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Title: Instrumentation for In situ/Operando X-ray Scattering Studies of Polymer Additive Manufacturing Processes

Abstract

With new opportunities and challenges from additive manufacturing (AM), novel characterization approaches are needed to realize reliable and industry-transferrable material systems and processes. The Complex Scattering Program at the National Synchrotron Light Source II (NSLS-II), a Department of Energy (DOE) Office of Science User Research Facility located at Brookhaven National Laboratory, has capabilities on three beamlines to support in situ and operando soft material additive manufacturing measurements. In this article, we describe some of the additive manufacturing capabilities that have been implemented on these beamlines, including in-line 3D printers for Continuous-flow Direct Writing (CDW), Fused Filament Fabrication (FFF) printing, and an instrument for Electrospray Deposition (ESD). We also describe a development program in autonomous experimentation that will be critical for addressing the complexity involved in optimizing additive manufacturing processes and materials.

Authors:
 [1];  [2];  [1];  [3];  [1];  [4];  [5];  [6];  [7];  [8];  [7];  [1];  [9];  [2];  [1]
  1. Brookhaven National Lab. (BNL), Upton, NY (United States). National Synchrotron Light Source II
  2. Brookhaven National Lab. (BNL), Upton, NY (United States). Center for Functional Nanomaterials
  3. Argonne National Lab. (ANL), Argonne, IL (United States). X-ray Science Division
  4. Hebrew Univ. of Jerusalem (Israel). Casali Inst. of Applied Chemistry. The Inst. of Chemistry. Center for Nanoscience and Nanotechnology
  5. Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). The Center for Advanced Mathematics for Energy Research Applications (CAMERA)
  6. Univ. of Pennsylvania, Philadelphia, PA (United States). Dept. of Chemical and Biomolecular Engineering
  7. Stony Brook Univ., NY (United States). Dept. of Materials Science and Chemical Engineering
  8. Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States). The Center for Advanced Mathematics for Energy Research Applications (CAMERA); Univ. of California, Berkeley, CA (United States). Dept. of Mathematics
  9. Yale Univ., New Haven, CT (United States). Dept. of Chemical and Environmental Engineering
Publication Date:
Research Org.:
Brookhaven National Lab. (BNL), Upton, NY (United States); Argonne National Lab. (ANL), Argonne, IL (United States); Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Yale Univ., New Haven, CT (United States); Univ. of Pennsylvania, Philadelphia, PA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Advanced Scientific Computing Research (ASCR) (SC-21); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); BNL Laboratory Directed Research and Development (LDRD) Program; National Science Foundation (NSF)
OSTI Identifier:
1506639
Alternate Identifier(s):
OSTI ID: 1512435
Report Number(s):
BNL-211527-2019-JAAM
Journal ID: ISSN 0894-0886
Grant/Contract Number:  
SC0012704; AC02-06CH11357; AC02-05CH11231; DGE-1122492; CBET-1703494; DMR-1410568
Resource Type:
Accepted Manuscript
Journal Name:
Synchrotron Radiation News
Additional Journal Information:
Journal Volume: 32; Journal Issue: 2; Journal ID: ISSN 0894-0886
Publisher:
Taylor & Francis
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE

Citation Formats

Wiegart, L., Doerk, G. S., Fukuto, M., Lee, S., Li, R., Marom, G., Noack, M. M., Osuji, C. O., Rafailovich, M. H., Sethian, J. A., Shmueli, Y., Torres Arango, M., Toth, K., Yager, K. G., and Pindak, R. Instrumentation for In situ/Operando X-ray Scattering Studies of Polymer Additive Manufacturing Processes. United States: N. p., 2019. Web. doi:10.1080/08940886.2019.1582285.
Wiegart, L., Doerk, G. S., Fukuto, M., Lee, S., Li, R., Marom, G., Noack, M. M., Osuji, C. O., Rafailovich, M. H., Sethian, J. A., Shmueli, Y., Torres Arango, M., Toth, K., Yager, K. G., & Pindak, R. Instrumentation for In situ/Operando X-ray Scattering Studies of Polymer Additive Manufacturing Processes. United States. doi:10.1080/08940886.2019.1582285.
Wiegart, L., Doerk, G. S., Fukuto, M., Lee, S., Li, R., Marom, G., Noack, M. M., Osuji, C. O., Rafailovich, M. H., Sethian, J. A., Shmueli, Y., Torres Arango, M., Toth, K., Yager, K. G., and Pindak, R. Fri . "Instrumentation for In situ/Operando X-ray Scattering Studies of Polymer Additive Manufacturing Processes". United States. doi:10.1080/08940886.2019.1582285. https://www.osti.gov/servlets/purl/1506639.
@article{osti_1506639,
title = {Instrumentation for In situ/Operando X-ray Scattering Studies of Polymer Additive Manufacturing Processes},
author = {Wiegart, L. and Doerk, G. S. and Fukuto, M. and Lee, S. and Li, R. and Marom, G. and Noack, M. M. and Osuji, C. O. and Rafailovich, M. H. and Sethian, J. A. and Shmueli, Y. and Torres Arango, M. and Toth, K. and Yager, K. G. and Pindak, R.},
abstractNote = {With new opportunities and challenges from additive manufacturing (AM), novel characterization approaches are needed to realize reliable and industry-transferrable material systems and processes. The Complex Scattering Program at the National Synchrotron Light Source II (NSLS-II), a Department of Energy (DOE) Office of Science User Research Facility located at Brookhaven National Laboratory, has capabilities on three beamlines to support in situ and operando soft material additive manufacturing measurements. In this article, we describe some of the additive manufacturing capabilities that have been implemented on these beamlines, including in-line 3D printers for Continuous-flow Direct Writing (CDW), Fused Filament Fabrication (FFF) printing, and an instrument for Electrospray Deposition (ESD). We also describe a development program in autonomous experimentation that will be critical for addressing the complexity involved in optimizing additive manufacturing processes and materials.},
doi = {10.1080/08940886.2019.1582285},
journal = {Synchrotron Radiation News},
number = 2,
volume = 32,
place = {United States},
year = {2019},
month = {3}
}

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