Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research

Chen, Xinzhong; Hu, Debo; Mescall, Ryan; You, Guanjun; Basov, D. N.; Dai, Qing; Liu, Mengkun

doi:10.1002/adma.201804774

Title: Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research

Authors:

^[1]; Hu, Debo ^[2]; Mescall, Ryan ^[1]; You, Guanjun ^[3]; Basov, D. N. ^[4]; Dai, Qing ^[2]; Liu, Mengkun ^[1]

Department of Physics and Astronomy Stony Brook University Stony Brook NY 11794 USA
Division of Nanophotonics CAS Center for Excellence in Nanoscience National Center for Nanoscience and Technology Beijing 100190 China
Shanghai Key Lab of Modern Optical Systems and Engineering Research Center of Optical Instrument and System Ministry of Education University of Shanghai for Science and Technology Shanghai 200093 China
Department of Physics Columbia University New York NY 10027 USA

Publication Date:: 2019-04-01

Sponsoring Org.:: USDOE

OSTI Identifier:: 1504499

Grant/Contract Number:: DE‐SC0019443

Resource Type:: Publisher's Accepted Manuscript

Journal Name:: Advanced Materials

Additional Journal Information:: Journal Name: Advanced Materials Journal Volume: 31 Journal Issue: 24; Journal ID: ISSN 0935-9648

Publisher:: Wiley Blackwell (John Wiley & Sons)

Country of Publication:: Germany

Language:: English

Citation Formats


                    Chen, Xinzhong, Hu, Debo, Mescall, Ryan, You, Guanjun, Basov, D. N., Dai, Qing, and Liu, Mengkun. Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research.  Germany: N. p., 2019. 
Web.  doi:10.1002/adma.201804774.

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                    Chen, Xinzhong, Hu, Debo, Mescall, Ryan, You, Guanjun, Basov, D. N., Dai, Qing, & Liu, Mengkun. Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research.  Germany.  https://doi.org/10.1002/adma.201804774

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                    Chen, Xinzhong, Hu, Debo, Mescall, Ryan, You, Guanjun, Basov, D. N., Dai, Qing, and Liu, Mengkun. Mon .  
"Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research".  Germany.  https://doi.org/10.1002/adma.201804774.

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@article{osti_1504499,

  title        = {Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research},

  author       = {Chen, Xinzhong and Hu, Debo and Mescall, Ryan and You, Guanjun and Basov, D. N. and Dai, Qing and Liu, Mengkun},

  abstractNote = {},

  doi          = {10.1002/adma.201804774},

  journal      = {Advanced Materials},

  number       = 24,

  volume       = 31,

  place        = {Germany},

  year         = {2019},

  month        = {4}

}

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Journal Article Chen, Xinzhong ; Hu, Debo ; Mescall, Ryan ; ... - Advanced Materials

Not provided.
https://doi.org/10.1002/adma.201804774
Widely tuneable scattering-type scanning near-field optical microscopy using pulsed quantum cascade lasers

Journal Article Yoxall, Edward ; Rahmani, Mohsen ; Maier, Stefan A. ; ... - Applied Physics Letters

We demonstrate the use of a pulsed quantum cascade laser, wavelength tuneable between 6 and 10 μm, with a scattering-type scanning near-field optical microscope (s-SNOM). A simple method for calculating the signal-to-noise ratio (SNR) of the s-SNOM measurement is presented. For pulsed lasers, the SNR is shown to be highly dependent on the degree of synchronization between the laser pulse and the sampling circuitry; in measurements on a gold sample, the SNR is 26 with good synchronization and less than 1 without. Simulations and experimental s-SNOM images, with a resolution of 100 nm, corresponding to λ/80, and an acquisition time of lessmore »« less
https://doi.org/10.1063/1.4832859
Phase stabilized homodyne of infrared scattering type scanning near-field optical microscopy

Journal Article Xu, Xiaoji G., E-mail: xgx214@lehigh.edu ; Gilburd, Leonid ; Walker, Gilbert C., E-mail: gwalker@chem.utoronto.ca - Applied Physics Letters

