3D printed structures for optimized carbon capture technology in packed bed columns

Bolton, Stephen R.; Kasturi, Abishek; Palko, Scott; Lai, Canhai; Love, Lonnie; Parks, Jim; Xin, Sun; Tsouris, Costas

doi:10.1080/01496395.2019.1622566

Title: 3D printed structures for optimized carbon capture technology in packed bed columns

Abstract

The use of 3D printed structured packing for the optimization of aqueous-amine based carbon capture in packed absorption columns is examined in this paper. An experimental testing system has been set up, and initial comparisons were made between metal, plastic, and 3D printed 16-inch packing elements and between three 8-inch 3D printed elements of different densities. Pressure drop measurements were obtained at various air flowrates under dry conditions. Measurements were also taken for a wet system by adding water at six different liquid flowrates. In each case, theoretical calculations for pressure drop were performed based on a model presented in the literature. It was found that, for the 16-inch dry column, the model slightly overpredicts the pressure drop. The model provides an accurate prediction for the dry 8-inch experimental data, especially for the two least dense packing elements. For the wet system, the model overpredicts the pressure drop, likely due to modeling deficiencies when the column reaches its loading limit. Furthermore, these results provide sufficient confidence to move forward with testing and process intensification of the CO₂ capture process.

Authors:

^[1];

^[2]; Palko, Scott ^[3];

^[3];

^[4]

Univ. of Delaware, Newark, DE (United States)
Georgia Inst. of Technology, Atlanta, GA (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Georgia Inst. of Technology, Atlanta, GA (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Publication Date:: 2019-06-03

Research Org.:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE Office of Fossil Energy (FE)

OSTI Identifier:: 1531255

Grant/Contract Number:: AC05-00OR22725

Resource Type:: Accepted Manuscript

Journal Name:: Separation Science and Technology

Additional Journal Information:: Journal Volume: 54; Journal Issue: 13; Journal ID: ISSN 0149-6395

Publisher:: Taylor & Francis

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 54 ENVIRONMENTAL SCIENCES; absorption column; post-combustion absorption; 3D printing; structured packing; carbon capture

Citation Formats


                    Bolton, Stephen R., Kasturi, Abishek, Palko, Scott, Lai, Canhai, Love, Lonnie, Parks, Jim, Xin, Sun, and Tsouris, Costas. 3D printed structures for optimized carbon capture technology in packed bed columns.  United States: N. p., 2019. 
Web.  doi:10.1080/01496395.2019.1622566.

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                    Bolton, Stephen R., Kasturi, Abishek, Palko, Scott, Lai, Canhai, Love, Lonnie, Parks, Jim, Xin, Sun, & Tsouris, Costas. 3D printed structures for optimized carbon capture technology in packed bed columns.  United States.  https://doi.org/10.1080/01496395.2019.1622566

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                    Bolton, Stephen R., Kasturi, Abishek, Palko, Scott, Lai, Canhai, Love, Lonnie, Parks, Jim, Xin, Sun, and Tsouris, Costas. Mon .  
"3D printed structures for optimized carbon capture technology in packed bed columns".  United States.  https://doi.org/10.1080/01496395.2019.1622566.  https://www.osti.gov/servlets/purl/1531255.

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@article{osti_1531255,

  title        = {3D printed structures for optimized carbon capture technology in packed bed columns},

  author       = {Bolton, Stephen R. and Kasturi, Abishek and Palko, Scott and Lai, Canhai and Love, Lonnie and Parks, Jim and Xin, Sun and Tsouris, Costas},

  abstractNote = {The use of 3D printed structured packing for the optimization of aqueous-amine based carbon capture in packed absorption columns is examined in this paper. An experimental testing system has been set up, and initial comparisons were made between metal, plastic, and 3D printed 16-inch packing elements and between three 8-inch 3D printed elements of different densities. Pressure drop measurements were obtained at various air flowrates under dry conditions. Measurements were also taken for a wet system by adding water at six different liquid flowrates. In each case, theoretical calculations for pressure drop were performed based on a model presented in the literature. It was found that, for the 16-inch dry column, the model slightly overpredicts the pressure drop. The model provides an accurate prediction for the dry 8-inch experimental data, especially for the two least dense packing elements. For the wet system, the model overpredicts the pressure drop, likely due to modeling deficiencies when the column reaches its loading limit. Furthermore, these results provide sufficient confidence to move forward with testing and process intensification of the CO2 capture process.},

  doi          = {10.1080/01496395.2019.1622566},

  journal      = {Separation Science and Technology},

  number       = 13,

  volume       = 54,

  place        = {United States},

  year         = {2019},

  month        = {6}

}

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Works referenced in this record:

