Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa

doi:10.1103/PhysRevB.99.134101

Title: Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa

Abstract

Here, solid-solid and solid-liquid transformations were examined in Ge(100), using in situ x-ray diffraction measurements during uniaxial strain compression and release. For final stresses above 15.7 GPa, the Ge transformed to a highly textured tetragonal β-Sn phase. At 31.5 GPa and above, Ge transformed to the molten phase. Full stress release (uniaxial strain) from the β-Sn phase, from the melt boundary, and from the completely molten phase, resulted in reversion to an untextured cubic diamond (cd) phase. Lastly, these findings demonstrate that the cd to β-Sn phase change is reversible, and that recrystallization from the liquid phase occurs on nanosecond timescales during release.

Authors:

Renganathan, P. ^[1]; Turneaure, Stefan J. ^[1]; Sharma, Surinder M. ^[1]; Gupta, Y. M. ^[1]

Washington State Univ., Pullman, WA (United States)

Publication Date:: 2019-04-04

Research Org.:: Washington State Univ., Pullman, WA (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA), Office of Defense Programs (DP)

OSTI Identifier:: 1504945

Alternate Identifier(s):: OSTI ID: 1504944; OSTI ID: 1505006

Grant/Contract Number:: NA0002442; NA0002007; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Physical Review B

Additional Journal Information:: Journal Volume: 99; Journal Issue: 13; Journal ID: ISSN 2469-9950

Publisher:: American Physical Society (APS)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE

Citation Formats


                    Renganathan, P., Turneaure, Stefan J., Sharma, Surinder M., and Gupta, Y. M. Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa.  United States: N. p., 2019. 
        Web.  doi:10.1103/PhysRevB.99.134101.

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                    Renganathan, P., Turneaure, Stefan J., Sharma, Surinder M., & Gupta, Y. M. Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa.  United States.  doi:10.1103/PhysRevB.99.134101.

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                    Renganathan, P., Turneaure, Stefan J., Sharma, Surinder M., and Gupta, Y. M. Thu .  
        "Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa".  United States.  doi:10.1103/PhysRevB.99.134101.  https://www.osti.gov/servlets/purl/1504945.

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@article{osti_1504945,

  title        = {Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa},

  author       = {Renganathan, P. and Turneaure, Stefan J. and Sharma, Surinder M. and Gupta, Y. M.},

  abstractNote = {Here, solid-solid and solid-liquid transformations were examined in Ge(100), using in situ x-ray diffraction measurements during uniaxial strain compression and release. For final stresses above 15.7 GPa, the Ge transformed to a highly textured tetragonal β-Sn phase. At 31.5 GPa and above, Ge transformed to the molten phase. Full stress release (uniaxial strain) from the β-Sn phase, from the melt boundary, and from the completely molten phase, resulted in reversion to an untextured cubic diamond (cd) phase. Lastly, these findings demonstrate that the cd to β-Sn phase change is reversible, and that recrystallization from the liquid phase occurs on nanosecond timescales during release.},

  doi          = {10.1103/PhysRevB.99.134101},

  journal      = {Physical Review B},

  number       = 13,

  volume       = 99,

  place        = {United States},

  year         = {2019},

  month        = {4}

}

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DOI: 10.1103/PhysRevB.99.134101

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Title: Structural transformations including melting and recrystallization during shock compression and release of germanium up to 45 GPa

Abstract

Citation Formats

Axial Yield Strengths and Two Successive Phase Transition Stresses for Crystalline Silicon journal, April 1971

Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS journal, May 2018

Direct Observation of the α − ε Transition in Shock-Compressed Iron via Nanosecond X-Ray Diffraction journal, August 2005

Phase transition lowering in dynamically compressed silicon journal, September 2018

Novel metastable metallic and semiconducting germaniums journal, March 2013

Polymorphism of Iron at High Pressure journal, March 1956

In situ X-Ray Diffraction of Shock-Compressed Fused Silica journal, March 2018

Laser interferometer for measuring high velocities of any reflecting surface journal, November 1972

Real-Time Examination of Atomistic Mechanisms during Shock-Induced Structural Transformation in Silicon journal, July 2016

Axial yield strengths and phase‐transition stresses for 〈100〉, 〈110〉, and 〈111〉 germanium journal, November 1972

Time-resolved diffraction of shock-released SiO2 and diaplectic glass formation journal, November 2017

β − tin → I m m a → sh Phase Transitions of Germanium journal, March 2011

Nonequilibrium phase transitions and amorphization in Si, Si/GaAs, Ge, and Ge/GaSb at the decompression of high-pressure phases journal, March 1995

High-pressure phases of group-IV, III–V, and II–VI compounds journal, July 2003

Generating gradient germanium nanostructures by shock-induced amorphization and crystallization journal, August 2017

Direct Observations of a Dynamically Driven Phase Transition with in situ X-Ray Diffraction in a Simple Ionic Crystal journal, December 2017

First-principles study of the structural properties of Ge journal, December 1986

Pressure dependence of the Imma phase of silicon journal, July 1994

Melting of iron at the physical conditions of the Earth's core journal, January 2004

Phase transitions under shock-wave loading journal, July 1977

Pressure induced amorphization of materials journal, January 1996

The Melting Curve of Iron to 250 Gigapascals: A Constraint on the Temperature at Earth's Center journal, April 1987