Scattering type scanning near-field optical microscopy (s-SNOM) allows sub diffraction limited spatial resolution. Interferometric homodyne detection in s-SNOM can amplify the signal and extract vibrational responses based on sample absorption. A stable reference phase is required for a high quality homodyne-detected near-field signal. This work presents the development of a phase stabilization mechanism for s-SNOM to provide stable homodyne conditions. The phase stability is found to be better than 0.05 rad for the mid infrared light source. Phase stabilization results in improved near field images and vibrational spectroscopies. Spatial inhomogeneities of the boron nitride nanotubes are measured and compared.
https://doi.org/10.1063/1.4905207
Scattering-type scanning near-field optical microscopy with Akiyama piezo-probes

Journal Article Dapolito, Michael ; Chen, Xinzhong ; Li, Chaoran ; ... - Applied Physics Letters
https://doi.org/10.1063/5.0074804
Infrared Scattering Scanning Near-Field Optical Microscopy Using An External Cavity Quantum Cascade Laser For Nanoscale Chemical Imaging And Spectroscopy of Explosive Residues

Conference Craig, Ian M. ; Phillips, Mark C. ; Taubman, Matthew S. ; ...

Infrared scattering scanning near-field optical microscopy (s-SNOM) is an apertureless superfocusing technique that uses the antenna properties of a conducting atomic force microscope (AFM) tip to achieve infrared spatial resolution below the diffraction limit. The instrument can be used either in imaging mode, where a fixed wavelength light source is tuned to a molecular resonance and the AFM raster scans an image, or in spectroscopy mode where the AFM is held stationary over a feature of interest and the light frequency is varied to obtain a spectrum. In either case, a strong, stable, coherent infrared source is required. Here wemore »« less
https://doi.org/10.1117/12.2004954

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Title: Modern Scattering‐Type Scanning Near‐Field Optical Microscopy for Advanced Material Research

Citation Formats

Terahertz imaging with nanometer resolution journal, October 2003

Edge Modes and Nonlocal Conductance in Graphene Superlattices journal, January 2018

Surface-enhanced optical microscopy journal, January 1985

Nanometer-precise optical length measurement using near-field scanning optical microscopy with sharpened single carbon nanotube probe journal, March 2018

Near-field thermal imaging of optically excited gold nanostructures: scaling principles for collective heating with heat dissipation into the surrounding medium journal, January 2018

Electromagnetic interactions of molecules with metal surfaces journal, November 1984

Introduction and overview journal, December 2007

Direct observation of oxygen configuration on individual graphene oxide sheets journal, February 2018

Recovery of Permittivity and Depth from Near-Field Data as a Step toward Infrared Nanotomography journal, June 2014

Low-temperature nanospectroscopy of the structural ferroelectric phases in single-crystalline barium titanate journal, January 2018

XXIII. An application of piezo-electricity to microscopy journal, February 1932

Protein Bricks: 2D and 3D Bio-Nanostructures with Shape and Function on Demand journal, March 2018

Probing optical anisotropy of nanometer-thin van der waals microcrystals by near-field imaging journal, November 2017

Mapping three-dimensional near-field responses with reconstruction scattering-type scanning near-field optical microscopy journal, May 2017

High-frequency near-field microscopy journal, July 2002

XXXVIII. A suggested method for extending microscopic resolution into the ultra-microscopic region journal, August 1928

Determination of critical diameters for intrinsic carrier diffusion-length of GaN nanorods with cryo-scanning near-field optical microscopy journal, February 2016

Local excitation and interference of surface phonon polaritons studied by near-field infrared microscopy journal, March 2008

Nanoscale simultaneous chemical and mechanical imaging via peak force infrared microscopy journal, June 2017

A tapered parallel-plate-waveguide probe for THz near-field reflection imaging journal, January 2012

Smart polymer surfaces: mapping chemical landscapes on the nanometre scale journal, January 2010

Nanoscale Mapping and Spectroscopy of Nonradiative Hyperbolic Modes in Hexagonal Boron Nitride Nanostructures journal, February 2018

Nano-imaging of an edge-excited plasmon mode in graphene journal, January 2018

Plasmonic Nickel Nanoantennas journal, June 2011

Development of a 500 Å spatial resolution light microscope journal, January 1984

Nanoscale near-field infrared spectroscopic imaging of silica-shell/gold-core and pure silica nanoparticles journal, February 2012