An overview of current status of carbon dioxide capture and storage technologies
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Leung, Dennis Y. C.; Caramanna, Giorgio; Maroto-Valer, M. Mercedes
Renewable and Sustainable Energy Reviews, Vol. 39
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The global carbon budget 1959–2011
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Le Quéré, C.; Andres, R. J.; Boden, T.
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Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation
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Bhattacharyya, Rupsha; Bhanja, Kalyan; Mohan, Sadhana
International Journal of Hydrogen Energy, Vol. 41, Issue 9
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Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification
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Jiang, Kaiqi; Li, Kangkang; Yu, Hai
Chemical Engineering Journal, Vol. 347
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Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column
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The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base
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Energy & Environmental Science, Vol. 2, Issue 2
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Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture
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Lavalle, Gianluca; Lucquiaud, Mathieu; Wehrli, Marc
Chemical Engineering Science, Vol. 178
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CO ₂ Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance
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Iliuta, Ion; Iliuta, Maria C.
Industrial & Engineering Chemistry Research, Vol. 54, Issue 49
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Development of a unique modular distillation column using 3D printing
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Mardani, Saeed; Ojala, Leo S.; Uusi-Kyyny, Petri
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General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns
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Stichlmair, J.; Bravo, J. L.; Fair, J. R.
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Mechanisms of CO ₂ Capture into Monoethanolamine Solution with Different CO ₂ Loading during the Absorption/Desorption Processes
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Lv, Bihong; Guo, Bingsong; Zhou, Zuoming
Environmental Science & Technology, Vol. 49, Issue 17
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A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants
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Wang, Yuan; Zhao, Li; Otto, Alexander
Energy Procedia, Vol. 114
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Works referencing / citing this record:

Systematic Study of the Pressure Drop in Confined Geometries with the Lattice Boltzmann Method
journal, April 2018

Bufe, Alexander; Brenner, Gunther
Transport in Porous Media, Vol. 123, Issue 2
DOI: 10.1007/s11242-018-1043-0

General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns
journal, March 1989

Stichlmair, J.; Bravo, J. L.; Fair, J. R.
Gas Separation & Purification, Vol. 3, Issue 1
DOI: 10.1016/0950-4214(89)80016-7

Economic analysis of CO2 capture from natural gas combined cycles using Molten Carbonate Fuel Cells
journal, October 2014

Campanari, S.; Chiesa, P.; Manzolini, G.
Applied Energy, Vol. 130
DOI: 10.1016/j.apenergy.2014.04.011

Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification
journal, September 2018

Jiang, Kaiqi; Li, Kangkang; Yu, Hai
Chemical Engineering Journal, Vol. 347
DOI: 10.1016/j.cej.2018.04.103

Development of a unique modular distillation column using 3D printing
journal, November 2016

Mardani, Saeed; Ojala, Leo S.; Uusi-Kyyny, Petri
Chemical Engineering and Processing - Process Intensification, Vol. 109
DOI: 10.1016/j.cep.2016.09.001

Additive manufacturing of packings for rotating packed beds
journal, May 2018

Gładyszewski, Konrad; Skiborowski, Mirko
Chemical Engineering and Processing - Process Intensification, Vol. 127
DOI: 10.1016/j.cep.2018.02.024

Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture
journal, March 2018

Lavalle, Gianluca; Lucquiaud, Mathieu; Wehrli, Marc
Chemical Engineering Science, Vol. 178
DOI: 10.1016/j.ces.2017.12.022

Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column
journal, January 2011

Zakeri, Ali; Einbu, Aslak; Wiig, Per Oscar
Energy Procedia, Vol. 4
DOI: 10.1016/j.egypro.2011.01.095

A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants
journal, July 2017

Wang, Yuan; Zhao, Li; Otto, Alexander
Energy Procedia, Vol. 114
DOI: 10.1016/j.egypro.2017.03.1209

A study of liquid spreading in laboratory scale random packing column with an optical method supplemented with liquid holdup characteristics
journal, September 2018

