skip to main content

DOE PAGESDOE PAGES

Title: Erratum: “A high precision gas flow cell for performing in situ neutron studies of local atomic structure in catalytic materials” [Rev. Sci. Instrum. 88, 034101 (2017)]

We report that in the original paper,1 the following chemical formula was reported erroneously: Na 78-2xCa xAl 78Si 144O 384, x ≈ 38. The correct formula for the material studied is Na 86-2xCa xAl 86Si 106O 384, x ≈ 43. The difference in formula values between this corrected composition and values in Table 1 has no effect on the refinement quality (within the reported error), the subsequent analysis, or overall conclusions of the manuscript. Specifically, the neutron diffraction data and crystallographic refinement are insensitive (within the reported error) to the corresponding change in the Si/Al ratios, and the corrected number of Ca (x ≈ 43) is found to be within the error of the value reported via crystallographic refinement of the Ca occupancy [x = 46(3)].
Authors:
ORCiD logo [1] ; ORCiD logo [1] ; ORCiD logo [2] ; ORCiD logo [1] ; ORCiD logo [1] ;  [1] ; ORCiD logo [1] ; ORCiD logo [2] ; ORCiD logo [1] ; ORCiD logo [1] ;  [2]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Colorado State Univ., Fort Collins, CO (United States)
Publication Date:
Grant/Contract Number:
AC05-00OR22725
Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 88; Journal Issue: 9; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Research Org:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org:
USDOE
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 36 MATERIALS SCIENCE
OSTI Identifier:
1490617
Alternate Identifier(s):
OSTI ID: 1398820

Olds, Daniel P., Page, Katharine L., Paecklar, Arnold, Peterson, Peter F., Liu, Jue, Rucker, Gerald M., Ruiz-Rodriguez, Mariano M., Olsen, Michael, Pawel, Michelle D., Overbury, Steven, and Neilson, James R.. Erratum: “A high precision gas flow cell for performing in situ neutron studies of local atomic structure in catalytic materials” [Rev. Sci. Instrum. 88, 034101 (2017)]. United States: N. p., Web. doi:10.1063/1.5000452.
Olds, Daniel P., Page, Katharine L., Paecklar, Arnold, Peterson, Peter F., Liu, Jue, Rucker, Gerald M., Ruiz-Rodriguez, Mariano M., Olsen, Michael, Pawel, Michelle D., Overbury, Steven, & Neilson, James R.. Erratum: “A high precision gas flow cell for performing in situ neutron studies of local atomic structure in catalytic materials” [Rev. Sci. Instrum. 88, 034101 (2017)]. United States. doi:10.1063/1.5000452.
Olds, Daniel P., Page, Katharine L., Paecklar, Arnold, Peterson, Peter F., Liu, Jue, Rucker, Gerald M., Ruiz-Rodriguez, Mariano M., Olsen, Michael, Pawel, Michelle D., Overbury, Steven, and Neilson, James R.. 2017. "Erratum: “A high precision gas flow cell for performing in situ neutron studies of local atomic structure in catalytic materials” [Rev. Sci. Instrum. 88, 034101 (2017)]". United States. doi:10.1063/1.5000452. https://www.osti.gov/servlets/purl/1490617.
@article{osti_1490617,
title = {Erratum: “A high precision gas flow cell for performing in situ neutron studies of local atomic structure in catalytic materials” [Rev. Sci. Instrum. 88, 034101 (2017)]},
author = {Olds, Daniel P. and Page, Katharine L. and Paecklar, Arnold and Peterson, Peter F. and Liu, Jue and Rucker, Gerald M. and Ruiz-Rodriguez, Mariano M. and Olsen, Michael and Pawel, Michelle D. and Overbury, Steven and Neilson, James R.},
abstractNote = {We report that in the original paper,1 the following chemical formula was reported erroneously: Na78-2xCaxAl78Si144O384, x ≈ 38. The correct formula for the material studied is Na86-2xCaxAl86Si106O384, x ≈ 43. The difference in formula values between this corrected composition and values in Table 1 has no effect on the refinement quality (within the reported error), the subsequent analysis, or overall conclusions of the manuscript. Specifically, the neutron diffraction data and crystallographic refinement are insensitive (within the reported error) to the corresponding change in the Si/Al ratios, and the corrected number of Ca (x ≈ 43) is found to be within the error of the value reported via crystallographic refinement of the Ca occupancy [x = 46(3)].},
doi = {10.1063/1.5000452},
journal = {Review of Scientific Instruments},
number = 9,
volume = 88,
place = {United States},
year = {2017},
month = {9}
}