New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments
Abstract
Fast compression experiments performed using dynamic diamond anvil cells (dDACs) employing piezoactuators offer the opportunity to study compression-rate dependent phenomena. In this paper, we describe an experimental setup which allows us to perform time-resolved x-ray diffraction during the fast compression of materials using improved dDACs. The combination of the high flux available using a 25.6 keV x-ray beam focused with a linear array of compound refractive lenses and the two fast GaAs LAMBDA detectors available at the Extreme Conditions Beamline (P02.2) at PETRA III enables the collection of x-ray diffraction patterns at an effective repetition rate of up to 4 kHz. Compression rates of up to 160 TPa/s have been achieved during the compression of gold in a 2.5 ms fast compression using improved dDAC configurations with more powerful piezoactuators. The application of this setup to low-Z compounds at lower compression rates is described, and the high temporal resolution of the setup is demonstrated. The possibility of applying finely tuned pressure profiles opens opportunities for future research, such as using oscillations of the piezoactuator to mimic propagation of seismic waves in the Earth.
- Authors:
-
[1];
[2];
[1];
[1];
[2];
[5];
[1]
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
- Univ. of Oxford (United Kingdom)
- Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); European X-ray Free-Electron Laser (XFEL), Schenefeld (Germany)
- Univ. of Frankfurt, Frankfurt (Germany)
- European Synchrotron Radiation Facility (ESRF), Grenoble (France)
- Publication Date:
- Research Org.:
- Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
- Sponsoring Org.:
- USDOE National Nuclear Security Administration (NNSA)
- OSTI Identifier:
- 1532620
- Alternate Identifier(s):
- OSTI ID: 1528659
- Report Number(s):
- LLNL-JRNL-772752
Journal ID: ISSN 0034-6748; 962704
- Grant/Contract Number:
- AC52-07NA27344
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 90; Journal Issue: 6; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS; Physics
Citation Formats
Jenei, Zs., Liermann, H. P., Husband, R., Méndez, A. S. J., Pennicard, D., Marquardt, H., O’Bannon, E. F., Pakhomova, A., Konopkova, Z., Glazyrin, K., Wendt, M., Wenz, S., McBride, E. E., Morgenroth, W., Winkler, B., Rothkirch, A., Hanfland, M., and Evans, W. J. New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments. United States: N. p., 2019.
Web. doi:10.1063/1.5098993.
Jenei, Zs., Liermann, H. P., Husband, R., Méndez, A. S. J., Pennicard, D., Marquardt, H., O’Bannon, E. F., Pakhomova, A., Konopkova, Z., Glazyrin, K., Wendt, M., Wenz, S., McBride, E. E., Morgenroth, W., Winkler, B., Rothkirch, A., Hanfland, M., & Evans, W. J. New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments. United States. https://doi.org/10.1063/1.5098993
Jenei, Zs., Liermann, H. P., Husband, R., Méndez, A. S. J., Pennicard, D., Marquardt, H., O’Bannon, E. F., Pakhomova, A., Konopkova, Z., Glazyrin, K., Wendt, M., Wenz, S., McBride, E. E., Morgenroth, W., Winkler, B., Rothkirch, A., Hanfland, M., and Evans, W. J. Fri .
"New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments". United States. https://doi.org/10.1063/1.5098993. https://www.osti.gov/servlets/purl/1532620.
@article{osti_1532620,
title = {New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments},
author = {Jenei, Zs. and Liermann, H. P. and Husband, R. and Méndez, A. S. J. and Pennicard, D. and Marquardt, H. and O’Bannon, E. F. and Pakhomova, A. and Konopkova, Z. and Glazyrin, K. and Wendt, M. and Wenz, S. and McBride, E. E. and Morgenroth, W. and Winkler, B. and Rothkirch, A. and Hanfland, M. and Evans, W. J.},
abstractNote = {Fast compression experiments performed using dynamic diamond anvil cells (dDACs) employing piezoactuators offer the opportunity to study compression-rate dependent phenomena. In this paper, we describe an experimental setup which allows us to perform time-resolved x-ray diffraction during the fast compression of materials using improved dDACs. The combination of the high flux available using a 25.6 keV x-ray beam focused with a linear array of compound refractive lenses and the two fast GaAs LAMBDA detectors available at the Extreme Conditions Beamline (P02.2) at PETRA III enables the collection of x-ray diffraction patterns at an effective repetition rate of up to 4 kHz. Compression rates of up to 160 TPa/s have been achieved during the compression of gold in a 2.5 ms fast compression using improved dDAC configurations with more powerful piezoactuators. The application of this setup to low-Z compounds at lower compression rates is described, and the high temporal resolution of the setup is demonstrated. The possibility of applying finely tuned pressure profiles opens opportunities for future research, such as using oscillations of the piezoactuator to mimic propagation of seismic waves in the Earth.},
doi = {10.1063/1.5098993},
journal = {Review of Scientific Instruments},
number = 6,
volume = 90,
place = {United States},
year = {2019},
month = {6}
}
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