Bi-continuous pattern formation in thin films via solid-state interfacial dealloying studied by multimodal characterization

Zhao, Chonghang; Kisslinger, Kim; Huang, Xiaojing; Lu, Ming; Camino, Fernando; Lin, Cheng -Hung; Yan, Hanfei; Nazaretski, Evgeny; Chu, Yong; Ravel, Bruce; Liu, Mingzhao; Chen-Wiegart, Yu-chen Karen

doi:10.1039/C9MH00669A

Title: Bi-continuous pattern formation in thin films via solid-state interfacial dealloying studied by multimodal characterization

Journal Article · 19 June 2019 · Materials Horizons

DOI: https://doi.org/10.1039/C9MH00669A · OSTI ID:1542282

^[1]; Kisslinger, Kim ^[2]; Huang, Xiaojing ^[2]; Lu, Ming ^[2]; Camino, Fernando ^[2]; Lin, Cheng -Hung ^[1]; Yan, Hanfei ^[2];

^[2]; Chu, Yong ^[2]; Ravel, Bruce ^[3];

^[2];

^[4]

Stony Brook Univ., Stony Brook, NY (United States)
Brookhaven National Lab. (BNL), Upton, NY (United States)
National Inst. of Standards and Technology (NIST), Gaithersburg, MD (United States)
Stony Brook Univ., Stony Brook, NY (United States); Brookhaven National Lab. (BNL), Upton, NY (United States)

Solid-state interfacial dealloying creates bi-continuous nanostructured thin films with 3D interconnected morphology, revealed by multimodal characterization, offering potential applications in catalysis, biomedical sensing and energy storage.

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Research Organization:: Brookhaven National Laboratory (BNL), Upton, NY (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE

Grant/Contract Number:: SC0012704

OSTI ID:: 1542282

Alternate ID(s):: OSTI ID: 1529999

Report Number(s):: BNL-211848-2019-JAAM; MHAOAL

Journal Information:: Materials Horizons, Vol. 6, Issue 10; ISSN 2051-6347

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 22 works

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Web of Science

References (61)

