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Title: Fly scan apparatus for high pressure research using diamond anvil cells

Journal Article · · Review of Scientific Instruments
DOI: https://doi.org/10.1063/1.5057445 · OSTI ID:1494058
ORCiD logo [1];  [1];  [1]
  1. Argonne National Lab. (ANL), Argonne, IL (United States)
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In this paper, the hardware and software used to execute fly scans at Sector 16 of the Advanced Photon Source is described. The system design and capabilities address dimensions and time scales relevant to samples in high pressure diamond anvil cells. The time required for routine sample positioning and centering is significantly reduced and, more importantly, the time savings associated with fly scanning makes it feasible for users to routinely generate two-dimensional x-ray transmission and x-ray diffraction maps. Consequently, this facilitates an important shift in high pressure research as experimentalists embrace the study of heterogeneous and minute sample volumes in the diamond anvil cell.

Research Organization:
Argonne National Laboratory (ANL), Argonne, IL (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division
Grant/Contract Number:
AC02-06CH11357; FG02-99ER45775
OSTI ID:
1494058
Journal Information:
Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 1 Vol. 90; ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)Copyright Statement
Country of Publication:
United States
Language:
English

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Selected techniques in diamond anvil cell crystallography: centring samples using X-ray transmission and rocking powder samples to improve X-ray diffraction image quality journal November 2008
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Formation of Optical Images by X-Rays journal January 1948
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Cited By (1)

Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments journal February 2019

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