Niegodajew, Paweł; Wilczyński, Michał; Marek, Maciej
Experimental Thermal and Fluid Science, Vol. 96
DOI: 10.1016/j.expthermflusci.2018.03.008

Process simulations of post-combustion CO 2 capture for coal and natural gas-fired power plants using a polyethyleneimine/silica adsorbent
journal, March 2017

Zhang, Wenbin; Sun, Chenggong; Snape, Colin E.
International Journal of Greenhouse Gas Control, Vol. 58
DOI: 10.1016/j.ijggc.2016.12.003

Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation
journal, March 2016

Bhattacharyya, Rupsha; Bhanja, Kalyan; Mohan, Sadhana
International Journal of Hydrogen Energy, Vol. 41, Issue 9
DOI: 10.1016/j.ijhydene.2016.01.106

An overview of current status of carbon dioxide capture and storage technologies
journal, November 2014

Leung, Dennis Y. C.; Caramanna, Giorgio; Maroto-Valer, M. Mercedes
Renewable and Sustainable Energy Reviews, Vol. 39
DOI: 10.1016/j.rser.2014.07.093

Mechanisms of CO ₂ Capture into Monoethanolamine Solution with Different CO ₂ Loading during the Absorption/Desorption Processes
journal, August 2015

Lv, Bihong; Guo, Bingsong; Zhou, Zuoming
Environmental Science & Technology, Vol. 49, Issue 17
DOI: 10.1021/acs.est.5b02356

CO ₂ Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance
journal, December 2015

Iliuta, Ion; Iliuta, Maria C.
Industrial & Engineering Chemistry Research, Vol. 54, Issue 49
DOI: 10.1021/acs.iecr.5b03454

Design Method for Distillation Columns Filled with Metallic, Ceramic, or Plastic Structured Packings
journal, May 1997

Gualito, J. J.; Cerino, F. J.; Cardenas, J. C.
Industrial & Engineering Chemistry Research, Vol. 36, Issue 5
DOI: 10.1021/ie960625z

The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base
journal, January 2009

House, Kurt Zenz; Harvey, Charles F.; Aziz, Michael J.
Energy & Environmental Science, Vol. 2, Issue 2
DOI: 10.1039/b811608c

The global carbon budget 1959–2011
journal, January 2012

Le Quéré, C.; Andres, R. J.; Boden, T.
Earth System Science Data Discussions, Vol. 5, Issue 2
DOI: 10.5194/essdd-5-1107-2012

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Similar Records

Title: 3D printed structures for optimized carbon capture technology in packed bed columns

Abstract

Citation Formats

An overview of current status of carbon dioxide capture and storage technologies journal, November 2014

The global carbon budget 1959–2011 journal, January 2012

Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation journal, March 2016

Separation of CO 2 from Flue Gas: A Review journal, January 2005

Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification journal, September 2018

Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column journal, January 2011

Pressure Drop Measurements on Distillation Columns journal, October 2011

Process simulations of post-combustion CO 2 capture for coal and natural gas-fired power plants using a polyethyleneimine/silica adsorbent journal, March 2017

Systematic Study of the Pressure Drop in Confined Geometries with the Lattice Boltzmann Method journal, April 2018

Additive manufacturing of packings for rotating packed beds journal, May 2018

The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base journal, January 2009

Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture journal, March 2018

CO 2 Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance journal, December 2015

Design Method for Distillation Columns Filled with Metallic, Ceramic, or Plastic Structured Packings journal, May 1997

A study of liquid spreading in laboratory scale random packing column with an optical method supplemented with liquid holdup characteristics journal, September 2018

Development of a unique modular distillation column using 3D printing journal, November 2016

General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns journal, March 1989

Economic analysis of CO2 capture from natural gas combined cycles using Molten Carbonate Fuel Cells journal, October 2014

Mechanisms of CO 2 Capture into Monoethanolamine Solution with Different CO 2 Loading during the Absorption/Desorption Processes journal, August 2015

A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants journal, July 2017

Systematic Study of the Pressure Drop in Confined Geometries with the Lattice Boltzmann Method journal, April 2018

General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns journal, March 1989

Economic analysis of CO2 capture from natural gas combined cycles using Molten Carbonate Fuel Cells journal, October 2014

Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification journal, September 2018

Development of a unique modular distillation column using 3D printing journal, November 2016