Fundamental developments in infrared spectroscopic imaging for biomedical applications journal, January 2016

Plasmon Reflections by Topological Electronic Boundaries in Bilayer Graphene journal, October 2017

Terahertz Near-Field Nanoscopy of Mobile Carriers in Single Semiconductor Nanodevices journal, November 2008

THz near-field imaging journal, May 1998

Ultrafast optical switching of infrared plasmon polaritons in high-mobility graphene journal, March 2016

A study of background signals in terahertz apertureless near-field microscopy and their use for scattering-probe imaging journal, June 2009

Dipole radiation in a conducting half space journal, November 1961

Ultrafast Dynamics of Surface Plasmons in InAs by Time-Resolved Infrared Nanospectroscopy journal, July 2014

Laser heating of scanning probe tips for thermal near-field spectroscopy and imaging journal, February 2017

Scattering near-field optical microscopy of optically anisotropic systems journal, March 2005

Highly confined low-loss plasmons in graphene–boron nitride heterostructures journal, December 2014

Nanoscale Near-Field Tomography of Surface States on (Bi 0.5 Sb 0.5 ) 2 Te 3 journal, November 2018

Near-field spectroscopy of silicon dioxide thin films journal, February 2012

Broadband-infrared assessment of phonon resonance in scattering-type near-field microscopy journal, January 2011

Complexity in Strongly Correlated Electronic Systems journal, July 2005

Infrared Imaging and Spectroscopy Beyond the Diffraction Limit journal, July 2015

Nanoscale Laser Terahertz Emission Microscopy journal, October 2017

Vibrational nano-spectroscopic imaging correlating structure with intermolecular coupling and dynamics journal, April 2014

Inhomogeneous electronic state near the insulator-to-metal transition in the correlated oxide VO 2 journal, September 2009

Nanoscale plasmonic phenomena in CVD-grown MoS_2 monolayer revealed by ultra-broadband synchrotron radiation based nano-FTIR spectroscopy and near-field microscopy journal, January 2016

Observation of a Luttinger-liquid plasmon in metallic single-walled carbon nanotubes journal, July 2015

Nanoscale electrodynamics of strongly correlated quantum materials journal, November 2016

Nanoscale control over optical singularities journal, January 2018

Near-field spatial mapping of strongly interacting multiple plasmonic infrared antennas journal, January 2013

Quantitative analysis and measurements of near-field interactions in terahertz microscopes journal, January 2011

Nanoscale geochemical and geomechanical characterization of organic matter in shale journal, December 2017

Experimental demonstration of the microscopic origin of circular dichroism in two-dimensional metamaterials journal, June 2016

Material-specific mapping of metal/semiconductor/dielectric nanosystems at 10 nm resolution by backscattering near-field optical microscopy journal, January 2002

Electrostatic Image Theory for the Dielectric Prolate Spheroid journal, January 2001

Broadband Multifunctional Plasmonic Logic Gates journal, April 2018

Optical nano-imaging of gate-tunable graphene plasmons journal, June 2012

Gate-tuning of graphene plasmons revealed by infrared nano-imaging journal, June 2012

Ultrafast multi-terahertz nano-spectroscopy with sub-cycle temporal resolution journal, October 2014

Near Field Scanning Optical Microscopy (NSOM) journal, January 1986

Infrared hyperbolic metasurface based on nanostructured van der Waals materials journal, February 2018

Inhomogeneity of the ultrafast insulator-to-metal transition dynamics of VO2 journal, April 2015

Electrodynamics of Solids: Optical Properties of Electrons in Matter journal, December 2002

Surface-Enhanced Raman Spectroscopy journal, July 2008

Substrate-enhanced infrared near-field spectroscopy journal, January 2008

All-electronic terahertz nanoscopy journal, January 2018

Polaritons in van der Waals materials journal, October 2016

Artifact free time resolved near-field spectroscopy journal, January 2017

Calibrated complex impedance and permittivity measurements with scanning microwave microscopy journal, March 2014

Resolving Power of Visible Light journal, January 1956

Analytical model for quantitative prediction of material contrasts in scattering-type near-field optical microscopy journal, January 2007

