Microstructure Development of 308L Stainless Steel During Additive Manufacturing
Abstract
In situ high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid-solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure. (C) The Minerals, Metals & Materials Society and ASM International 2019
- Authors:
-
[1];
[1];
[1];
[1];
[1];
- Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
- Colorado School of Mines, Golden, CO (United States)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Publication Date:
- Research Org.:
- Los Alamos National Laboratory (LANL), Los Alamos, NM (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Laboratory Directed Research and Development (LDRD) Program; USDOE Office of Science (SC)
- OSTI Identifier:
- 1511613
- Alternate Identifier(s):
- OSTI ID: 1530877
- Report Number(s):
- LA-UR-18-29774
Journal ID: ISSN 1073-5623
- Grant/Contract Number:
- 89233218CNA000001; AC52-06NA25396; AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science
- Additional Journal Information:
- Journal Volume: 50; Journal Issue: 5; Journal ID: ISSN 1073-5623
- Publisher:
- ASM International
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 42 ENGINEERING; additive manufacture
Citation Formats
Brown, Donald William, Losko, Adrian Simon, Carpenter, John S., Cooley, Jason Christopher, Clausen, Bjorn, Dahal, Jinesh, Kenesei, Peter, and Park, J. S. Microstructure Development of 308L Stainless Steel During Additive Manufacturing. United States: N. p., 2019.
Web. doi:10.1007/s11661-019-05169-1.
Brown, Donald William, Losko, Adrian Simon, Carpenter, John S., Cooley, Jason Christopher, Clausen, Bjorn, Dahal, Jinesh, Kenesei, Peter, & Park, J. S. Microstructure Development of 308L Stainless Steel During Additive Manufacturing. United States. https://doi.org/10.1007/s11661-019-05169-1
Brown, Donald William, Losko, Adrian Simon, Carpenter, John S., Cooley, Jason Christopher, Clausen, Bjorn, Dahal, Jinesh, Kenesei, Peter, and Park, J. S. Fri .
"Microstructure Development of 308L Stainless Steel During Additive Manufacturing". United States. https://doi.org/10.1007/s11661-019-05169-1. https://www.osti.gov/servlets/purl/1511613.
@article{osti_1511613,
title = {Microstructure Development of 308L Stainless Steel During Additive Manufacturing},
author = {Brown, Donald William and Losko, Adrian Simon and Carpenter, John S. and Cooley, Jason Christopher and Clausen, Bjorn and Dahal, Jinesh and Kenesei, Peter and Park, J. S.},
abstractNote = {In situ high-energy X-ray diffraction measurements were completed during deposition of 308L stainless steel wire onto a 304L stainless steel substrate. Attempts were made to extract microstructural features such as phase fraction and internal stress, as well as temperature evolution immediately following the deposition. The limited data that could be collected during deposition and rapid solidification are critically examined. High-energy X-rays coupled with relatively slow detectors were utilized to enable determination of orientation-dependent lattice parameters accurately enough to comment on phase strain evolution between austenite and ferrite. Information about the hydrostatic and deviatoric stress states of the constituent phases was determined on time scales that are relevant to their development. However, the time resolution of the technique was insufficient to monitor phase evolution during the solid-solid phase transformation and, more so, during solidification. Moreover, the accurate and absolute determination of inherently statistical parameters, such as phase fraction, depends critically on the ability to sample a statistically significant numbers of grains in the microstructure. (C) The Minerals, Metals & Materials Society and ASM International 2019},
doi = {10.1007/s11661-019-05169-1},
journal = {Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science},
number = 5,
volume = 50,
place = {United States},
year = {Fri Mar 15 00:00:00 EDT 2019},
month = {Fri Mar 15 00:00:00 EDT 2019}
}
Free Publicly Available Full Text
Publisher's Version of Record
Other availability
Search WorldCat to find libraries that may hold this journal
Cited by: 13 works
Citation information provided by
Web of Science
Web of Science
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Microstructure and mechanical behavior of hot-work tool steels processed by Selective Laser Melting
journal, March 2018
- Casati, Riccardo; Coduri, Mauro; Lecis, Nora
- Materials Characterization, Vol. 137
On the fatigue crack growth behavior in 316L stainless steel manufactured by selective laser melting
journal, April 2014
- Riemer, A.; Leuders, S.; Thöne, M.
- Engineering Fracture Mechanics, Vol. 120
Synchrotron applications of an amorphous silicon flat-panel detector
journal, July 2008
- Lee, John H.; Aydıner, C. Can; Almer, Jonathan
- Journal of Synchrotron Radiation, Vol. 15, Issue 5
Residual stresses in selective laser sintering and selective laser melting
journal, October 2006
- Mercelis, Peter; Kruth, Jean‐Pierre
- Rapid Prototyping Journal, Vol. 12, Issue 5
Thermal Expansion
book, January 1975
- Touloukian, Y. S.; Kirby, R. K.; Taylor, R. E.
- Thermophysical Properties of Matter - the TPRC Data Series., Vol. 12
An X-ray investigation of pure iron-nickel alloys. Part 4: the variation of lattice-parameter with composition
journal, May 1937
- Owen, E. A.; Yates, E. L.; Sully, A. H.
- Proceedings of the Physical Society, Vol. 49, Issue 3
Impact of Interlayer Dwell Time on Microstructure and Mechanical Properties of Nickel and Titanium Alloys
journal, June 2017
- Foster, B. K.; Beese, A. M.; Keist, J. S.