Additive manufacturing of packings for rotating packed beds journal, May 2018

Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture journal, March 2018

Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column journal, January 2011

A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants journal, July 2017

A study of liquid spreading in laboratory scale random packing column with an optical method supplemented with liquid holdup characteristics journal, September 2018

Process simulations of post-combustion CO 2 capture for coal and natural gas-fired power plants using a polyethyleneimine/silica adsorbent journal, March 2017

Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation journal, March 2016

An overview of current status of carbon dioxide capture and storage technologies journal, November 2014

Mechanisms of CO 2 Capture into Monoethanolamine Solution with Different CO 2 Loading during the Absorption/Desorption Processes journal, August 2015

CO 2 Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance journal, December 2015

Design Method for Distillation Columns Filled with Metallic, Ceramic, or Plastic Structured Packings journal, May 1997

The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base journal, January 2009

The global carbon budget 1959–2011 journal, January 2012

An overview of current status of carbon dioxide capture and storage technologies
journal, November 2014

The global carbon budget 1959–2011
journal, January 2012

Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation
journal, March 2016

Separation of CO ₂ from Flue Gas: A Review
journal, January 2005

Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification
journal, September 2018

Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column
journal, January 2011

Pressure Drop Measurements on Distillation Columns
journal, October 2011

Process simulations of post-combustion CO 2 capture for coal and natural gas-fired power plants using a polyethyleneimine/silica adsorbent
journal, March 2017

Systematic Study of the Pressure Drop in Confined Geometries with the Lattice Boltzmann Method
journal, April 2018

Additive manufacturing of packings for rotating packed beds
journal, May 2018

The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base
journal, January 2009

Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture
journal, March 2018

CO ₂ Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance
journal, December 2015

Design Method for Distillation Columns Filled with Metallic, Ceramic, or Plastic Structured Packings
journal, May 1997

A study of liquid spreading in laboratory scale random packing column with an optical method supplemented with liquid holdup characteristics
journal, September 2018

Development of a unique modular distillation column using 3D printing
journal, November 2016

General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns
journal, March 1989

Economic analysis of CO2 capture from natural gas combined cycles using Molten Carbonate Fuel Cells
journal, October 2014

Mechanisms of CO ₂ Capture into Monoethanolamine Solution with Different CO ₂ Loading during the Absorption/Desorption Processes
journal, August 2015

A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants
journal, July 2017

Systematic Study of the Pressure Drop in Confined Geometries with the Lattice Boltzmann Method
journal, April 2018

General model for prediction of pressure drop and capacity of countercurrent gas/liquid packed columns
journal, March 1989

Economic analysis of CO2 capture from natural gas combined cycles using Molten Carbonate Fuel Cells
journal, October 2014

Piperazine-promoted aqueous-ammonia-based CO2 capture: Process optimisation and modification
journal, September 2018

Development of a unique modular distillation column using 3D printing
journal, November 2016

Additive manufacturing of packings for rotating packed beds
journal, May 2018

Cross-flow structured packing for the process intensification of post-combustion carbon dioxide capture
journal, March 2018

Experimental investigation of pressure drop, liquid hold-up and mass transfer parameters in a 0.5 m diameter absorber column
journal, January 2011

A Review of Post-combustion CO2 Capture Technologies from Coal-fired Power Plants
journal, July 2017

A study of liquid spreading in laboratory scale random packing column with an optical method supplemented with liquid holdup characteristics
journal, September 2018

Process simulations of post-combustion CO 2 capture for coal and natural gas-fired power plants using a polyethyleneimine/silica adsorbent
journal, March 2017

Simulation studies of the characteristics of a cryogenic distillation column for hydrogen isotope separation
journal, March 2016

An overview of current status of carbon dioxide capture and storage technologies
journal, November 2014

Mechanisms of CO ₂ Capture into Monoethanolamine Solution with Different CO ₂ Loading during the Absorption/Desorption Processes
journal, August 2015

CO ₂ Removal in Packed-Bed Columns and Hollow-Fiber Membrane Reactors. Investigation of Reactor Performance
journal, December 2015

Design Method for Distillation Columns Filled with Metallic, Ceramic, or Plastic Structured Packings
journal, May 1997

The energy penalty of post-combustion CO2 capture & storage and its implications for retrofitting the U.S. installed base
journal, January 2009

The global carbon budget 1959–2011
journal, January 2012