Prediction of an orthorhombic phase of germanium journal, February 1994

Phase Diagrams of Silicon and Germanium to 200 kbar, 1000°C journal, December 1964

In situ X-ray diffraction study of germanium at pressures up to 11 GPa and temperatures up to 950K journal, November 2003

Shock induced phase change in KCl single crystals: Orientation relations between the B1 and B2 lattices journal, January 2009

Equation of State for Nineteen Metallic Elements from Shock‐Wave Measurements to Two Megabars journal, July 1960

Nanosecond Melting and Recrystallization in Shock-Compressed Silicon journal, September 2018

Germanium multiphase equation of state journal, May 2014

Direct Observation of Melting in Shock-Compressed Bismuth With Femtosecond X-ray Diffraction journal, August 2015

Real-Time X-Ray Diffraction Measurements of the Phase Transition in KCl Shocked along [100] journal, July 2000

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Analysis of the x-ray diffraction signal for the α − ϵ transition in shock-compressed iron: Simulation and experiment journal, November 2006

Phase transitions, Grüneisen parameter, and elasticity for shocked iron between 77 GPa and 400 GPa journal, June 1986

The MgSiO 3 system at high pressure: Thermodynamic properties of perovskite, postperovskite, and melt from global inversion of shock and static compression data : MgSiO journal, January 2009

Two-dimensional detector software: From real detector to idealised image or two-theta scan journal, January 1996

Crystal Structures at High Pressures of Metallic Modifications of Silicon and Germanium journal, February 1963

Axial Yield Strengths and Two Successive Phase Transition Stresses for Crystalline Silicon
journal, April 1971

Simultaneous 8.2 keV phase-contrast imaging and 24.6 keV X-ray diffraction from shock-compressed matter at the LCLS
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Direct Observation of the $α − ε$ Transition in Shock-Compressed Iron via Nanosecond X-Ray Diffraction
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Novel metastable metallic and semiconducting germaniums
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Polymorphism of Iron at High Pressure
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In situ X-Ray Diffraction of Shock-Compressed Fused Silica
journal, March 2018

Laser interferometer for measuring high velocities of any reflecting surface
journal, November 1972

Real-Time Examination of Atomistic Mechanisms during Shock-Induced Structural Transformation in Silicon
journal, July 2016

Axial yield strengths and phase‐transition stresses for 〈100〉, 〈110〉, and 〈111〉 germanium
journal, November 1972

Time-resolved diffraction of shock-released SiO2 and diaplectic glass formation
journal, November 2017

$β − tin \to I m m a \to sh$ Phase Transitions of Germanium
journal, March 2011

Nonequilibrium phase transitions and amorphization in Si, Si/GaAs, Ge, and Ge/GaSb at the decompression of high-pressure phases
journal, March 1995

High-pressure phases of group-IV, III–V, and II–VI compounds
journal, July 2003

Generating gradient germanium nanostructures by shock-induced amorphization and crystallization
journal, August 2017

Direct Observations of a Dynamically Driven Phase Transition with in situ X-Ray Diffraction in a Simple Ionic Crystal
journal, December 2017

First-principles study of the structural properties of Ge
journal, December 1986

Pressure dependence of the Imma phase of silicon
journal, July 1994

Melting of iron at the physical conditions of the Earth's core
journal, January 2004

Phase transitions under shock-wave loading
journal, July 1977

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journal, January 1996

The Melting Curve of Iron to 250 Gigapascals: A Constraint on the Temperature at Earth's Center
journal, April 1987

Prediction of an orthorhombic phase of germanium
journal, February 1994

Phase Diagrams of Silicon and Germanium to 200 kbar, 1000°C
journal, December 1964

In situ X-ray diffraction study of germanium at pressures up to 11 GPa and temperatures up to 950K
journal, November 2003

Shock induced phase change in KCl single crystals: Orientation relations between the B1 and B2 lattices
journal, January 2009

Equation of State for Nineteen Metallic Elements from Shock‐Wave Measurements to Two Megabars
journal, July 1960

Nanosecond Melting and Recrystallization in Shock-Compressed Silicon
journal, September 2018

Germanium multiphase equation of state
journal, May 2014

Direct Observation of Melting in Shock-Compressed Bismuth With Femtosecond X-ray Diffraction
journal, August 2015

Real-Time X-Ray Diffraction Measurements of the Phase Transition in KCl Shocked along [100]
journal, July 2000

Melting and Polymorphism at High Pressures in Some Group IV Elements and III-V Compounds with the Diamond/Zincblende Structure
journal, April 1963

Analysis of the x-ray diffraction signal for the $α − ϵ$ transition in shock-compressed iron: Simulation and experiment
journal, November 2006

Phase transitions, Grüneisen parameter, and elasticity for shocked iron between 77 GPa and 400 GPa
journal, June 1986

The MgSiO ₃ system at high pressure: Thermodynamic properties of perovskite, postperovskite, and melt from global inversion of shock and static compression data : MgSiO
journal, January 2009

Two-dimensional detector software: From real detector to idealised image or two-theta scan
journal, January 1996

Crystal Structures at High Pressures of Metallic Modifications of Silicon and Germanium
journal, February 1963