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Title: A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory

Abstract

The suite of neutron powder diffractometers at Oak Ridge National Laboratory (ORNL) utilizes the distinct characteristics of the Spallation Neutron Source and High Flux Isotope Reactor to enable the measurements of powder samples over an unparalleled regime at a single laboratory. Full refinements over large Q ranges, total scattering methods, fast measurements under changing conditions, and a wide array of sample environments are available. Here, this article provides a brief overview of each powder instrument at ORNL and details the complementarity across the suite. Future directions for the powder suite, including upgrades and new instruments, are also discussed.

Authors:
ORCiD logo [1]; ORCiD logo [1];  [2]; ORCiD logo [1]; ORCiD logo [1];  [3]; ORCiD logo [1]; ORCiD logo [1];  [1]; ORCiD logo [1]; ORCiD logo [1]; ORCiD logo [1]; ORCiD logo [1];  [1]; ORCiD logo [1]; ORCiD logo [1]; ORCiD logo [1]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Carnegie Inst. of Washington, Washington, D.C. (United States)
  3. European Spallation Source, Lund (Sweden); Univ. of Edinburgh, Edinburgh (United Kingdom)
Publication Date:
Research Org.:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22)
OSTI Identifier:
1485000
Alternate Identifier(s):
OSTI ID: 1474780
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 89; Journal Issue: 9; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION

Citation Formats

Calder, Stuart A., An, Ke, Boehler, Reinhard, Dela Cruz, Clarina R., Frontzek, Matthias D., Guthrie, M., Haberl, Bianca, Huq, Ashfia, Kimber, Simon A. J., Liu, Jue, Molaison, Jamie J., Neuefeind, Joerg C., Page, Katharine L., dos Santos, A. M., Taddei, Keith M., Tulk, Christopher, and Tucker, Matthew G. A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory. United States: N. p., 2018. Web. doi:10.1063/1.5033906.
Calder, Stuart A., An, Ke, Boehler, Reinhard, Dela Cruz, Clarina R., Frontzek, Matthias D., Guthrie, M., Haberl, Bianca, Huq, Ashfia, Kimber, Simon A. J., Liu, Jue, Molaison, Jamie J., Neuefeind, Joerg C., Page, Katharine L., dos Santos, A. M., Taddei, Keith M., Tulk, Christopher, & Tucker, Matthew G. A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory. United States. doi:10.1063/1.5033906.
Calder, Stuart A., An, Ke, Boehler, Reinhard, Dela Cruz, Clarina R., Frontzek, Matthias D., Guthrie, M., Haberl, Bianca, Huq, Ashfia, Kimber, Simon A. J., Liu, Jue, Molaison, Jamie J., Neuefeind, Joerg C., Page, Katharine L., dos Santos, A. M., Taddei, Keith M., Tulk, Christopher, and Tucker, Matthew G. Fri . "A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory". United States. doi:10.1063/1.5033906. https://www.osti.gov/servlets/purl/1485000.
@article{osti_1485000,
title = {A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory},
author = {Calder, Stuart A. and An, Ke and Boehler, Reinhard and Dela Cruz, Clarina R. and Frontzek, Matthias D. and Guthrie, M. and Haberl, Bianca and Huq, Ashfia and Kimber, Simon A. J. and Liu, Jue and Molaison, Jamie J. and Neuefeind, Joerg C. and Page, Katharine L. and dos Santos, A. M. and Taddei, Keith M. and Tulk, Christopher and Tucker, Matthew G.},
abstractNote = {The suite of neutron powder diffractometers at Oak Ridge National Laboratory (ORNL) utilizes the distinct characteristics of the Spallation Neutron Source and High Flux Isotope Reactor to enable the measurements of powder samples over an unparalleled regime at a single laboratory. Full refinements over large Q ranges, total scattering methods, fast measurements under changing conditions, and a wide array of sample environments are available. Here, this article provides a brief overview of each powder instrument at ORNL and details the complementarity across the suite. Future directions for the powder suite, including upgrades and new instruments, are also discussed.},
doi = {10.1063/1.5033906},
journal = {Review of Scientific Instruments},
number = 9,
volume = 89,
place = {United States},
year = {2018},
month = {9}
}

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Works referenced in this record:

Micromechanical characterization of casting-induced inhomogeneity in an Al0.8CoCrCuFeNi high-entropy alloy
journal, May 2011