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Title: Mapping the mechanical properties of rocks using automated microindentation tests

Abstract

A microindentation scanner is constructed that measures the spatial fluctuation in the elastic properties of natural rocks. This novel instrument performs automated indentation tests on the surface of a rock slab and outputs 2-D maps of the indentation modulus at submillimeter resolution. Maps obtained for clean, well-consolidated, sandstone are presented and demonstrate the capabilities of the instrument. We postulate that the elastic structure of sandstones correlates well with their visual appearance. Moreover, we observe that the probability distribution of the indentation modulus fluctuations across the slab surfaces can be modeled using a lognormal probability density function. To illustrate possible use of the data obtained with the microindentation scanner, we use roughly 10 cm × 10 cm scans with millimeter resolution over four sandstone planar slabs to numerically compute the overall drained elastic moduli for each sandstone sample. We demonstrate that such numerically computed moduli are well modeled using the multicomponent form of the Hashin-Shtrikman lower bound that employs the observed lognormal probability distribution for the mesoscopic-scale moduli (the geometric mean works almost the same). We also compute the seismic attenuation versus frequency associated with wave-induced fluid flow between the heterogeneities in the scanned sandstones and report relatively small values formore » the inverse quality factor (Q -1<10 -2) in the seismic frequency band 10 2 Hz 4 Hz. The numerically computed frequency dependence in the attenuation varies from one type of sandstone to another, and we determine vital anisotropy in the attenuation associated with waves propagating in different directions.« less

Authors:
 [1];  [2]
  1. Institut de Physique du Globe de Paris, Paris (France)
  2. Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Publication Date:
Research Org.:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22); European Union Seventh Framework Program
OSTI Identifier:
1501368
Grant/Contract Number:  
AC02-05CH11231
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Geophysical Research. Solid Earth
Additional Journal Information:
Journal Volume: 120; Journal Issue: 10; Journal ID: ISSN 2169-9313
Publisher:
American Geophysical Union
Country of Publication:
United States
Language:
English
Subject:
58 GEOSCIENCES; mechanical properties of rocks; indentation; poroelasticity; attenuation

Citation Formats

Masson, Yder, and Pride, Steven R. Mapping the mechanical properties of rocks using automated microindentation tests. United States: N. p., 2015. Web. doi:10.1002/2015JB012248.
Masson, Yder, & Pride, Steven R. Mapping the mechanical properties of rocks using automated microindentation tests. United States. doi:10.1002/2015JB012248.
Masson, Yder, and Pride, Steven R. Tue . "Mapping the mechanical properties of rocks using automated microindentation tests". United States. doi:10.1002/2015JB012248. https://www.osti.gov/servlets/purl/1501368.
@article{osti_1501368,
title = {Mapping the mechanical properties of rocks using automated microindentation tests},
author = {Masson, Yder and Pride, Steven R.},
abstractNote = {A microindentation scanner is constructed that measures the spatial fluctuation in the elastic properties of natural rocks. This novel instrument performs automated indentation tests on the surface of a rock slab and outputs 2-D maps of the indentation modulus at submillimeter resolution. Maps obtained for clean, well-consolidated, sandstone are presented and demonstrate the capabilities of the instrument. We postulate that the elastic structure of sandstones correlates well with their visual appearance. Moreover, we observe that the probability distribution of the indentation modulus fluctuations across the slab surfaces can be modeled using a lognormal probability density function. To illustrate possible use of the data obtained with the microindentation scanner, we use roughly 10 cm × 10 cm scans with millimeter resolution over four sandstone planar slabs to numerically compute the overall drained elastic moduli for each sandstone sample. We demonstrate that such numerically computed moduli are well modeled using the multicomponent form of the Hashin-Shtrikman lower bound that employs the observed lognormal probability distribution for the mesoscopic-scale moduli (the geometric mean works almost the same). We also compute the seismic attenuation versus frequency associated with wave-induced fluid flow between the heterogeneities in the scanned sandstones and report relatively small values for the inverse quality factor (Q-1<10-2) in the seismic frequency band 102 Hz 4 Hz. The numerically computed frequency dependence in the attenuation varies from one type of sandstone to another, and we determine vital anisotropy in the attenuation associated with waves propagating in different directions.},
doi = {10.1002/2015JB012248},
journal = {Journal of Geophysical Research. Solid Earth},
number = 10,
volume = 120,
place = {United States},
year = {2015},
month = {9}
}

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Works referenced in this record:

An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments
journal, June 1992

  • Oliver, W. C.; Pharr, G. M.
  • Journal of Materials Research, Vol. 7, Issue 06, p. 1564-1583
  • DOI: 10.1557/JMR.1992.1564