Near-Field Raman Spectroscopy with Aperture Tips journal, December 2016

Internal strain tunes electronic correlations on the nanoscale journal, December 2018

Near-Field Localization in Plasmonic Superfocusing: A Nanoemitter on a Tip journal, February 2010

Near-Field Optics: Microscopy, Spectroscopy, and Surface Modification Beyond the Diffraction Limit journal, July 1992

Discrete-dipole approximation for scattering by features on surfaces by means of a two-dimensional fast Fourier transform technique journal, January 1997

Near-field diffraction by a slit: implications for superresolution microscopy journal, January 1986

Apertureless Near-Field Scanning Probes Based on Graphene Plasmonics journal, February 2017

Terahertz imaging with nanometer resolution
journal, October 2003

Edge Modes and Nonlocal Conductance in Graphene Superlattices
journal, January 2018

Surface-enhanced optical microscopy
journal, January 1985

Nanometer-precise optical length measurement using near-field scanning optical microscopy with sharpened single carbon nanotube probe
journal, March 2018

Near-field thermal imaging of optically excited gold nanostructures: scaling principles for collective heating with heat dissipation into the surrounding medium
journal, January 2018

Electromagnetic interactions of molecules with metal surfaces
journal, November 1984

Introduction and overview
journal, December 2007

Direct observation of oxygen configuration on individual graphene oxide sheets
journal, February 2018

Recovery of Permittivity and Depth from Near-Field Data as a Step toward Infrared Nanotomography
journal, June 2014

Low-temperature nanospectroscopy of the structural ferroelectric phases in single-crystalline barium titanate
journal, January 2018

XXIII. An application of piezo-electricity to microscopy
journal, February 1932

Protein Bricks: 2D and 3D Bio-Nanostructures with Shape and Function on Demand
journal, March 2018

Probing optical anisotropy of nanometer-thin van der waals microcrystals by near-field imaging
journal, November 2017

Mapping three-dimensional near-field responses with reconstruction scattering-type scanning near-field optical microscopy
journal, May 2017

High-frequency near-field microscopy
journal, July 2002

XXXVIII. A suggested method for extending microscopic resolution into the ultra-microscopic region
journal, August 1928

Determination of critical diameters for intrinsic carrier diffusion-length of GaN nanorods with cryo-scanning near-field optical microscopy
journal, February 2016

Local excitation and interference of surface phonon polaritons studied by near-field infrared microscopy
journal, March 2008

Nanoscale simultaneous chemical and mechanical imaging via peak force infrared microscopy
journal, June 2017

A tapered parallel-plate-waveguide probe for THz near-field reflection imaging
journal, January 2012

Smart polymer surfaces: mapping chemical landscapes on the nanometre scale
journal, January 2010

Nanoscale Mapping and Spectroscopy of Nonradiative Hyperbolic Modes in Hexagonal Boron Nitride Nanostructures
journal, February 2018

Nano-imaging of an edge-excited plasmon mode in graphene
journal, January 2018

Plasmonic Nickel Nanoantennas
journal, June 2011

Development of a 500 Å spatial resolution light microscope
journal, January 1984

Nanoscale near-field infrared spectroscopic imaging of silica-shell/gold-core and pure silica nanoparticles
journal, February 2012

Fundamental developments in infrared spectroscopic imaging for biomedical applications
journal, January 2016

Plasmon Reflections by Topological Electronic Boundaries in Bilayer Graphene
journal, October 2017

Terahertz Near-Field Nanoscopy of Mobile Carriers in Single Semiconductor Nanodevices
journal, November 2008

THz near-field imaging
journal, May 1998

Ultrafast optical switching of infrared plasmon polaritons in high-mobility graphene
journal, March 2016

A study of background signals in terahertz apertureless near-field microscopy and their use for scattering-probe imaging
journal, June 2009

Dipole radiation in a conducting half space
journal, November 1961

Ultrafast Dynamics of Surface Plasmons in InAs by Time-Resolved Infrared Nanospectroscopy
journal, July 2014

Laser heating of scanning probe tips for thermal near-field spectroscopy and imaging
journal, February 2017

Scattering near-field optical microscopy of optically anisotropic systems
journal, March 2005