Structural evolution of nanoporous gold during thermal coarsening Chen-Wiegart, Yu-chen Karen; Wang, Steve; Chu, Yong S. Acta Materialia, Vol. 60, Issue 12 https://doi.org/10.1016/j.actamat.2012.05.012	journal	July 2012
Data set for diffusion coefficients of alloying elements in dilute Mg alloys from first-principles Zhou, Bi-Cheng; Shang, Shun-Li; Wang, Yi Data in Brief, Vol. 5 https://doi.org/10.1016/j.dib.2015.10.024	journal	December 2015
Dealloying by metallic melt Wada, Takeshi; Yubuta, Kunio; Inoue, Akihisa Materials Letters, Vol. 65, Issue 7 https://doi.org/10.1016/j.matlet.2011.01.054	journal	April 2011
Classification of Bulk Metallic Glasses by Atomic Size Difference, Heat of Mixing and Period of Constituent Elements and Its Application to Characterization of the Main Alloying Element Takeuchi, Akira; Inoue, Akihisa MATERIALS TRANSACTIONS, Vol. 46, Issue 12 https://doi.org/10.2320/matertrans.46.2817	journal	January 2005
Transition metals in silicon Weber, Eicke R. Applied Physics A Solids and Surfaces, Vol. 30, Issue 1 https://doi.org/10.1007/BF00617708	journal	January 1983
Fly-scan ptychography Huang, Xiaojing; Lauer, Kenneth; Clark, Jesse N. Scientific Reports, Vol. 5, Issue 1 https://doi.org/10.1038/srep09074	journal	March 2015
Three-dimensional open-cell macroporous iron, chromium and ferritic stainless steel Wada, Takeshi; Kato, Hidemi Scripta Materialia, Vol. 68, Issue 9 https://doi.org/10.1016/j.scriptamat.2013.01.011	journal	May 2013
Three-Dimensional Morphological and Chemical Evolution of Nanoporous Stainless Steel by Liquid Metal Dealloying Zhao, Chonghang; Wada, Takeshi; De Andrade, Vincent ACS Applied Materials & Interfaces, Vol. 9, Issue 39 https://doi.org/10.1021/acsami.7b04659	journal	April 2017
Kinetics of formation and coarsening of nanoporous α-titanium dealloyed with Mg melt Tsuda, Masashi; Wada, Takeshi; Kato, Hidemi Journal of Applied Physics, Vol. 114, Issue 11 https://doi.org/10.1063/1.4821066	journal	September 2013
NIH Image to ImageJ: 25 years of image analysis Schneider, Caroline A.; Rasband, Wayne S.; Eliceiri, Kevin W. Nature Methods, Vol. 9, Issue 7 https://doi.org/10.1038/nmeth.2089	journal	June 2012
Comparison of the agglomeration behavior of Au and Cu films sputter deposited on silicon dioxide Kwon, Jang-Yeon; Yoon, Tae-Sik; Kim, Ki-Bum Journal of Applied Physics, Vol. 93, Issue 6 https://doi.org/10.1063/1.1556178	journal	March 2003
Effect of Ag–Au composition and acid concentration on dealloying front velocity and cracking during nanoporous gold formation Chen-Wiegart, Yu-chen Karen; Wang, Steve; McNulty, Ian Acta Materialia, Vol. 61, Issue 15 https://doi.org/10.1016/j.actamat.2013.05.039	journal	September 2013
Stability of thin platinum films implemented in high-temperature microdevices Tiggelaar, R. M.; Sanders, R. G. P.; Groenland, A. W. Sensors and Actuators A: Physical, Vol. 152, Issue 1 https://doi.org/10.1016/j.sna.2009.03.017	journal	May 2009
Prominent Electron Penetration through Ultrathin Graphene Layer from FeNi Alloy for Efficient Reduction of CO ₂ to CO Bi, Qingyuan; Wang, Xin; Gu, Feng ChemSusChem, Vol. 10, Issue 15 https://doi.org/10.1002/cssc.201700787	journal	July 2017
Intermetallic compound formation in thin‐film and in bulk samples of the Ni‐Si binary system Tu, K. N.; Ottaviani, G.; Gösele, U. Journal of Applied Physics, Vol. 54, Issue 2 https://doi.org/10.1063/1.332034	journal	February 1983
Volume Change during the Formation of Nanoporous Gold by Dealloying Parida, S.; Kramer, D.; Volkert, C. A. Physical Review Letters, Vol. 97, Issue 3 https://doi.org/10.1103/PhysRevLett.97.035504	journal	July 2006
Evolution of a bicontinuous nanostructure via a solid-state interfacial dealloying reaction Wada, Takeshi; Yubuta, Kunio; Kato, Hidemi Scripta Materialia, Vol. 118 https://doi.org/10.1016/j.scriptamat.2016.03.008	journal	June 2016
The dominant diffusing species and initial phase formation in Al‐Cu, Mg‐Cu, and Mg‐Ni systems Hong, Q. Z.; d’Heurle, F. M. Journal of Applied Physics, Vol. 72, Issue 9 https://doi.org/10.1063/1.352258	journal	November 1992
Diffusion coefficients of alloying elements in dilute Mg alloys: A comprehensive first-principles study Zhou, Bi-Cheng; Shang, Shun-Li; Wang, Yi Acta Materialia, Vol. 103 https://doi.org/10.1016/j.actamat.2015.10.010	journal	January 2016
Diffusion of Aluminum, Magnesium, Silicon, and Zirconium in Nickel Allison, Herbert W.; Samelson, Harold Journal of Applied Physics, Vol. 30, Issue 9 https://doi.org/10.1063/1.1735346	journal	September 1959
