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Title: Antisolvent processing of lead halide perovskite thin films studied by in situ X-ray diffraction


The conversion mechanism from the precursor ink to the perovskite film using antisolvent-induced crystallization has been studied usingin situX-ray diffraction during blade coating and antisolvent deposition.

ORCiD logo [1];  [1]
  1. SLAC National Accelerator Lab., Menlo Park, CA (United States)
Publication Date:
Research Org.:
SLAC National Accelerator Lab., Menlo Park, CA (United States)
Sponsoring Org.:
OSTI Identifier:
Alternate Identifier(s):
OSTI ID: 1474756; OSTI ID: 1491404
Grant/Contract Number:  
ECCS-1542152; AC02-76SF00515
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Materials Chemistry. A
Additional Journal Information:
Journal Volume: 6; Journal Issue: 39; Journal ID: ISSN 2050-7488
Royal Society of Chemistry
Country of Publication:
United States

Citation Formats

Bruening, Karsten, and Tassone, Christopher J. Antisolvent processing of lead halide perovskite thin films studied by in situ X-ray diffraction. United States: N. p., 2018. Web.
Bruening, Karsten, & Tassone, Christopher J. Antisolvent processing of lead halide perovskite thin films studied by in situ X-ray diffraction. United States.
Bruening, Karsten, and Tassone, Christopher J. Tue . "Antisolvent processing of lead halide perovskite thin films studied by in situ X-ray diffraction". United States.
title = {Antisolvent processing of lead halide perovskite thin films studied by in situ X-ray diffraction},
author = {Bruening, Karsten and Tassone, Christopher J.},
abstractNote = {The conversion mechanism from the precursor ink to the perovskite film using antisolvent-induced crystallization has been studied usingin situX-ray diffraction during blade coating and antisolvent deposition.},
doi = {10.1039/c8ta06025h},
journal = {Journal of Materials Chemistry. A},
number = 39,
volume = 6,
place = {United States},
year = {2018},
month = {9}

Journal Article:
Free Publicly Available Full Text
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Cited by: 2 works
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Figures / Tables:

Fig. 1 Fig. 1: Experimental setup and observation of phase transitions of blade coated films during drying. (a) Schematic of blade coating setup with in situ X-ray diffraction. (b–d) [(b) DMF, (c) NMP, (d) DMSO] evolution of film thickness (blue dots), integrated crystalline intermediate XRD signal (a.u., red squares), integrated perovskite XRDmore » signal (a.u., black circles), film color (red channel on ordinate, curve plotted in actual film color) over time (after blade coating) during drying at room temperature. The time window for optimum antisolvent deposition is indicated in green.« less

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    Works referencing / citing this record:

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