Highly confined low-loss plasmons in graphene–boron nitride heterostructures
journal, December 2014

Nanoscale Near-Field Tomography of Surface States on (Bi _0.5 Sb _0.5 ) ₂ Te ₃
journal, November 2018

Near-field spectroscopy of silicon dioxide thin films
journal, February 2012

Broadband-infrared assessment of phonon resonance in scattering-type near-field microscopy
journal, January 2011

Complexity in Strongly Correlated Electronic Systems
journal, July 2005

Infrared Imaging and Spectroscopy Beyond the Diffraction Limit
journal, July 2015

Nanoscale Laser Terahertz Emission Microscopy
journal, October 2017

Vibrational nano-spectroscopic imaging correlating structure with intermolecular coupling and dynamics
journal, April 2014

Inhomogeneous electronic state near the insulator-to-metal transition in the correlated oxide ${VO}_{2}$
journal, September 2009

Nanoscale plasmonic phenomena in CVD-grown MoS_2 monolayer revealed by ultra-broadband synchrotron radiation based nano-FTIR spectroscopy and near-field microscopy
journal, January 2016

Observation of a Luttinger-liquid plasmon in metallic single-walled carbon nanotubes
journal, July 2015

Nanoscale electrodynamics of strongly correlated quantum materials
journal, November 2016

Nanoscale control over optical singularities
journal, January 2018

Near-field spatial mapping of strongly interacting multiple plasmonic infrared antennas
journal, January 2013

Quantitative analysis and measurements of near-field interactions in terahertz microscopes
journal, January 2011

Nanoscale geochemical and geomechanical characterization of organic matter in shale
journal, December 2017

Experimental demonstration of the microscopic origin of circular dichroism in two-dimensional metamaterials
journal, June 2016

Material-specific mapping of metal/semiconductor/dielectric nanosystems at 10 nm resolution by backscattering near-field optical microscopy
journal, January 2002

Electrostatic Image Theory for the Dielectric Prolate Spheroid
journal, January 2001

Broadband Multifunctional Plasmonic Logic Gates
journal, April 2018

Optical nano-imaging of gate-tunable graphene plasmons
journal, June 2012

Gate-tuning of graphene plasmons revealed by infrared nano-imaging
journal, June 2012

Ultrafast multi-terahertz nano-spectroscopy with sub-cycle temporal resolution
journal, October 2014

Near Field Scanning Optical Microscopy (NSOM)
journal, January 1986

Infrared hyperbolic metasurface based on nanostructured van der Waals materials
journal, February 2018

Inhomogeneity of the ultrafast insulator-to-metal transition dynamics of VO2
journal, April 2015

Electrodynamics of Solids: Optical Properties of Electrons in Matter
journal, December 2002

Surface-Enhanced Raman Spectroscopy
journal, July 2008

Substrate-enhanced infrared near-field spectroscopy
journal, January 2008

All-electronic terahertz nanoscopy
journal, January 2018

Polaritons in van der Waals materials
journal, October 2016

Artifact free time resolved near-field spectroscopy
journal, January 2017

Calibrated complex impedance and permittivity measurements with scanning microwave microscopy
journal, March 2014

Resolving Power of Visible Light
journal, January 1956

Analytical model for quantitative prediction of material contrasts in scattering-type near-field optical microscopy
journal, January 2007

Near-Field Raman Spectroscopy with Aperture Tips
journal, December 2016

Internal strain tunes electronic correlations on the nanoscale
journal, December 2018

Near-Field Localization in Plasmonic Superfocusing: A Nanoemitter on a Tip
journal, February 2010

Near-Field Optics: Microscopy, Spectroscopy, and Surface Modification Beyond the Diffraction Limit
journal, July 1992

Discrete-dipole approximation for scattering by features on surfaces by means of a two-dimensional fast Fourier transform technique
journal, January 1997

Near-field diffraction by a slit: implications for superresolution microscopy
journal, January 1986

Apertureless Near-Field Scanning Probes Based on Graphene Plasmonics
journal, February 2017

Tuning quantum nonlocal effects in graphene plasmonics
journal, June 2017

Carrier dynamics in semiconductors studied with time-resolved terahertz spectroscopy
journal, June 2011