Investigation of high-temperature degradation of platinum thin films with an in situ resistance measurement apparatus Firebaugh, S. L.; Jensen, K. F.; Schmidt, M. A. Journal of Microelectromechanical Systems, Vol. 7, Issue 1, p. 128-135 https://doi.org/10.1109/84.661395	journal	March 1998
Solid-State Dewetting of Thin Films Thompson, Carl V. Annual Review of Materials Research, Vol. 42, Issue 1 https://doi.org/10.1146/annurev-matsci-070511-155048	journal	August 2012
ATHENA , ARTEMIS , HEPHAESTUS : data analysis for X-ray absorption spectroscopy using IFEFFIT Ravel, B.; Newville, M. Journal of Synchrotron Radiation, Vol. 12, Issue 4 https://doi.org/10.1107/S0909049505012719	journal	June 2005
3D morphological evolution of porous titanium by x-ray micro- and nano-tomography Chen-Wiegart, Yu-chen Karen; Wada, Takeshi; Butakov, Nikita Journal of Materials Research, Vol. 28, Issue 17 https://doi.org/10.1557/jmr.2013.151	journal	June 2013
Alloy Design Criteria for Solid Metal Dealloying of Thin Films McCue, Ian; Demkowicz, Michael J. JOM, Vol. 69, Issue 11 https://doi.org/10.1007/s11837-017-2571-8	journal	September 2017
Reconstructing a Nanoporous Metal in Three Dimensions: An Electron Tomography Study of Dealloyed Gold Leaf Rösner, H.; Parida, S.; Kramer, D. Advanced Engineering Materials, Vol. 9, Issue 7 https://doi.org/10.1002/adem.200700063	journal	July 2007
Quantitative size-factors for metallic solid solutions King, H. W. Journal of Materials Science, Vol. 1, Issue 1 https://doi.org/10.1007/BF00549722	journal	February 1966
Structural changes during the reaction of Ni thin films with (100) silicon substrates Thron, Andrew M.; Greene, Peter K.; Liu, Kai Acta Materialia, Vol. 60, Issue 6-7 https://doi.org/10.1016/j.actamat.2012.01.033	journal	April 2012
Pattern formation during electrochemical and liquid metal dealloying McCue, Ian; Karma, Alain; Erlebacher, Jonah MRS Bulletin, Vol. 43, Issue 1 https://doi.org/10.1557/mrs.2017.301	journal	January 2018
Oxygen reduction in nanoporous metal–ionic liquid composite electrocatalysts Snyder, J.; Fujita, T.; Chen, M. W. Nature Materials, Vol. 9, Issue 11 https://doi.org/10.1038/nmat2878	journal	October 2010
Mechanism of Coarsening and Bubble Formation in High-Genus Nanoporous Metals Erlebacher, J. Physical Review Letters, Vol. 106, Issue 22 https://doi.org/10.1103/PhysRevLett.106.225504	journal	June 2011
Coarsening by network restructuring in model nanoporous gold Kolluri, Kedarnath; Demkowicz, Michael J. Acta Materialia, Vol. 59, Issue 20 https://doi.org/10.1016/j.actamat.2011.08.037	journal	December 2011
Vegard’s law Denton, A. R.; Ashcroft, N. W. Physical Review A, Vol. 43, Issue 6 https://doi.org/10.1103/PhysRevA.43.3161	journal	March 1991
Characterization of Nanoporous Materials with Atom Probe Tomography Pfeiffer, Björn; Erichsen, Torben; Epler, Eike Microscopy and Microanalysis, Vol. 21, Issue 3 https://doi.org/10.1017/S1431927615000501	journal	May 2015
Imaging of 3D morphological evolution of nanoporous silicon anode in lithium ion battery by X-ray nano-tomography Zhao, Chonghang; Wada, Takeshi; De Andrade, Vincent Nano Energy, Vol. 52 https://doi.org/10.1016/j.nanoen.2018.08.009	journal	October 2018
Three-dimensional bicontinuous porous graphite generated in low temperature metallic liquid Yu, Seung-Geun; Yubuta, Kunio; Wada, Takeshi Carbon, Vol. 96 https://doi.org/10.1016/j.carbon.2015.09.093	journal	January 2016
Bulk-Nanoporous-Silicon Negative Electrode with Extremely High Cyclability for Lithium-Ion Batteries Prepared Using a Top-Down Process Wada, Takeshi; Ichitsubo, Tetsu; Yubuta, Kunio Nano Letters, Vol. 14, Issue 8 https://doi.org/10.1021/nl501500g	journal	July 2014
Decoupling the role of stress and corrosion in the intergranular cracking of noble-metal alloys Badwe, N.; Chen, X.; Schreiber, D. K. Nature Materials, Vol. 17, Issue 10 https://doi.org/10.1038/s41563-018-0162-x	journal	September 2018
TomoPy: a framework for the analysis of synchrotron tomographic data Gürsoy, Dogˇa; De Carlo, Francesco; Xiao, Xianghui Journal of Synchrotron Radiation, Vol. 21, Issue 5 https://doi.org/10.1107/S1600577514013939	journal	August 2014
Evolution of nanoporosity in dealloying Erlebacher, Jonah; Aziz, Michael J.; Karma, Alain Nature, Vol. 410, Issue 6827, p. 450-453 https://doi.org/10.1038/35068529	journal	March 2001