- Metallurgical and Materials Transactions A, Vol. 48, Issue 9
Study of grain-level deformation and residual stresses in Ti-7Al under combined bending and tension using high energy diffraction microscopy (HEDM)
journal, September 2016
- Chatterjee, K.; Venkataraman, A.; Garbaciak, T.
- International Journal of Solids and Structures, Vol. 94-95
In-situ observations of phase transformations during solidification and cooling of austenitic stainless steel welds using time-resolved x-ray diffraction
journal, September 2000
- Elmer, John W.; Wong, Joe; Ressler, Thorsten
- Scripta Materialia, Vol. 43, Issue 8
GSAS-II : the genesis of a modern open-source all purpose crystallography software package
journal, March 2013
- Toby, Brian H.; Von Dreele, Robert B.
- Journal of Applied Crystallography, Vol. 46, Issue 2
Laser additive manufacturing of metallic components: materials, processes and mechanisms
journal, May 2012
- Gu, D. D.; Meiners, W.; Wissenbach, K.
- International Materials Reviews, Vol. 57, Issue 3, p. 133-164
Experimental measurements and numerical simulation of stress and microstructure in carburized 5120 steel disks
journal, January 2001
- Rangaswamy, P.; Scherer, C. P.; Bourke, M. A. M.
- Materials Science and Engineering: A, Vol. 298, Issue 1-2
Bright x-rays reveal shifting deformation states and effects of the microstructure on the plastic deformation of crystalline materials
journal, November 2017
- Beaudoin, A. J.; Shade, P. A.; Schuren, J. C.
- Physical Review B, Vol. 96, Issue 17
Additively manufactured hierarchical stainless steels with high strength and ductility
journal, October 2017
- Wang, Y. Morris; Voisin, Thomas; McKeown, Joseph T.
- Nature Materials, Vol. 17, Issue 1
Evaluation of residual stress in stainless steel 316L and Ti6Al4V samples produced by selective laser melting
journal, April 2015
- Yadroitsev, Igor; Yadroitsava, Ina
- Virtual and Physical Prototyping, Vol. 10, Issue 2
Microstructures and Properties of 17-4 PH Stainless Steel Fabricated by Selective Laser Melting
journal, October 2012
- Murr, Lawrence E.; Martinez, Edwin; Hernandez, Jennifer
- Journal of Materials Research and Technology, Vol. 1, Issue 3
An Experimental Investigation into Additive Manufacturing-Induced Residual Stresses in 316L Stainless Steel
journal, September 2014
- Wu, Amanda S.; Brown, Donald W.; Kumar, Mukul
- Metallurgical and Materials Transactions A, Vol. 45, Issue 13
The full-field strain distribution and the evolution behavior during additive manufacturing through in-situ observation
journal, July 2018
- Xie, Ruishan; Zhao, Yue; Chen, Gaoqiang
- Materials & Design, Vol. 150
Combined in situ synchrotron micro X-ray diffraction and high-speed imaging on rapidly heated and solidified Ti–48Al under additive manufacturing conditions
journal, March 2016
- Kenel, C.; Grolimund, D.; Fife, J. L.
- Scripta Materialia, Vol. 114
Cold metal transfer (CMT) technology - An overview
journal, February 2018
- Selvi, S.; Vishvaksenan, A.; Rajasekar, E.
- Defence Technology, Vol. 14, Issue 1
Investigation of Real-Time Microstructure Evolution in Steep Thermal Gradients Using in-Situ Spatially Resolved X-ray Diffraction: A Case Study for Ti Fusion Welds
journal, December 1998
- Ressler, Thorsten; Wong, Joe; Elmer, John W.
- The Journal of Physical Chemistry B, Vol. 102, Issue 52
Cryogenically cooled bent double-Laue monochromator for high-energy undulator X-rays (50–200 keV)
journal, August 2002
- Shastri, S. D.; Fezzaa, K.; Mashayekhi, A.
- Journal of Synchrotron Radiation, Vol. 9, Issue 5
The use of high energy X-rays from the Advanced Photon Source to study stresses in materials
journal, June 2005
- Haeffner, D. R.; Almer, J. D.; Lienert, U.
- Materials Science and Engineering: A, Vol. 399, Issue 1-2
Debye-Waller Factors of Cubic Metals
journal, February 1971
- Singh, Narain; Sharma, P. K.
- Physical Review B, Vol. 3, Issue 4
In situ monitoring and characterization of distortion during laser cladding of Inconel® 625
journal, June 2015
- Heigel, J. C.; Michaleris, P.; Palmer, T. A.
- Journal of Materials Processing Technology, Vol. 220
A comparative study of additive manufacturing techniques: Residual stress and microstructural analysis of CLAD and WAAM printed Ti–6Al–4V components
journal, January 2016
- Szost, Blanka A.; Terzi, Sofiane; Martina, Filomeno
- Materials & Design, Vol. 89
A study of stress relaxation in AZ31 using high-energy X-ray diffraction
journal, December 2015
- Tang, W.; Halm, K. L.; Trinkle, D. R.
- Acta Materialia, Vol. 101
Real-time monitoring of laser powder bed fusion process using high-speed X-ray imaging and diffraction
journal, June 2017
- Zhao, Cang; Fezzaa, Kamel; Cunningham, Ross W.
- Scientific Reports, Vol. 7, Issue 1
Neutron diffraction measurements of residual stress in additively manufactured stainless steel
journal, December 2016
- Brown, D. W.; Bernardin, J. D.; Carpenter, J. S.
- Materials Science and Engineering: A, Vol. 678