysis, Vol. 15, Issue 1
  • DOI: 10.1017/S1431927609090096

Distance-Ordered Homotopic Thinning: A Skeletonization Algorithm for 3D Digital Images
journal, December 1998


Block lift-out sample preparation for 3D experiments in a dual beam focused ion beam microscope
journal, September 2007


Rock characterization of Fayetteville shale gas plays
journal, March 2013


Control of charging in low-voltage SEM
journal, January 1989


Implementation of a 3D thinning algorithm
journal, October 2007


Adsorption of Gases in Multimolecular Layers
journal, February 1938

  • Brunauer, Stephen; Emmett, P. H.; Teller, Edward
  • Journal of the American Chemical Society, Vol. 60, Issue 2, p. 309-319
  • DOI: 10.1021/ja01269a023

The NumPy Array: A Structure for Efficient Numerical Computation
journal, March 2011

  • van der Walt, Stéfan; Colbert, S. Chris; Varoquaux, Gaël
  • Computing in Science & Engineering, Vol. 13, Issue 2
  • DOI: 10.1109/MCSE.2011.37

Three Dimensional Microstructural Characterization of Cathode Degradation in SOFCs Using Focused Ion Beam and SEM
journal, March 2014

  • Taillon, Joshua A.; Pellegrinelli, Christopher; Huang, Yilin
  • ECS Transactions, Vol. 61, Issue 1
  • DOI: 10.1149/06101.0109ecst

A pyramid approach to subpixel registration based on intensity
journal, January 1998

  • Thevenaz, P.; Ruttimann, U. E.; Unser, M.
  • IEEE Transactions on Image Processing, Vol. 7, Issue 1
  • DOI: 10.1109/83.650848