Topology-generating interfacial pattern formation during liquid metal dealloying Geslin, Pierre-Antoine; McCue, Ian; Gaskey, Bernard Nature Communications, Vol. 6, Issue 1 https://doi.org/10.1038/ncomms9887	journal	November 2015
Experimental investigation and thermodynamic calculation of the Fe–Mg–Mn and Fe–Mg–Ni systems Wang, Peisheng; Zhao, Jingrui; Du, Yong International Journal of Materials Research, Vol. 102, Issue 1 https://doi.org/10.3139/146.110442	journal	January 2011
In situ imaging of dealloying during nanoporous gold formation by transmission X-ray microscopy Chen-Wiegart, Yu-chen Karen; Wang, Steve; Lee, Wah-Keat Acta Materialia, Vol. 61, Issue 4 https://doi.org/10.1016/j.actamat.2012.10.017	journal	February 2013
Influence of buffer layers on Ni thin film structure and graphene growth by CVD Ozceri, Elif; Selamet, Yusuf Journal of Physics D: Applied Physics, Vol. 48, Issue 45 https://doi.org/10.1088/0022-3727/48/45/455302	journal	October 2015
Kinetics and morphological evolution of liquid metal dealloying McCue, Ian; Gaskey, Bernard; Geslin, Pierre-Antoine Acta Materialia, Vol. 115 https://doi.org/10.1016/j.actamat.2016.05.032	journal	August 2016
High-throughput ab-initio dilute solute diffusion database Wu, Henry; Mayeshiba, Tam; Morgan, Dane Scientific Data, Vol. 3, Issue 1 https://doi.org/10.1038/sdata.2016.54	journal	July 2016
Morphological and topological analysis of coarsened nanoporous gold by x-ray nanotomography Chen, Yu-chen Karen; Chu, Yong S.; Yi, JaeMock Applied Physics Letters, Vol. 96, Issue 4 https://doi.org/10.1063/1.3285175	journal	January 2010
Nanoporous Gold Catalysts for Selective Gas-Phase Oxidative Coupling of Methanol at Low Temperature Wittstock, A.; Zielasek, V.; Biener, J. Science, Vol. 327, Issue 5963 https://doi.org/10.1126/science.1183591	journal	January 2010
Length scales in alloy dissolution and measurement of absolute interfacial free energy Rugolo, J.; Erlebacher, J.; Sieradzki, K. Nature Materials, Vol. 5, Issue 12 https://doi.org/10.1038/nmat1780	journal	November 2006
Interfacial reaction and the dominant diffusing species in Mg–Ni system Tsai, M. Y.; Chou, M. H.; Kao, C. R. Journal of Alloys and Compounds, Vol. 471, Issue 1-2 https://doi.org/10.1016/j.jallcom.2008.03.124	journal	March 2009
High-Performance Multi-Mode Ptychography Reconstruction on Distributed GPUs Dong, Zhihua; Fang, Yao-Lung L.; Huang, Xiaojing 2018 New York Scientific Data Summit (NYSDS) https://doi.org/10.1109/nysds.2018.8538964	conference	August 2018
Surface and bulk diffusion of adsorbed nickel on ultrathin thermally grown silicon dioxide Mayer, J. T.; Lin, R. F.; Garfunkel, E. Surface Science, Vol. 265, Issue 1-3 https://doi.org/10.1016/0039-6028(92)90491-N	journal	April 1992
Design and performance of an X-ray scanning microscope at the Hard X-ray Nanoprobe beamline of NSLS-II Nazaretski, E.; Yan, H.; Lauer, K. Journal of Synchrotron Radiation, Vol. 24, Issue 6 https://doi.org/10.1107/S1600577517011183	journal	October 2017
Nickel: A very fast diffuser in silicon Lindroos, J.; Fenning, D. P.; Backlund, D. J. Journal of Applied Physics, Vol. 113, Issue 20 https://doi.org/10.1063/1.4807799	journal	May 2013
Fabrication, formation mechanism and properties of three-dimensional nanoporous titanium dealloyed in metallic powders Zhang, Faming; Li, Ping; Yu, Jin Journal of Materials Research, Vol. 32, Issue 8 https://doi.org/10.1557/jmr.2017.19	journal	February 2017
A pyramid approach to subpixel registration based on intensity Thevenaz, P.; Ruttimann, U. E.; Unser, M. IEEE Transactions on Image Processing, Vol. 7, Issue 1 https://doi.org/10.1109/83.650848	journal	January 1998
Are Nanoporous Materials Radiation Resistant? Bringa, E. M.; Monk, J. D.; Caro, A. Nano Letters, Vol. 12, Issue 7 https://doi.org/10.1021/nl201383u	journal	June 2011
TomoPy: A framework for the analysis of synchrotron tomographic data Gürsoy, Doğa; De Carlo, Francesco; Xiao, Xianghui SPIE Optical Engineering + Applications, SPIE Proceedings https://doi.org/10.1117/12.2061373	conference	September 2014
High-Throughput ab-initio Dilute Solute Diffusion Database Wu, Henry; Mayeshiba, Tam; Morgan, Dane arXiv https://doi.org/10.48550/arxiv.1602.01725	text	January 2016
High-Performance Multi-Mode Ptychography Reconstruction on Distributed GPUs Dong, Zhihua; Fang, Yao-Lung L.; Huang, Xiaojing arXiv https://doi.org/10.48550/arxiv.1808.10375	text	January 2018
Evolution of Nanoporosity in Dealloying Erlebacher, Jonah; Aziz, Michael J.; Karma, Alain arXiv https://doi.org/10.48550/arxiv.cond-mat/0103615	text	January 2001